Stress Induced Void Nucleation in Narrow Aluminum Alloy Lines

1991 ◽  
Vol 226 ◽  
Author(s):  
P. Børgesen ◽  
M. A. Korhonen ◽  
C. Basa ◽  
W. R. Lafontaine ◽  
B. Land ◽  
...  
Keyword(s):  
Cooling Rate ◽  
Aging Temperature ◽  
Void Nucleation ◽  
Grain Boundary Sliding ◽  
Nucleation And Growth ◽  
Nucleation Mechanism ◽  
Initial Cool ◽  
Boundary Sliding ◽  
Lift Off ◽  
Growth Of Voids

AbstractThe stress induced failure of passivated aluminum based metallizations is the combined result of the stress induced void nucleation and growth of voids. The present work investigates the dependence of the void nucleation on aging temperature and cooling rate. Narrow Al, Al(0.2%Cu) and Al(2%Si) lines of different widths were fabricated by lift-off and passivated with various thicknesses of Si3N4. After a 400°C anneal, the specimens were cooled directly to the selected aging temperature and aged for up to 1100 hours. Void nucleation was found to occur predominantly during the initial cool-down. The rate of nucleation varied in quite different ways with the combination of aging temperature and cooling rate for the different alloys, which is consistent with a grain boundary sliding controlled nucleation mechanism.

Stress Induced Void Nucleation in Narrow Aluminum Alloy Lines

1991 ◽  
Vol 225 ◽  
Author(s):  
P. Børgesen ◽  
M. A. Korhonen ◽  
C. Basa ◽  
W. R. LaFontaine ◽  
B. Land ◽  
...  
Keyword(s):  
Cooling Rate ◽  
Aging Temperature ◽  
Void Nucleation ◽  
Grain Boundary Sliding ◽  
Nucleation And Growth ◽  
Nucleation Mechanism ◽  
Initial Cool ◽  
Boundary Sliding ◽  
Lift Off ◽  
Growth Of Voids

ABSTRACTThe stress induced failure of passivated aluminum based metallizations is the combined result of the stress induced void nucleation and growth of voids. The present work investigates the dependence of the void nucleation on aging temperature and cooling rate. Narrow Al, Al(0.2%Cu) and Al(2%Si) lines of different widths were fabricated by lift-off and passivated with various thicknesses of Si3N4. After a 400°C anneal, the specimens were cooled directly to the selected aging temperature and aged for up to 1100 hours. Void nucleation was found to occur predominantly during the initial cool-down. The rate of nucleation varied in quite different ways with the combination of aging temperature and cooling rate for the different alloys, which is consistent with a grain boundary sliding controlled nucleation mechanism.

Dynamic Twin Nucleation at Triple Junctions in Fe-32%Ni Stainless Steel

2005 ◽  
Vol 495-497 ◽  
pp. 1159-1164
Author(s):  
Hiromi Miura ◽  
Sutandyo Andiarwanto ◽  
Tetsuo Sakai ◽  
John J. Jonas
Keyword(s):  
Stainless Steel ◽  
Grain Boundary Sliding ◽  
Nucleation Mechanism ◽  
Peak Strain ◽  
Triple Junctions ◽  
Compression Axis ◽  
Twin Nucleation ◽  
The Matrix ◽  
Boundary Sliding

The preferential initiation of dynamic recrystallization (DRX) at triple junctions (TJs) in stainless steel polycrystals was investigated in compression at 1123 K to 1323 K at a strain rate of 2 x 10-4 s-1. Nucleation appeared at TJs at strains as low as 0.1. This strain is only about 1/5 to 1/2 of the peak strain at which DRX is conventionally believed to occur extensively. Furthermore, DRX nucleation was not observed to take place at grain boundaries or in the matrix at this strain. The probability of DRX nucleation at TJs increased monotonically with strain and temperature. It also depended on the angle, y, between the compression axis and the sliding boundary. That is, when the angle, y, approaches 45 degrees, the probability of DRX nucleation at TJs is higher. These results reveal the important role of grain-boundary sliding (GBS) on DRX nucleation at TJs. It should also be noted that more than 90% of the grains nucleated at TJs were twins. Such dynamic twinning suggests that the essential DRX nucleation mechanism is twinning.

Observations oh Nucleation and Growth of Voids in Nickel

1970 ◽  
Vol 28 ◽  
pp. 414-415
Author(s):  
J. L. Brimhall ◽  
H. E. Kissinger ◽  
B. Mastel
Keyword(s):  
High Purity ◽  
Growth Stage ◽  
Elevated Temperatures ◽  
Early Growth ◽  
Nucleation And Growth ◽  
Pure Nickel ◽  
Different Temperatures ◽  
Total Fluence ◽  
Neutron Exposure ◽  
Growth Of Voids

Some information on the size and density of voids that develop in several high purity metals and alloys during irradiation with neutrons at elevated temperatures has been reported as a function of irradiation parameters. An area of particular interest is the nucleation and early growth stage of voids. It is the purpose of this paper to describe the microstructure in high purity nickel after irradiation to a very low but constant neutron exposure at three different temperatures.Annealed specimens of 99-997% pure nickel in the form of foils 75μ thick were irradiated in a capsule to a total fluence of 2.2 × 1019 n/cm2 (E > 1.0 MeV). The capsule consisted of three temperature zones maintained by heaters and monitored by thermocouples at 350, 400, and 450°C, respectively. The temperature was automatically dropped to 60°C while the reactor was down.

Examination of Fracture Interfaces in Silicon Nitride

1975 ◽  
Vol 33 ◽  
pp. 60-61
Author(s):  
Nancy J. Tighe
Keyword(s):  
Silicon Nitride ◽  
Grain Boundary ◽  
Crack Growth ◽  
Subcritical Crack Growth ◽  
Slow Crack Growth ◽  
Ceramic Materials ◽  
Grain Boundary Sliding ◽  
Boundary Phase ◽  
Turbine Engines ◽  
Boundary Sliding

Silicon nitride is one of the ceramic materials being considered for the components in gas turbine engines which will be exposed to temperatures of 1000 to 1400°C. Test specimens from hot-pressed billets exhibit flexural strengths of approximately 50 MN/m2 at 1000°C. However, the strength degrades rapidly to less than 20 MN/m2 at 1400°C. The strength degradition is attributed to subcritical crack growth phenomena evidenced by a stress rate dependence of the flexural strength and the stress intensity factor. This phenomena is termed slow crack growth and is associated with the onset of plastic deformation at the crack tip. Lange attributed the subcritical crack growth tb a glassy silicate grain boundary phase which decreased in viscosity with increased temperature and permitted a form of grain boundary sliding to occur.

INTERNAL FRICTION PEAKS CONNECTED WITH GRAIN BOUNDARY SLIDING IN Al

1983 ◽  
Vol 44 (C9) ◽  
pp. C9-759-C9-764
Author(s):  
E. Bonetti ◽  
A. Cavallini ◽  
E. Evangelista ◽  
P. Gondi
Keyword(s):  
Internal Friction ◽  
Grain Boundary ◽  
Grain Boundary Sliding ◽  
Boundary Sliding

scholarly journals Friction of Metals: A Review of Microstructural Evolution and Nanoscale Phenomena in Shearing Contacts

2021 ◽  
Vol 69 (4) ◽  
Author(s):  
Michael Chandross ◽  
Nicolas Argibay
Keyword(s):  
Shear Strength ◽  
Grain Boundary Sliding ◽  
Deformation Mechanisms ◽  
Low Friction ◽  
Friction Behavior ◽  
Important Conclusion ◽  
Fundamental Properties ◽  
Wide Range ◽  
Boundary Sliding ◽  
Metal Interfaces

AbstractThe friction behavior of metals is directly linked to the mechanisms that accommodate deformation. We examine the links between mechanisms of strengthening, deformation, and the wide range of friction behaviors that are exhibited by shearing metal interfaces. Specifically, the focus is on understanding the shear strength of nanocrystalline and nanostructured metals, and conditions that lead to low friction coefficients. Grain boundary sliding and the breakdown of Hall–Petch strengthening at the shearing interface are found to generally and predictably explain the low friction of these materials. While the following is meant to serve as a general discussion of the strength of metals in the context of tribological applications, one important conclusion is that tribological research methods also provide opportunities for probing the fundamental properties and deformation mechanisms of metals.

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