The Kinetics of Electromigration Damage in Copper Films Studied by Isothermal Resistance Change Analysis

1991 ◽  
Vol 225 ◽  
Author(s):  
C. W. Park ◽  
R. W. Vook

ABSTRACTElectromigration damage is one of the primary causes of the failure of interconnects in VLSI circuits. In this work, the response of Cu films to electromigration stress has been studied by an isothermal electrical resistance method. Accurate temperature measurement and control of Cu stripes stressed at elevated temperatures and high current densities were accomplished by use of a thin film thermistor. The activation energy and current density exponent were measured for vacuum evaporated Cu films and the values that were obtained are 0.79±0.02eV and 3.6±0.2, respectively. Scanning electron micrographs of stripes that underwent electromigration damage showed many voids in the cathode region, hillocks in the anode region, and both voids and hillocks in the rest of the stripe. The activation energies of two aluminum stripes were also measured by the same method. An average value of 0.54±0.02eV was obtained.

1992 ◽  
Vol 67 (04) ◽  
pp. 424-427 ◽  
Author(s):  
P J Gaffney ◽  
A B Heath ◽  
J W Fenton II

SummarySince 1975 an International Standard for Thrombin of low purity has been used. While this standard was stable and of value for calibrating thrombins of unknown potency the need for a pure a-thrombin standard arose both for accurate calibration and for precise measurement of thrombin inhibitors, notably hirudin. An international collaborative study was undertaken to establish the potency and stability of an ampouled pure a-thrombin preparation. A potency of 97.5 international units (95% confidence limits 86.5-98.5) was established for the new a-thrombin standard (89/ 588) using a clotting-assay procedure. Stability data at various elevated temperatures indicated that the standard could be transported and stored with no significant loss of potency.Ampoules of lyophilised a-thrombin (coded 89/588) have been recommended as an International Standard for a-thrombin with an assigned potency of 100 international units per ampoule by the International Society for Thrombosis and Haemostasis (Thrombin and its Inhibitors Sub-Committee) in Barcelona, Spain in July 1990 while the Expert Committee on Biological Standardisation and Control of the World Health Organisation will consider its status at its next meeting in Geneva in 1991.


2001 ◽  
Author(s):  
G. Mainelis ◽  
R. Gorny ◽  
K. Willeke ◽  
S. Grinshpun ◽  
T. Reponen ◽  
...  

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