Influence of Heat Treatments on a NiTi Shape Memory Alloy Obtained Using Vacuum Induction Melting and Reprocessed by Plasma Skull Push-Pull

2015 ◽  
Vol 1765 ◽  
pp. 121-126 ◽  
Author(s):  
Jackson de Brito Simões ◽  
Francisco Fernando Roberto Pereira ◽  
Jorge Otubo ◽  
Carlos José de Araújo
Keyword(s):  
Shape Memory Alloy ◽  
Shape Memory ◽  
Electrical Resistance ◽  
Heat Treatments ◽  
Vacuum Induction Melting ◽  
Niti Shape Memory Alloy ◽  
Induction Melting ◽  
Thermal Treatments ◽  
Scanning Calorimetry ◽  
Thermally Induced

ABSTRACTShape memory alloys (SMA) are metallic attractive engineering materials due to their capacity to store pre-defined shapes through a thermally induced phase transition from a solid state. This paper aims to evaluate the influence of solubilization thermal treatments on a NiTi shape memory alloy originally fabricated by vacuum induction melting and then reprocessed by plasma melting followed by injection molding (Plasma Skull Push Pull process) into different metal molds (steel, aluminum, brass and copper) in order to compare the thermal properties regarding to its raw state. The thermal treatments of solubilization were carried out at 850°C in different times (2n function, n = 0, 1, 2 and 3, in hours). The influence of solubilizing treatments in the NiTi shape memory alloy was analyzed using the following characterization techniques: Differential Scanning Calorimetry (DSC) and Electrical Resistance as a function of Temperature (ERT). The results demonstrate that the solubilization heat treatments applied on the reprocessed NiTi shape memory alloy through the plasma skull push pull process, provides important changes in the phase transformation of the material. Therefore, it was demonstrated that it is necessary to solubilize the material after melting or remelting the NiTi shape memory alloy via this process to obtain mini-actuators products with homogeneous properties.

The Segregation of Chemical Composition in NiTi Shape Memory Alloy Melted by VIM in Lime Crucible

2009 ◽  
Vol 610-613 ◽  
pp. 1315-1318 ◽  
Author(s):  
Zhi Shan Yuan ◽  
Zhao Wei Feng ◽  
Jiang Bo Wang ◽  
Wei Dong Miao ◽  
Chong Jian Li ◽  
...  
Keyword(s):  
Chemical Composition ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Large Scale ◽  
Vacuum Induction Melting ◽  
Niti Shape Memory Alloy ◽  
Induction Melting ◽  
Ingot Metallurgy ◽  
Chemical Homogeneity ◽  
Section Area

Binary NiTi shape memory alloy cast ingots with large scale size are produced by using vacuum induction melting (VIM) in lime crucible, the oxygen and carbon contents are less than 500ppm. Usually, oxygen was introduced into the melts by the dissolution of lime during melting, resulting in higher content of oxygen over 500ppm. VAR + VIM ingot metallurgy is prone to produce materials with a good chemical homogeneity. However, it is difficult for one single melting of NiTi by VIM in the lime crucible. So in the present paper, the segregation of chemical composition and the consistency of transformation temperature in NiTi alloys in as-casted condition along the cross-section area on edge and center, in homogeneization-treated condition, and in as-forged condition along the longitudinal-section area on head and tail, are measured and analyzed by differential scanning calorimetry (DSC), OM, SEM, and XRD, to indicate the chemical homogeneity in microscopic and macroscopic scale.

scholarly journals Effect of Sn Addition on Phase Transformation Behavior of Equiatomic Ni-Ti Shape Memory Alloy

2020 ◽  
Vol 17 (3(Suppl.)) ◽  
pp. 0961
Author(s):  
Ali Abadi Aljubouri ◽  
Safa hasan Mohammed ◽  
Mudhafar ali Mohammed
Keyword(s):  
Phase Transformation ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Optical Microscope ◽  
Vacuum Induction Melting ◽  
Induction Melting ◽  
Micro Hardness ◽  
Transformation Behavior ◽  
Scanning Calorimetry ◽  
Phase Transformation Behavior

Sn effect on the phase transformation behavior, microstructure, and micro hardness of equiatomic Ni-Ti shape memory alloy was studied. NiTi and NiTiSn alloys were produced using vacuum induction melting process with alloys composition (50% at. Ni, 50% at.Ti) and (Ni 48% at., Ti 50% at., Sn 2% at.). The characteristics of both alloys were investigated by utilizing Differential Scanning Calorimetry, X- ray Diffraction Analysis, Scanning Electron Microscope, optical microscope and vicker's micro hardness test. The results showed that adding Sn element leads to decrease the phase transformation temperatures evidently. Both alloy samples contain NiTi matrix phase and Ti2Ni secondary phase, but the Ti2Ni phase content decreases with Sn addition and this is one of the reasons that leads to decrease the micro hardness of alloy with adding Sn element in a noticeable manner. The micro hardness decreases from 238.74 for NiTi equiatomic alloy to 202 for NiTiSn alloy after heat treatment.

Modeling of Electrical Resistivity Evolution Using Free Energy Analysis for NiTi Shape Memory Alloy Wires

2011 ◽  
Vol 311-313 ◽  
pp. 2282-2285
Author(s):  
Jian Jun Zhang
Keyword(s):  
Electrical Resistivity ◽  
Free Energy ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Free Energy Change ◽  
Energy Change ◽  
Niti Shape Memory Alloy ◽  
Scanning Calorimetry ◽  
Proposed Model ◽  
Free Energy Analysis

This paper presents a transformation kinetics model of NiTi shape memory alloy (SMA) wires based on electrical resistivity (ER) derivative study under the assumption that the derivative of electrical resistivity with respect to temperature is in linear relationship with the derivative of free energy change with respect to temperature. Free energy change and electrical resistivity properties of SMA are analyzed based on differential scanning calorimetry (DSC) experiments during phase transformation. The simulated evolution of electrical resistivity during thermomechanical transformation is presented using the proposed model.

NiTi Shape Memory Alloy Used for Multiple-Resetting Actuator for Fire Protection

2017 ◽  
Vol 907 ◽  
pp. 8-13 ◽  
Author(s):  
Lucian Burlacu ◽  
Nicanor Cimpoeşu ◽  
Nicoleta Monica Lohan ◽  
Leandru Gheorghe Bujoreanu
Keyword(s):  
Thermal Analysis ◽  
Shape Memory Alloy ◽  
Shape Memory ◽  
Fire Protection ◽  
Room Temperature ◽  
Parent Phase ◽  
Niti Shape Memory Alloy ◽  
Scanning Calorimetry ◽  
Protection Systems ◽  
Executive Elements

The paper introduces the possibility to replace the “wet alloy”, used for sprinkler-triggering within automatic fire protection systems, with a shape memory alloy (SMA) type. The idea of the present application is based on the thermoelastic reversible martensitic transformation, governing SMA functioning, which has completely reversible character, and enables the occurrence of two-way shape memory effect (TWSME) after the application of a thermomechanical treatment called “training”. For this purpose a commercial NiTi rod, which was martensitic at room temperature, was subjected to thermal analysis tests, performed by differential scanning calorimetry (DSC) and dilatometry. Martensite (M) reversion to parent phase (A), during heating, was emphasized by an endothermic peak on the DSC thermogram and by a length shrinkage, on the dilatogram. The capacity to develop TWSME was revealed by the change in displacement-temperature variation, with increasing the number of training cycles. This stabilized fully reversible behavior recommends NiTi rods as executive elements of a new concept of resettable sprinkler for fire protection.

Response of Optical Fiber Bragg Sensors With a Thin Film Shape Memory Alloy Coating

2008 ◽  
Author(s):  
K. P. Mohanchadra ◽  
Michael C. Emmons ◽  
Sunny Karnani ◽  
Gregory P. Carman ◽  
W. Lance Richards
Keyword(s):  
Thin Film ◽  
Shape Memory Alloy ◽  
Optical Fiber ◽  
Shape Memory ◽  
Alloy Coating ◽  
Niti Shape Memory Alloy ◽  
Alloy Thin Film ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Transformation Temperatures

This paper describes the sputter deposition and characterization of nickel titanium (NiTi) shape memory alloy thin film onto the surface of an optical fiber Bragg sensor. The NiTi coating uniformity, crystallinity and transformation temperatures are measured using scanning electron microsocopy, x-ray diffraction and differential scanning calorimetry respectively. The strain in the optical fiber is measured using centroid calculation of wavelength shifts. Results show distinct and abrupt changes in the optical fiber signal with the four related transformation temperatures represented by the austenite-martensite forward and reverse phase transformations. These tests demonstrate a coupling present between optical energy and thermal energy, i.e. a modified multiferroic material.

An Innovative Laser-Processed NiTi Self-Biasing Linear Actuator

2013 ◽  
Author(s):  
B. Panton ◽  
A. Michael ◽  
A. Pequegnat ◽  
M. Daly ◽  
Y. Zhou ◽  
...  
Keyword(s):  
Shape Memory Alloy ◽  
Shape Memory ◽  
Laser Energy ◽  
Current Control ◽  
Niti Shape Memory Alloy ◽  
Scanning Calorimetry ◽  
Material Technology ◽  
Thermomechanical Characteristics ◽  
Alloy Material ◽  
Local Modification

The revolutionary multiple memory material technology allows local modification of shape memory alloy functional properties to create monolithic actuators that exhibit several different thermomechanical characteristics. In this work, high density laser energy was used to process a monolithic piece of NiTi shape memory alloy material to allow synergistic pseudoelastic and shape memory effect behavior. The resulting actuator contains self-biasing properties eliminating the need for a separate biasing mechanism for cyclic actuation. The characteristics of these different local behaviors were analyzed using tensile testing and differential scanning calorimetry. The stress and strain amplitude of the self-biasing linear actuation was characterized with relation to input current control. This work provides proof of concept for local modification of martensitic and austenitic phases; enabling self-biasing linear actuation.

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