Rapid Synthesis of Monodispersed TATB Microparticles in Ionic Liquid Micelles

MRS Advances ◽  
2018 ◽  
Vol 4 (15) ◽  
pp. 843-849
Author(s):  
Casey Karler ◽  
Leanne Alarid ◽  
David Rosenberg ◽  
Hongyou Fan
Keyword(s):  
Ionic Liquid ◽  
Energetic Materials ◽  
High Explosive ◽  
Research Effort ◽  
Synthesis Method ◽  
Explosive Material ◽  
Rapid Synthesis ◽  
Hydrophilic Lipophilic Balance ◽  
Significant Interest ◽  
Microscopic Morphology

ABSTRACTControlling microscopic morphology of energetic materials is of significant interest for the improvement of their performance and production consistency. As an important insensitive high explosive material, triaminotrinitrobenzene (TATB) has attracted tremendous research effort for military grade explosives and propellants. In this study, a new, rapid and inexpensive synthesis method for monodispersed TATB microparticles based on micelle-confined precipitation was developed. Surfactant with proper hydrophilic-lipophilic balance value was found to be critical to the success of this synthesis. The morphology of the TATB microparticles can be tuned between quasi-spherical and faceted by controlling the speed of recrystallization.

Pure-silica ZSM-22 zeolite rapidly synthesized by novel ionic liquid-directed dry-gel conversion

RSC Advances ◽  
2014 ◽  
Vol 4 (91) ◽  
pp. 49647-49654 ◽  
Author(s):  
Haimeng Wen ◽  
Yu Zhou ◽  
Jingyan Xie ◽  
Zhouyang Long ◽  
Wei Zhang ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Conversion Process ◽  
Rapid Synthesis ◽  
Structure Directing Agent ◽  
Dry Gel Conversion ◽  
Pure Silica

Rapid synthesis of pure-silica ZSM-22 was achieved through dry-gel conversion process by using ionic liquid as the structure directing agent.

Room Temperature Ionic Liquid Promoted Improved and Rapid Synthesis of 2,4,5-Triaryl Imidazoles from Aryl Aldehydes and 1,2-Diketones or α-Hydroxyketone.

ChemInform ◽  
2005 ◽  
Vol 36 (31) ◽  
Author(s):  
Shapi A. Siddiqui ◽  
Umesh C. Narkhede ◽  
Sanjay S. Palimkar ◽  
Thomas Daniel ◽  
Rajgopal J. Lahoti ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Room Temperature ◽  
Room Temperature Ionic Liquid ◽  
Rapid Synthesis ◽  
Aryl Aldehydes

Air blast TNT equivalence factors of high explosive material PETN for bare charges

2019 ◽  
Vol 377 ◽  
pp. 152-162 ◽  
Author(s):  
Weifang Xiao ◽  
Matthias Andrae ◽  
Norbert Gebbeken
Keyword(s):  
High Explosive ◽  
Explosive Material ◽  
Air Blast ◽  
Tnt Equivalence

Ionic-liquid supported rapid synthesis of an N-glycan core pentasaccharide on a 10 g scale

2018 ◽  
Vol 16 (25) ◽  
pp. 4720-4727 ◽  
Author(s):  
Wei Li ◽  
Yu Gao ◽  
Qing Li ◽  
Zhong-Jun Li
Keyword(s):  
Ionic Liquid ◽  
Rapid Synthesis ◽  
Ionic Liquid Support

A hetero-branched N-glycan core pentasaccharide was rapidly assembled on a new ionic liquid support on a 10 g scale.

A series of energetic cyclo-pentazolate salts: rapid synthesis, characterization, and promising performance

2019 ◽  
Vol 7 (20) ◽  
pp. 12468-12479 ◽  
Author(s):  
Yuangang Xu ◽  
Lili Tian ◽  
Dongxue Li ◽  
Pengcheng Wang ◽  
Ming Lu
Keyword(s):  
Rapid Method ◽  
Energetic Materials ◽  
Next Generation ◽  
Rapid Synthesis ◽  
Energetic Salts

A family of cyclo-pentazolate anion-based energetic salts was designed and synthesized by a rapid method, and these salts were evaluated as potential next generation energetic materials.

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