A solid-phase extraction-thin-layer chromatographic-fiber optical scanning densitometric method for determination of flavonol aglycones in extracts of rose leaves

2005 ◽  
Vol 18 (106) ◽  
pp. 437-442 ◽  
Author(s):  
Renata Nowak ◽  
Tomasz Tuzimski
1998 ◽  
Vol 81 (4) ◽  
pp. 844-847 ◽  
Author(s):  
Wynne W Landgraf ◽  
P Frank Ross

Abstract Monensin is extracted from feed with methanol and purified by solvent-partitioning solid-phase extraction. After solvent reduction, monensin is separated by thin-layer chromatography on silica gel and visualized by color development with vanillin. No false-positive results were obtained in validation studies by submitting or peer laboratories when blank samples were analyzed. Three of 20 samples spiked with 5 ppm monensin were reported as containing no monensin. All samples spiked with 10 ppm monensin were reported positive for monensin.


2005 ◽  
Vol 18 (106) ◽  
pp. 423-426 ◽  
Author(s):  
Sandra Babić ◽  
Danijela Ašperger ◽  
Dragana Mutavdžić ◽  
Alka Horvat ◽  
Marija Kaštelan-Macan

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