A Comparison of the Capabilities of Atomic Absorption and Inductively Coupled Plasma Spectroscopy for the Analysis of Metallurgical Samples

2009 ◽  
pp. 55-55-9
Author(s):  
GF Wallace
Keyword(s):  
Atomic Absorption ◽  
Inductively Coupled Plasma ◽  
Plasma Spectroscopy ◽  
Inductively Coupled

scholarly journals Heavy Metal Contamination

2021 ◽  
Author(s):  
Soni Kumari ◽  
Amarnath Mishra
Keyword(s):  
Heavy Metal ◽  
Sewage Sludge ◽  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Metal Contamination ◽  
Industrial Waste ◽  
Inductively Coupled Plasma ◽  
Heavy Metal Contamination ◽  
Inductively Coupled

In the era of industrialization, pollution has totally deteriorated the quality and diversity of life. Heavy metal contaminations are the major causes of environment deteriorations. The basic reasons are natural as well as anthropogenic. Chief sources of heavy metal contamination are air pollution, river sediments, sewage sludge, town waste composts, agricultural chemicals like fertilizers and pesticides, and industrial waste like factories releasing chemicals, anthropogenic activities, etc. Agricultural soils in many parts of the world are generally contaminated by heavy metal toxicity such as Cd, Cu, Zn, Ni, Co, Pb, Hg, As, etc. These are due to the long-term use of phosphate fertilizers, sewage sludge, dust from smelters, industrial waste, etc. Heavy metals in soils are detected with some specific instruments like atomic absorption spectroscopy, inductively coupled plasma, inductively coupled plasma-mass spectroscopy, and X-ray fluorescence and spectroscopy. Among all these instruments, atomic absorption spectroscopy (AAS) is the best because it gives the precise quantitative determination. AAS is a method applied for measuring the quantity of the trace elements present in the soil or any other samples.

scholarly journals Arsenic quantification techniques and ISO/IEC 17025 accreditation in Brazil

2019 ◽  
Vol 6 (14) ◽  
pp. 803-817
Author(s):  
Jefferson Luiz Antunes Santos ◽  
Jader Galba Busato ◽  
Rodrigo de Almeida Heringer ◽  
Juscimar da Silva ◽  
Leonardo Barros Dobbss
Keyword(s):  
Atomic Absorption Spectrometry ◽  
Atomic Absorption ◽  
Inductively Coupled Plasma ◽  
Hydride Generation ◽  
Absorption Spectrometry ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Analytical Technique ◽  
Inductively Coupled ◽  
Icp Ms

The importance of arsenic (As) quantification in environmental compartments is due to its risks to ecosystems and public health. There are reports of high concentrations of this metalloid in Brazil and technological differences between states are observed. The objective of this work was to present and discuss current scenarios of accreditation and compare the limit of quantification (LOQ) of As by analytical technique in Brazil. Data from accredited laboratories were collected on Inmetro website and in state metrological networks and then grouped and analyzed by state, matrix and analytical technique. There are large discrepancies between the number of laboratories per state and a good correlation with gross domestic product (GDP). Almost all laboratories have a LOQ less than the environmental limits. The observed list of techniques sorted from lowest to highest LOQ values is: for liquid samples ICP MS (inductively coupled plasma mass spectrometry), ET AAS (electrothermal atomic absorption spectrometry), HG AAS (hydride generation combined with atomic absorption spectrometry) or HG ICP OES (hydride generation combined with inductively coupled plasma optical emission spectrometry) and UV VIS (visible ultraviolet spectroscopy); for solids samples HG ICP OES, ICP MS, HG AAS, ET AAS and FAAS (flame atomic absorption spectrometry); and for bioindicators ICP MS, HG ICP OES. Analysis of As species is accredited in only one laboratory, but does not include all species.

Quantitative analysis of palladacycle-tagged PLGA nanoparticle biodistribution in rat organs by means of atomic absorption spectrometry and inductively coupled plasma mass spectrometry

2021 ◽  
Author(s):  
Yulia Ermolenko ◽  
Olga N. Gorunova ◽  
Valery V. Dunina ◽  
Dmitriy B. Petrenko ◽  
Nadejda G. Novikova ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Atomic Absorption Spectrometry ◽  
Atomic Absorption ◽  
Inductively Coupled Plasma ◽  
Graphite Furnace ◽  
Absorption Spectrometry ◽  
Plga Nanoparticles ◽  
Inductively Coupled ◽  
Plasma Mass Spectrometry ◽  
Plga Nanoparticle

The biodistribution of PLGA nanoparticles labelled with Pd in the form of a dimeric cyclopalladated derivative of N,N-dimethyldiphenylmethylamine was investigated in rats using graphite furnace atomic absorption spectrometry and inductively coupled plasma mass spectrometry.

Nanocomposite Detection of Elemental Impurities and Process Correlation Analysis of Ceftriaxone Sodium for Injection

2020 ◽  
Vol 12 (12) ◽  
pp. 1458-1463
Author(s):  
Li Zhu ◽  
Xiaomeng Chong ◽  
Yu Zhao ◽  
Mingzhe Xu ◽  
Lihui Yin
Keyword(s):  
Activated Carbon ◽  
Generic Drug ◽  
Inductively Coupled Plasma ◽  
Plasma Spectroscopy ◽  
Inductively Coupled ◽  
Elemental Impurities ◽  
Ceftriaxone Sodium ◽  
The Stability ◽  
Impurity Elements ◽  
First Time

An inductively coupled plasma spectroscopy method was established to detect 29 elemental impurities in ceftriaxone sodium for injection by nanocomposite, and also used to detect the elemental impurities in the generic, domestic original and foreign original ceftriaxone sodium for injection. This paper for the first time analysed the possible sources of elemental impurities and their potential impacts on the drug quality based on the process. The results showed that zinc and potassium were detected in both the generic drug and the domestic original ceftriaxone sodium for injection, and zinc was not detected but potassium was detected in the foreign original drug; the content of zinc in the generic drug was significantly higher than that in the domestic original drug, and the content of potassium in generic drug and domestic original drug was higher than that in the foreign original drug, according to the process, the elemental impurities may come from the activated carbon or nanocarriers used in the process, and further stability analysis of the samples showed that the stability of the generic drug was slightly lower than that of the original drug, so it was speculated that impurity elements might also be one of the reasons for its instability.

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