High temperature creep strength in a nanodispersion-strengthened ferritic alloy prepared by heavy plastic deformation

2011 ◽  
Vol 1298 ◽  
Author(s):  
David G. Morris ◽  
Maria Antonia Muñoz-Morris

ABSTRACTProcesses of severe plastic deformation have been investigated for a wide range of ductile alloys over the past decade, generally with an objective of refining the microstructural scale, for example the grain size, but have hardly been considered for intermetallics. This presentation discusses processing of a boride-containing Fe3Al alloy using a multidirectional, high-strain and high-temperature forging technique. Iron aluminides with relatively low Al contents can be regarded as Al-rich ferritic steels with outstanding oxidation-corrosion properties. However, as for many ferritic steels, they show poor creep resistance at temperatures above about 600ºC. The deformation processing leads to a material with large grain size and refined dispersion of thermally-stable boride particles. The particles produce a large increase in creep strength under conditions of moderate stresses and low strain rates at temperatures near 700ºC. This high-strain forging technique can be seen as an intermediate processing method between conventional wrought metallurgy and mechanical-alloying powder metallurgy, whereby an initially coarse and inhomogeneous dispersion of second phase is refined and made more homogeneous, and can be considered as a useful processing technique for a wide range of particle-containing materials.

2011 ◽  
Vol 1295 ◽  
Author(s):  
David G. Morris ◽  
Maria Antonia Muñoz-Morris

ABSTRACTIron aluminides show many interesting properties, but still show relatively poor ductility at room temperature and only moderate creep resistance at temperatures above about 600ºC. Processes of severe plastic deformation have been investigated for a wide range of ductile alloys over the past decade, but have hardly been considered for intermetallics. This presentation discusses two studies aimed at refining microstructure by the use of severe plastic deformation of iron aluminides. The first considers processing Fe3Al by heavy cold rolling, followed by annealing for recovery or recrystallization, with an objective of refining grain size to improve strength at the same time as ductility. The high strength and poor ductility of the work hardened material leads to a danger of cracking during rolling, which is a problem for manufacturing large quantities of healthy material. Suitable rolling and recovery treatments can, nevertheless, lead to strong materials with some plastic ductility. A different technique of multidirectional, high-strain and high-temperature forging applied to a boride-containing Fe3Al alloy produces a material with large grain size and refined dispersion of boride particles. These particles lead to a considerable increase in creep strength under conditions of moderate stresses at temperatures around 700ºC. This high-strain forging technique can be seen as an intermediate processing method between conventional wrought metallurgy and mechanical-alloying powder metallurgy. This technique offers the possibility to improve high temperature behaviour of such intermetallics containing second-phase dispersions, and can be scaled to produce large quantities of high-quality material.


Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 645
Author(s):  
Igor Litovchenko ◽  
Sergey Akkuzin ◽  
Nadezhda Polekhina ◽  
Kseniya Almaeva ◽  
Evgeny Moskvichev

The effect of high-temperature thermomechanical treatment on the structural transformations and mechanical properties of metastable austenitic steel of the AISI 321 type is investigated. The features of the grain and defect microstructure of steel were studied by scanning electron microscopy with electron back-scatter diffraction (SEM EBSD) and transmission electron microscopy (TEM). It is shown that in the initial state after solution treatment the average grain size is 18 μm. A high (≈50%) fraction of twin boundaries (annealing twins) was found. In the course of hot (with heating up to 1100 °C) plastic deformation by rolling to moderate strain (e = 1.6, where e is true strain) the grain structure undergoes fragmentation, which gives rise to grain refining (the average grain size is 8 μm). Partial recovery and recrystallization also occur. The fraction of low-angle misorientation boundaries increases up to ≈46%, and that of twin boundaries decreases to ≈25%, compared to the initial state. The yield strength after this treatment reaches up to 477 MPa with elongation-to-failure of 26%. The combination of plastic deformation with heating up to 1100 °C (e = 0.8) and subsequent deformation with heating up to 600 °C (e = 0.7) reduces the average grain size to 1.4 μm and forms submicrocrystalline fragments. The fraction of low-angle misorientation boundaries is ≈60%, and that of twin boundaries is ≈3%. The structural states formed after this treatment provide an increase in the strength properties of steel (yield strength reaches up to 677 MPa) with ductility values of 12%. The mechanisms of plastic deformation and strengthening of metastable austenitic steel under the above high-temperature thermomechanical treatments are discussed.


2007 ◽  
Vol 558-559 ◽  
pp. 1283-1294 ◽  
Author(s):  
Cheng Xu ◽  
Z. Horita ◽  
Terence G. Langdon

It is now well-established that processing through the application of severe plastic deformation (SPD) leads to a significant reduction in the grain size of a wide range of metallic materials. This paper examines the fabrication of ultrafine-grained materials using high-pressure torsion (HPT) where this process is attractive because it leads to exceptional grain refinement with grain sizes that often lie in the nanometer or submicrometer ranges. Two aspects of HPT are examined. First, processing by HPT is usually confined to samples in the form of very thin disks but recent experiments demonstrate the potential for extending HPT also to bulk samples. Second, since the strains imposed in HPT vary with the distance from the center of the disk, it is important to examine the development of inhomogeneities in disk samples processed by HPT.


Materia Japan ◽  
2003 ◽  
Vol 42 (12) ◽  
pp. 863-863 ◽  
Author(s):  
Keiichiro Ohishi ◽  
Takeshi Fujita ◽  
Kunihiro Ohashi ◽  
Kenji Kaneko ◽  
Zenji Horita

2009 ◽  
Vol 131 (5) ◽  
Author(s):  
Philip J. Maziasz ◽  
John P. Shingledecker ◽  
Neal D. Evans ◽  
Michael J. Pollard

Oak Ridge National Laboratory and Caterpillar (CAT) have recently developed a new cast austenitic stainless steel, CF8C-Plus, for a wide range of high-temperature applications, including diesel exhaust components and turbine casings. The creep-rupture life of the new CF8C-Plus is over ten times greater than that of the standard cast CF8C stainless steel, and the creep-rupture strength is about 50–70% greater. Another variant, CF8C-Plus Cu/W, has been developed with even more creep strength at 750–850°C. The creep strength of these new cast austenitic stainless steels is close to that of wrought Ni-based superalloys such as 617. CF8C-Plus steel was developed in about 1.5 years using an “engineered microstructure” alloy development approach, which produces creep resistance based on the formation of stable nanocarbides (NbC), and resistance to the formation of deleterious intermetallics (sigma, Laves) during aging or service. The first commercial trial heats (227.5 kg or 500 lb) of CF8C-Plus steel were produced in 2002, and to date, over 27,215 kg (300 tons) have been produced, including various commercial component trials, but mainly for the commercial production of the Caterpillar regeneration system (CRS). The CRS application is a burner housing for the on-highway heavy-duty diesel engines that begins the process to burn-off particulates trapped in the ceramic diesel particulate filter (DPF). The CRS/DPF technology was required to meet the new more stringent emissions regulations in January, 2007, and subjects the CRS to frequent and severe thermal cycling. To date, all CF8C-Plus steel CRS units have performed successfully. The status of testing for other commercial applications of CF8C-Plus steel is also summarized.


1985 ◽  
Vol 54 ◽  
Author(s):  
Albertus G. Dirks ◽  
Tien Tien ◽  
Janet M. Towner

ABSTRACTThe microstructure and properties of thin films depends strongly upon the alloy composition. A study was made of the metallurgical aspects of homogeneous Al alloy films, particularly the binary Al-Ti and the ternary Al-Ti-Si systems. Electrical resistivity, grain size morphology, second phase formation and electromigration have been studied as a function of the alloy composition and its heat treatment.


1992 ◽  
Vol 273 ◽  
Author(s):  
A. K. Ghosh ◽  
A. Basu ◽  
H. Kung

ABSTRACTIn an effort to enhance the toughness and creep strength of MoSi2, the role of various metallic and ceramic reinforcements is being examined. In this work, the effects of an oxide, a carbide and a nitride reinforcement on the compression creep behavior of MoSi2 are explored. Variations in the deformability of reinforcements and their relative strength and flaw population appear to influence the creep strength of the composites. Refinements in grain size also improve crack tolerance of the composite during deformation at 1200°C.


Author(s):  
Adewale Olasumboye ◽  
Gbadebo Owolabi ◽  
Olufemi Koya ◽  
Horace Whitworth ◽  
Nadir Yilmaz

Abstract This study investigates the dynamic response of AA2519 aluminum alloy in T6 temper condition during plastic deformation at high strain rates. The aim was to determine how the T6 temper condition affects the flow stress response, strength properties and microstructural morphologies of the alloy when impacted under compression at high strain rates. The specimens (with aspect ratio, L/D = 0.8) of the as-cast alloy used were received in the T8 temper condition and further heat-treated to the T6 temper condition based on the standard ASTM temper designation procedures. Split-Hopkinson pressure bar experiment was used to generate true stress-strain data for the alloy in the range of 1000–3500 /s strain rates while high-speed cameras were used to monitor the test compliance with strain-rate constancy measures. The microstructures of the as received and deformed specimens were assessed and compared for possible disparities in their initial microstructures and post-deformation changes, respectively, using optical microscopy. Results showed no clear evidence of strain-rate dependency in the dynamic yield strength behavior of T6-temper designated alloy while exhibiting a negative trend in its flow stress response. On the contrary, AA2519-T8 showed marginal but positive response in both yield strength and flow behavior for the range of strain rates tested. Post-deformation photomicrographs show clear disparities in the alloys’ initial microstructures in terms of the second-phase particle size differences, population density and, distribution; and in the morphological changes which occurred in the microstructures of the different materials during large plastic deformation. AA2519-T6 showed a higher susceptibility to adiabatic shear localization than AA2519-T8, with deformed and bifurcating transformed band occurring at 3000 /s followed by failure at 3500 /s.


2003 ◽  
Vol 341 (1-2) ◽  
pp. 273-281 ◽  
Author(s):  
Kyung-Tae Park ◽  
Duck-Young Hwang ◽  
Young-Kook Lee ◽  
Young-Kuk Kim ◽  
Dong Hyuk Shin

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