Effect of Interstitial Carbon Atoms on Phase Stability and Mechanical Properties of E21 (L12) Ni3AlC1-x Single Crystals

2013 ◽  
Vol 1516 ◽  
pp. 243-248
Author(s):  
Yoshisato Kimura ◽  
Masato Kawakita ◽  
Hiroyasu Yuyama ◽  
Yaw-Wang Chai
Keyword(s):  
Mechanical Properties ◽  
Carbon Content ◽  
Single Crystals ◽  
Carbon Concentration ◽  
Room Temperature ◽  
Zone Melting ◽  
Compression Tests ◽  
Interstitial Carbon ◽  
Solute Carbon ◽  
Critical Resolved Shear Stress

ABSTRACTSingle crystals of E21 (L12) Ni3AlC1-x were prepared by the unidirectional solidification using the optical floating zone melting method to determine their mechanical properties. Particularly the effects of interstitial carbon atoms on mechanical properties were evaluated by compression tests at room temperature. Operative slip system of E21 Ni3AlC is {111}<011> type which is the same as that of L12 Ni3Al. Strength of Ni3AlC single crystals increases with carbon concentration due to the solid solution effect, though the stress relief of yielding behavior is enhanced at the intermediate carbon content at around 3at%. A large gap appears in the carbon concentration dependence of critical resolved shear stress (as well as yield stress) at almost the same carbon content. This discontinuity in strengthening is attributed to the interaction between multiple solute carbon atoms and mobile dislocations.

THE EFFECT OF ORIENTATION AND IMPURITIES ON THE MECHANICAL PROPERTIES OF MOLYBDENUM SINGLE CRYSTALS

1967 ◽  
Vol 45 (2) ◽  
pp. 1063-1074 ◽  
Author(s):  
D. F. Stein
Keyword(s):  
Mechanical Properties ◽  
Shear Stress ◽  
Single Crystals ◽  
Tensile Axis ◽  
Zone Melting ◽  
Hydrogen Gas ◽  
Axis Orientation ◽  
Stereographic Triangle ◽  
Tension And Compression ◽  
Critical Resolved Shear Stress

Molybdenum single crystals containing less than 10 p.p.m. of carbon, 5 p.p.m. of nitrogen, and 5 p.p.m. of oxygen have been prepared by zone melting and hydrogen gas purification. The mechanical properties of the crystals have been measured in tension and compression over a range of temperature from 20 to 298 °K. It was found that the critical resolved shear stress and the temperature dependence of the critical resolved shear stress decreased with increasing purity. It was found that at all test temperatures the CRSS law fails. The critical resolved shear stress is a minimum in the (100) tension axis orientation and reaches a maximum with the tensile axis along the (110)(111) line of the stereographic triangle. It was also found that the ductility of molybdenum single crystals was not improved by purification.

scholarly journals Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Zhenghao Chen ◽  
Bhaskar Paul ◽  
Sanjib Majumdar ◽  
Norihiko L. Okamoto ◽  
Kyosuke Kishida ◽  
...  
Keyword(s):  
Single Crystals ◽  
Plastic Flow ◽  
Room Temperature ◽  
Resolve Shear Stress ◽  
Temperature Deformation ◽  
Slip Systems ◽  
Compression Tests ◽  
Plastic Deformation Behavior ◽  
Bulk Single Crystals ◽  
Micropillar Compression

AbstractThe plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observed at all for their bulk single crystals at room temperature, plastic flow is successfully observed at room temperature by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> in ZrB2 and by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> in TiB2. Critical resolve shear stress values at room temperature are very high, exceeding 1 GPa for all observed slip systems; 3.01 GPa for {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> slip in ZrB2 and 1.72 GPa and 5.17 GPa, respectively for {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> slip in TiB2. The identified operative slip systems and their CRSS values are discussed in comparison with those identified in the corresponding bulk single crystals at high temperatures and those inferred from micro-hardness anisotropy in the early studies.

Plastic Deformation of Mo(Si,Al)2 Single Crystals with the C40 Structure

1996 ◽  
Vol 460 ◽  
Author(s):  
M. Moriwaki ◽  
K. Ito ◽  
H. Inui ◽  
M. Yamaguchi
Keyword(s):  
Single Crystals ◽  
Deformation Behavior ◽  
Basal Slip ◽  
Room Temperature ◽  
Slip Systems ◽  
Temperature Range ◽  
Al Content ◽  
Partial Dislocations ◽  
Increasing Temperature ◽  
Critical Resolved Shear Stress

ABSTRACTThe deformation behavior of single crystals of Mo(Si,Al)2 with the C40 structure has been studied as a function of crystal orientation and Al content in the temperature range from room temperature to 1500°C in compression. Plastic flow is possible only above 1100°C for orientations where slip along <1120> on (0001) is operative and no other slip systems are observed over whole temperature range investigated. The critical resolved shear stress for basal slip decreases rapidly with increasing temperature and the Schmid law is valid. Basal slip appears to occur through a synchroshear mechanism, in which a-dislocations (b=1/3<1120>) dissociate into two synchro-partial dislocations with the identical Burgers vector(b*1/6<1120>) and each synchro-partial further dissociates into two partials on two adjacent planes.

Influence of High Temperatures on the Mechanical Properties of Wood Bio-Concretes

2022 ◽  
Author(s):  
Amanda Lorena Dantas Aguiar ◽  
M’hamed Yassin Rajiv da Gloria ◽  
Romildo Dias Toledo Filho
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
High Temperatures ◽  
Room Temperature ◽  
Plant Biomass ◽  
Compression Tests ◽  
Wood Degradation ◽  
Cementitious Matrix ◽  
Wood Shavings ◽  
Temperature Reference

The use of wood wastes in the production of bio-concrete shows high potential for the development of sustainable civil construction, since this material, in addition to having low density, increases the energy efficiency of buildings in terms of thermal insulation. However, a concern arising from the production of bio-concretes with high amounts of plant biomass is how this material behaves when subjected to high temperatures. Therefore, this work aims to evaluate the influence of high temperatures on the mechanical properties of wood bio-concretes. The mixtures were produced with wood shavings volumetric fractions of 40, 50 and 60% and cementitious matrix composed of a combination of cement, fly ash and metakaolin. Uniaxial compression tests and scanning electron microscopy (SEM) were performed, with bio-concrete at age of 28 days, at room temperature (reference) and after exposure to temperatures of 100, 150, 200 and 250 °C. The density and compressive strength of the bio-concrete gradually decreased with increasing biomass content. Up to 200 °C, reductions in strength and densities less than 19% and 13%, respectively, were observed. At 250 °C, reductions of compressive strength reached 87%. Analysis performed by SEM showed an increase in the number of cracks in the wood-cementitious matrix interface and wood degradation by increasing the temperature.

scholarly journals The orientation dependence of the strength of ice single crystals

2000 ◽  
Vol 46 (152) ◽  
pp. 41-44 ◽  
Author(s):  
Y. L. Trickett ◽  
I. Baker ◽  
P. M. S. Pradhan
Keyword(s):  
Strain Rate ◽  
Single Crystals ◽  
Axial Strain ◽  
Constant Strain Rate ◽  
Peak Stress ◽  
Deformation Mode ◽  
Orientation Dependence ◽  
Compression Tests ◽  
Ice Flow ◽  
Critical Resolved Shear Stress

AbstractSingle crystals with a wide variety of orientations were cut from large pucks of laboratory-grown ice. Constant-strain-rate compression tests were performed on the crystals either at an axial strain rate of 1 × 10−5 s−1at –20°C or at axial strain rates from 1 × 10−6 s−1 to 1 × 10−4 s−1 at –10°C. In agreement with previous studies of ice flow, the compression tests showed a linearly rising stress with increasing strain, followed by a sharply declining stress after reaching a peak. With further strain, the sharp decline in stress slowed and the flow stress approached a plateau that was only weakly dependent on strain. For all crystallographic orientations, it was found that Schmid’s (critical resolved shear stress) law was obeyed by the peak stress. Slip lines clearly showed that basal slip was the deformation mode.

Microstructure Control of Co3AlC-Base Heat Resistant Alloys Using Optical Floating Zone Melting

2005 ◽  
Vol 475-479 ◽  
pp. 833-836 ◽  
Author(s):  
Yoshisato Kimura ◽  
Kiichi Sakai ◽  
Shinya Teramoto ◽  
Yoshinao Mishima
Keyword(s):  
Mechanical Properties ◽  
Single Phase ◽  
Zone Melting ◽  
Floating Zone ◽  
Compression Tests ◽  
Microstructure Control ◽  
Two Phase ◽  
Elevated Temperature Strength ◽  
Heat Resistant ◽  
First Time

Aiming for further improvement of mechanical properties of Co3AlC-based heat resistant alloys, microstructure control was conducted using optical floating zone (OFZ) melting. Unidirectional solidification was performed to align Co3AlC/a(Co) two-phase eutectic microstructure. Co3AlC single phase poly-crystal alloys were successfully fabricated for the first time by taking advantage of OFZ. Mechanical properties were evaluated for selected alloys by compression tests at ambient temperature, 1073 K and 1273 K. Excellent elevated temperature strength is achieved in Co3AlC single phase alloys and ductility is sufficiently improved in Co3AlC/a(Co) two-phase alloys.

Plastic Deformations in L10-Ordered Single Crystals with their c/a Ratios Less than Unity

2007 ◽  
Vol 561-565 ◽  
pp. 459-462
Author(s):  
Katsushi Tanaka ◽  
Hiromitsu Ide ◽  
Yoshinori Sumi ◽  
Kyosuke Kishida ◽  
Haruyuki Inui
Keyword(s):  
Shear Stress ◽  
Temperature Dependence ◽  
Single Crystals ◽  
Room Temperature ◽  
The Other ◽  
Compressive Deformation ◽  
Positive Temperature ◽  
Plastic Deformations ◽  
Temperature Range ◽  
Critical Resolved Shear Stress

Compressive deformation of L10-ordered single crystals of FePd whose c/a ratio less than unity have been investigated from room temperature to 823 K. The results show that the critical resolved shear stress (CRSS) for octahedral glide of ordinary dislocations is smaller than that of super-lattice dislocations in all the temperature range investigated, that is the opposite sense to the case of Ti-56 mol% Al. The CRSS for ordinary dislocations virtually independent to the temperature. On the other hand, the CRSS for super dislocations exhibits a weak positive temperature dependence from room temperature up to 573 K and decreases in higher temperatures.

Deformation of an extruded nickel beryllide between room temperature and 820 °C

1991 ◽  
Vol 6 (12) ◽  
pp. 2653-2659 ◽  
Author(s):  
G.M. Pharr ◽  
S.V. Courington ◽  
J. Wadsworth ◽  
T.G. Nieh
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Elevated Temperature ◽  
Flow Stress ◽  
Strain Hardening ◽  
Room Temperature ◽  
High Temperature Strength ◽  
Compression Tests ◽  
Tension And Compression ◽  
Better Than

The mechanical properties of nickel beryllide, NiBe, have been investigated in the temperature range 20–820 °C. The room temperature properties were studied using tension, bending, and compression tests, while the elevated temperature properties were characterized in compression only. NiBe exhibits some ductility at room temperature; the strains to failure in tension and compression are 1.3% and 13%, respectively. Fracture is controlled primarily by the cohesive strength of grain boundaries. At high temperatures, NiBe is readily deformable—strains in excess of 30% can be achieved at temperatures as low as 400 °C. Strain hardening rates are high, and the flow stress decreases monotonically with temperature. The high temperature strength of NiBe is as good or better than that of NiAl, but not quite as good as CoAl.

Room Temperature Deformation in “Soft” Orientation Nial Single Crystals

1990 ◽  
Vol 213 ◽  
Author(s):  
R.D. Field ◽  
D.F. Lahrman ◽  
R. Darolia
Keyword(s):  
Shear Stress ◽  
Elevated Temperature ◽  
Single Crystals ◽  
Room Temperature ◽  
Dislocation Motion ◽  
Temperature Deformation ◽  
Slip Planes ◽  
Schmid Factor ◽  
Critical Resolved Shear Stress ◽  
Active Slip

ABSTRACTA detailed study of deformation of NiAl single crystals in two soft orientations, <110> and <111>, has been conducted. The Schmid factor favors {100} slip in the former and {110} slip in the latter. Detailed dislocation analysis, critical resolved shear stress measurements, and slip trace analysis have been performed to determine the nature of dislocation motion and interactions in this material. Particular attention is given to prismatic loops formed during deformation, since the shapes of these loops reveal the active slip planes. Similar loop morphologies observed in elevated temperature [001] oriented tensile specimens are also discussed.

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