Small Angle Neutron Scattering and Small Angle X-Ray Scattering from Bulk Microporous Silica

1989 ◽  
Vol 166 ◽  
Author(s):  
G. G. Long ◽  
S. Krueger ◽  
D. R. Black ◽  
J. P. Cline ◽  
P. R. Jemian ◽  
...  

ABSTRACTThe microstructure of low-density porous silica precursor (unsintered) bodies was studied as a function of starting chemistry. The ratio of colloidal silica sol to potassium silicate is known to have a marked effect on the size distribution of pores in this material, which in turn have a major impact on the resultant physical properties of the sintered product. In the present research, the sizes and the size distributions of particles underlying the pore microstructure was investigated, and it was found that the lower the amount of colloidal silica, the greater the size distribution of particle aggregates.

1968 ◽  
Vol 12 ◽  
pp. 87-96
Author(s):  
R. W. Gould ◽  
S. R. Bates

AbstractIt has been recently shown that particle size distributions can be determined from small angle x-ray scattering data. Size distributions have previously been measured in aluminum-zinc and aluminum-silver alloys containing spherical Guinier-Preston zones. Inorder to obtain the size distribution it is only necessary to calculate the Guinier radius and the Porod radius.Dispersion hardened nickel alloys containing small spherical particles of thoria appear to be amenable to this type of analysis. A nickel-20% chromium-2% ThO2 alloy was selected for this study. The particle size distribution obtained by small angle x-ray scattering is compared with the transmission electron microscopy results found in the literature.


1991 ◽  
Vol 74 (10) ◽  
pp. 2538-2546 ◽  
Author(s):  
Susan Krueger ◽  
Gabrielle G. Long ◽  
David R. Black ◽  
Dennis Minor ◽  
Pete R. Jemian ◽  
...  

2008 ◽  
Vol 460 (1-3) ◽  
pp. 173-177 ◽  
Author(s):  
Kazuyuki Hino ◽  
Rie Shingai ◽  
Takeshi Morita ◽  
Kiyohisa Toku ◽  
Takahiro Hirano ◽  
...  

2012 ◽  
Vol 7 (4) ◽  
pp. 107-116
Author(s):  
Sergey Bardakhanov ◽  
Ludmila Vikulina ◽  
Vladimir Lysenko ◽  
Andrey Nomoev ◽  
Sergey Poluyanov ◽  
...  

The possibility of application of small-angle X-ray scattering (SAXS) for nanopowders analysis was studied. The research for eight silica powders (including four powders obtained by the authors with help of electron accelerator) was conducted. The possibility of application of small angle X-ray scattering for determination of size distribution function of nanoparticles was shown


2019 ◽  
Vol 125 (1) ◽  
pp. 014301
Author(s):  
Georg Heldt ◽  
Philip Thompson ◽  
Rajesh V. Chopdekar ◽  
Joachim Kohlbrecher ◽  
Stephen Lee ◽  
...  

2006 ◽  
Vol 24 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Y. Mori ◽  
M. Furukawa ◽  
T. Hayashi ◽  
K. Nakamura

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