The Effect of Elevated Temperature Exposure of Composites on the Strength Distribution of the Reinforcing Fibers

1994 ◽  
Vol 350 ◽  
Author(s):  
M. L. Gambone ◽  
F. E. Wawner

AbstractUnidirectionally-reinforced Timetal® 21S composite specimens were subjected to elevated temperature heat treatments. The SiC fibers were then chemically extracted from the matrix, and their tensile strengths were measured at room temperature. A Weibull statistical analysis of fiber strength distribution was performed to compare the Weibull parameters of fibers from the as-consolidated and heat-treated composites. Fractographic analysis of the tested fibers was used to identify the flaws which caused failure in each condition. Surface flaws were found to initiate low strength failures in all conditions, and the number of surface initiated failures increased with an increase in severity of heat-treatment. A relationship between the fiber/matrix chemical reaction and surface flaw development is demonstrated. A fracture mechanics analysis that explains the relationship between surface flaw size, fiber fracture toughness, and the measured tensile strengths is suggested.

Materials ◽  
2003 ◽  
Author(s):  
D. M. Pai ◽  
S. N. Yarmolenko ◽  
E. Freeman ◽  
L. P. Zawada

The tensile behavior of Nextel 720 fibers at elevated temperature was compared with room temperature results for both bare and monazite-coated fibers. While coated and uncoated fibers have nearly identical tensile strengths and Weibull moduli at room temperature, differences in response were seen at elevated temperature. Coated fibers tested at 1200°C were found to have a 40% drop in strength. Uncoated fibers at high temperature exhibited 55% less strength than at room temperature. However, the tensile strength distribution for uncoated fibers tested at high temperature exhibited two distinct populations, indicating two different failure mechanisms. One population showed a 50% drop while the other showed a 64% drop. The coating was thus found to have a protective effect in terms of short-duration high-temperature exposure. Further, the effect of soaking on strength was investigated by thermally soaking coated and uncoated fibers in air at 1200°C for 100 hours prior to tensile testing at elevated temperature. In this case, the long duration of thermal exposure appeared to eliminate the beneficial effects of the coating. Soaked fibers, both coated and uncoated, were found to have nearly identical strengths at 1200°C—a reduction of about 60%.


2011 ◽  
Vol 295-297 ◽  
pp. 1901-1904 ◽  
Author(s):  
Xiao Li ◽  
Kai Shi ◽  
Tao Peng ◽  
Yan Ming Liu ◽  
Hong Duo Wang

The domestic manufactured CT80, Φ33×3.18 coiled tubing is supplied as heat-treated low-alloy steel. The relationship between thermo cycle, microstructure, tensile properties and hardness were researched for butt welded joint. The results show that CT80 is very sensitive to welding heat input, and the thermo accumulation was obvious for small dimension coiled tubing, varying degrees of softening always exist in HAZ. The reasons include growing of block ferrite, decreasing and isolating of continuous directional bainite. In order to get good properties, the strength of consumable welding wire should be properly matched with base metal, keep uniform strength distribution along welded joint, and avoid the plastic strain concentrate in local area.


2019 ◽  
Vol 395 ◽  
pp. 1-15 ◽  
Author(s):  
Antonín Kříž ◽  
Vojtěch Průcha

Although heat treatment of high-speed steels has been covered in numerous treatises, their microstructure before treatment still receives insufficient attention. This article therefore explores the relationship between the initial microstructure and resultant properties in heat treated steels for cutting tools and sonotrodes (special tools for ultrasonic welding). As shown in experiments, the size of fragments of primary carbides affects the properties of the matrix after heat treatment and the precipitation of secondary carbides. Hence, the decisive factor is the method by which the initial stock is mechanically worked, as it may produce primary carbides with more uniform distribution and size. In contrast, the article lists some cases where clusters of carbides caused cracking after heat treatment. The article also covers multidirectional forging by which the desired initial microstructure is obtained.


Author(s):  
A.H. Advani ◽  
L.E. Murr ◽  
D.J. Matlock ◽  
W.W. Fisher ◽  
P.M. Tarin ◽  
...  

Plastic deformation is a key variable producing accelerated intergranular (IG) carbide precipitation and chromium-depletion (sensitization) development in stainless steels. Deformation above 20% also produces transgranular (TG) carbides and depletion in the material. Research on TG carbides in SS is, however, limited and has indicated that the precipitation is site-specific preferring twin-fault intersections in 316 SS versus deformation-induced martensite and martensite lath-boundaries in 304 SS. Evidences indicating the relation between martensite and carbides were, however, sketchy.The objective of this work was to fundamentally understand the relationship between TG carbides and strain-induced martensite in 304 SS. Since strain-induced martensite forms at twin-fault intersections in 304 SS and the crystallography of the transformation is well understood, we believed that it could be key in understanding mechanisms of carbides and sensitization in SS. A 0.051% C, 304 SS deformed to ∽33% engineering strain (40% true strain) and heat treated at 670°C/ 0.1-10h was used for the research. The study was carried out on a Hitachi H-8000 STEM at 200 kV.


1992 ◽  
Vol 23 (1) ◽  
pp. 13-26 ◽  
Author(s):  
W. H. Hendershot ◽  
L. Mendes ◽  
H. Lalande ◽  
F. Courchesne ◽  
S. Savoie

In order to determine how water flowpath controls stream chemistry, we studied both soil and stream water during spring snowmelt, 1985. Soil solution concentrations of base cations were relatively constant over time indicating that cation exchange was controlling cation concentrations. Similarly SO4 adsorption-desorption or precipitation-dissolution reactions with the matrix were controlling its concentrations. On the other hand, NO3 appeared to be controlled by uptake by plants or microorganisms or by denitrification since their concentrations in the soil fell abruptly as snowmelt proceeded. Dissolved Al and pH varied vertically in the soil profile and their pattern in the stream indicated clearly the importance of water flowpath on stream chemistry. Although Al increased as pH decreased, the relationship does not appear to be controlled by gibbsite. The best fit of calculated dissolved inorganic Al was obtained using AlOHSO4 with a solubility less than that of pure crystalline jurbanite.


1998 ◽  
Vol 25 (1) ◽  
pp. 81-86 ◽  
Author(s):  
N Hearn ◽  
J Aiello

Experimental work on prismatic concrete specimens was conducted to determine the relationship between mechanical restraint and the rate of corrosion. The current together with the changes in strain of the confining frame were monitored during the accelerated corrosion tests. The effect of mix design and cracking on the corrosion rates was also investigated. The results show that one-dimensional mechanical restraint retards the corrosion process, as indicated by the reduction in the steel loss. Improved quality of the matrix, with and without cracking, reduces the rate of steel loss. In the inferior quality concrete, the effect of cracking on the corrosion rate is minimal.Key words: corrosion, concrete, repair.


Author(s):  
Irzam Sarfraz ◽  
Muhammad Asif ◽  
Joshua D Campbell

Abstract Motivation R Experiment objects such as the SummarizedExperiment or SingleCellExperiment are data containers for storing one or more matrix-like assays along with associated row and column data. These objects have been used to facilitate the storage and analysis of high-throughput genomic data generated from technologies such as single-cell RNA sequencing. One common computational task in many genomics analysis workflows is to perform subsetting of the data matrix before applying down-stream analytical methods. For example, one may need to subset the columns of the assay matrix to exclude poor-quality samples or subset the rows of the matrix to select the most variable features. Traditionally, a second object is created that contains the desired subset of assay from the original object. However, this approach is inefficient as it requires the creation of an additional object containing a copy of the original assay and leads to challenges with data provenance. Results To overcome these challenges, we developed an R package called ExperimentSubset, which is a data container that implements classes for efficient storage and streamlined retrieval of assays that have been subsetted by rows and/or columns. These classes are able to inherently provide data provenance by maintaining the relationship between the subsetted and parent assays. We demonstrate the utility of this package on a single-cell RNA-seq dataset by storing and retrieving subsets at different stages of the analysis while maintaining a lower memory footprint. Overall, the ExperimentSubset is a flexible container for the efficient management of subsets. Availability and implementation ExperimentSubset package is available at Bioconductor: https://bioconductor.org/packages/ExperimentSubset/ and Github: https://github.com/campbio/ExperimentSubset. Supplementary information Supplementary data are available at Bioinformatics online.


2011 ◽  
Vol 261-263 ◽  
pp. 416-420 ◽  
Author(s):  
Fu Ping Jia ◽  
Heng Lin Lv ◽  
Yi Bing Sun ◽  
Bu Yu Cao ◽  
Shi Ning Ding

This paper presents the results of elevated temperatures on the compressive of high fly ash content concrete (HFCC). The specimens were prepared with three different replacements of cement by fly ash 30%, 40% and 50% by mass and the residual compressive strength was tested after exposure to elevated temperature 250, 450, 550 and 650°C and room temperature respectively. The results showed that the compressive strength apparently decreased with the elevated temperature increased. The presence of fly ash was effective for improvement of the relative strength, which was the ratio of residual compressive strength after exposure to elevated temperature and ordinary concrete. The relative compressive strength of fly ash concrete was higher than those of ordinary concrete. Based on the experiments results, the alternating simulation formula to determine the relationship among relative strength, elevated temperature and fly ash replacement is developed by using regression of results, which provides the theoretical basis for the evaluation and repair of HFCC after elevated temperature.


2007 ◽  
Vol 344 ◽  
pp. 383-390 ◽  
Author(s):  
Marion Merklein ◽  
Uwe Vogt

Tailored Heat Treated Blanks (THTB) are blanks that exhibit locally different strength specifically optimized for the succeeding forming process. The strength distribution is set by a local, short-term heat treatment modifying the mechanical properties of the material. Hence, THTB allow enhancing forming limits significantly leading to shorter and more robust manufacture process chains. In order to qualify the use of THTB under quasi series conditions, the interdependencies of the blank’s local heat treatment and the entire process chain of the car body manufacture have to be analyzed. In this respect, the impact of a short-term heat treatment on the mechanical properties of AA6181PX, a commonly used aluminum alloy in today’s car bodies, was studied. Also the influence of a short-term heat treatment on the coil lubricant, usually already applied by the material supplier, was given a closer look. Based on these experiments process restrictions for the application of THTB in an industrial automotive environment were derived and a process window for the THTB design was set up. In conclusion, strategies were defined how to enhance the found process boundaries leading to a more robust process window.


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