Synthesis of Si3N4 Powder by Thermal Decomposition of SI(NH)2
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ABSTRACTA fine white α-Si3N4 powder has been produced by the thermal decomposition of the coprecipitation product of the reaction between SiC14 and NH3. The Cl content, due to a reaction between Si(NH)2 and the NH4Cl by-product during the thermal treatment of the coprecipitate, has been reduced by using an isothermal step at ≈ 250°C in the heat treatment cycle.
2006 ◽
Vol 116-117
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pp. 505-508
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2009 ◽
Vol 60
(8)
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pp. 817-823
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2016 ◽
Vol 106
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pp. 330-341
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2019 ◽
Vol 6
(11)
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pp. 116599
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2013 ◽
Vol 30
(1)
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pp. 109-115
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1998 ◽
Vol 28
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pp. 1595-1604
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