Film Conductivity Controlled Variation of the Amplitude Distribution of High-temperature Resonators

2011 ◽  
Vol 1299 ◽  
Author(s):  
Silja Schmidtchen ◽  
Denny Richter ◽  
Han Xia ◽  
Holger Fritze

ABSTRACTHigh-temperature measurements of the spatial distribution of the displacement characteristics of a thickness shear mode langasite (La3Ga5SiO14) resonator are obtained using a laser Doppler interferometer. Thereby, the resonator is excited in the fundamental mode and the third overtone. Further, the resonator is coated with a gas sensitive CeO2-x film which exceeds the metal electrode. In reducing atmospheres the conductivity of the film increases and induces an increase of the effective electrode area. This effect leads to a broadening of the mechanical displacement distribution. The latter depends strongly on the size of the excited part of the resonator which is determined by the effective size of the electrodes. The direct determination of the mechanical displacement at different oxygen partial pressures confirms a model as derived from the electrical impedance of resonator devices [1]. Further, information about the mass sensitivity distribution of resonators is obtained since the property is directly proportional to the amplitude.

2021 ◽  
Vol 10 (2) ◽  
pp. 271-279
Author(s):  
Michal Schulz ◽  
Rezvan Ghanavati ◽  
Fabian Kohler ◽  
Jürgen Wilde ◽  
Holger Fritze

Abstract. A temperature sensor based on piezoelectric single crystals allowing stable operation in harsh environments such as extreme temperatures and highly reducing or oxidizing atmospheres is presented. The temperature dependence of the mechanical stiffness of thickness shear mode resonators is used to determine temperature changes. The sensor is based on catangasite (Ca3TaGa3Si2O14 – CTGS), a member of a langasite crystal family. CTGS exhibits an ordered crystal structure and low acoustic losses, even at 1000 ∘C. The resonance frequency and quality factor of unhoused and of housed CTGS resonators are measured up to about 1030 ∘C. A temperature coefficient of the resonance frequency of about 200 Hz K−1 for a 5 MHz device is found and enables determination of temperature changes as small as 0.04 K. Housed CTGS resonators do not show any significant change in the resonance behavior during a 30 d, long-term test at 711 ∘C.


1995 ◽  
Vol 50 (8) ◽  
pp. 770-774 ◽  
Author(s):  
Y. Waseda ◽  
K. Sugiyama ◽  
J. M. Toguri

Abstract A high temperature X-ray diffraction study of molten alumina has been carried out at 2363 K (2090°C). The local ordering parameters in molten alumina were estimated by using the interference function refining technique. Octahedrally coordinated aluminum is suggested to remain in the melt as the fundamental local structure.


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