Compositional Analysis of Drugs and Injectable Biological Products by Thermogravimetry

2009 ◽  
pp. 48-48-8 ◽  
Author(s):  
JC May ◽  
RM Wheeler ◽  
A Del Grosso
Author(s):  
A. Olsen ◽  
J.C.H. Spence ◽  
P. Petroff

Since the point resolution of the JEOL 200CX electron microscope is up = 2.6Å it is not possible to obtain a true structure image of any of the III-V or elemental semiconductors with this machine. Since the information resolution limit set by electronic instability (1) u0 = (2/πλΔ)½ = 1.4Å for Δ = 50Å, it is however possible to obtain, by choice of focus and thickness, clear lattice images both resembling (see figure 2(b)), and not resembling, the true crystal structure (see (2) for an example of a Fourier image which is structurally incorrect). The crucial difficulty in using the information between Up and u0 is the fractional accuracy with which Af and Cs must be determined, and these accuracies Δff/4Δf = (2λu2Δf)-1 and ΔCS/CS = (λ3u4Cs)-1 (for a π/4 phase change, Δff the Fourier image period) are strongly dependent on spatial frequency u. Note that ΔCs(up)/Cs ≈ 10%, independent of CS and λ. Note also that the number n of identical high contrast spurious Fourier images within the depth of field Δz = (αu)-1 (α beam divergence) decreases with increasing high voltage, since n = 2Δz/Δff = θ/α = λu/α (θ the scattering angle). Thus image matching becomes easier in semiconductors at higher voltage because there are fewer high contrast identical images in any focal series.


Author(s):  
John B. Vander Sande ◽  
Thomas F. Kelly ◽  
Douglas Imeson

In the scanning transmission electron microscope (STEM) a fine probe of electrons is scanned across the thin specimen, or the probe is stationarily placed on a volume of interest, and various products of the electron-specimen interaction are then collected and used for image formation or microanalysis. The microanalysis modes usually employed in STEM include, but are not restricted to, energy dispersive X-ray analysis, electron energy loss spectroscopy, and microdiffraction.


2015 ◽  
Vol 7 (1) ◽  
pp. 271-276
Author(s):  
MA Zubair ◽  
MA Haque ◽  
MM Sultana ◽  
S Akter

16th February 2015. Due to a number of missing tables and figures, this article (DOI: http://dx.doi.org/10.3329/jesnr.v7i1.22182) was withdrawn from Vol.7(1) and has been republished with corrections in Vol.7(2) pp.185-190 (DOI: http://dx.doi.org/10.3329/jesnr.v7i2.22230). The Editor  


2020 ◽  
Author(s):  
KJ Nunan ◽  
Ian Sims ◽  
A Bacic ◽  
SP Robinson ◽  
GB Fincher

Cell walls have been isolated from the mesocarp of mature grape (Vitis vinifera L.) berries. Tissue homogenates were suspended in 80% (v/v) ethanol to minimise the loss of water-soluble wall components and wet-sieved on nylon mesh to remove cytoplasmic material. The cell wall fragments retained on the sieve were subsequently treated with buffered phenol at pH 7.0, to inactivate any wall-bound enzymes and to dislodge small amounts of cytoplasmic proteins that adhered to the walls. Finally, the wall preparation was washed with chloroform/methanol (1:1, v/v) to remove lipids and dried by solvent exchange. Scanning electron microscopy showed that the wall preparation was essentially free of vascular tissue and adventitious protein of cytoplasmic origin. Compositional analysis showed that the walls consisted of approximately 90% by weight of polysaccharide and less than 10% protein. The protein component of the walls was shown to be rich in arginine and hydroxyproline residues. Cellulose and polygalacturonans were the major constituents, and each accounted for 30-40% by weight of the polysaccharide component of the walls. Substantial varietal differences were observed in the relative abundance of these two polysaccharides. Xyloglucans constituted approximately 10% of the polysaccharide fraction and the remainder was made up of smaller amounts of mannans, heteroxylans, arabinans and galactans.


2019 ◽  
Vol 6 (1) ◽  
pp. 40-46
Author(s):  
Tadjidin Uraimov Tadjidin Uraimov ◽  
◽  
Matluba Yakhyokulova

Author(s):  
O.I. Vlasova ◽  
◽  
E.A. Danilets ◽  
V.M. Perederieva ◽  
I.A. Volters

the article provides data on the effectiveness of the use of biological products in the fight against septoria infection of winter wheat, placed on various predecessors and the formation of yield.


Spring wheat is the main grain crop. Stable production of high-quality wheat grain is the key to the country's food independence. Therefore, the study of the elements of growing spring wheat technology, aimed at increasing the productivity of crops, is important. The study of the interaction of plants and microorganisms depending on the level of mineral nutrition in crop planning is currently ofparticular relevance. The use of biological products, growth regulators improves the mineral nutrition of plants, increases productivity and its quality, and also provides savings in mineral fertilizers. In the upper Volga region, the main spring crops are wheat, barley and oats. To further increase them in the region, it is necessary to study the characteristics of the formation of yields and determine the most productive crops depending on the level of nutrition, biological products and growth regulators. The scientific article presents the results of the study of these drugs on the productivity of spring wheat. In field experiments, it was planned to get 30, 40 and 50 tons of grain per hectare. Fertilizers for the planned harvest were made taking into account the agrochemical properties of the soil. From biological products used Flavobacterin, which has a protective effect against diseases and improves product quality, from growth regulators used agrochemicals HUMATE + 7 (10 % liquid concentrate), which is characterized by high biological activity. The yield level was determined taking into account the average long-term moisture supply and qualitative assessment of arable land. The indicators of photosynthetic activity of crops, crop and its structure, quality characteristics of grain and economic efficiency of growing spring wheat in the upper Volga region are presented. As a result of researches the optimum level of mineral nutrition for wheat, the efficacy of agrochemical diazotroph and programming yields of spring wheat, determined the photosynthetic activity of crops and grain yield, calculated economic efficiency of the studied techniques and established the qualitative characteristics of the crop. The program for obtaining the planned wheat yields in the years of the experiments was completed by 68-91 %. Close to the planned the program was implemented using a biological product and growth regulator-74-91 %.


2018 ◽  
Vol 62 (1) ◽  
pp. 31-37
Author(s):  
Noritaka Hashii ◽  
Akiko Ishii-Watabe

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