Effect of High Temperature on the Change in Color, Dimensional Stability and Mechanical Properties of Spruce Wood

Holzforschung ◽  
2003 ◽  
Vol 57 (5) ◽  
pp. 539-546 ◽  
Author(s):  
P. Bekhta ◽  
P. Niemz

Summary In this study the effect of high temperature on mechanical properties, dimensional stability and color of spruce was investigated. Wood specimens conditioned at different relative humidities (50, 65, 80 and 95%) were subjected to heat treatment at 200°C for 2, 4, 8, 10 and 24 h and at 100, 150 and 200°C for 24 h. Color changes were measured in the Minolta Croma-Meter CR-300 color system. Bending strength and modulus of elasticity were determined according to DIN 52186. The results show that heat treatment mainly resulted in a darkening of wood tissues, improvement of the dimensional stability of wood and reduction of its mechanical properties. The darkening accelerated generally when treatment temperature exceeded approximately 200°C. Most of the darkening occurred within the first 4 h of exposure. For the specimens heated to high temperatures, the average decrease in bending strength was about 44–50%, while modulus of elasticity was reduced by only 4–9%. We found that treatment time and temperature were more important than relative humidity regarding the color responses. Strong correlations between total color difference and both modulus of elasticity and bending strength were found. Thus, the color parameters can be estimated quantitatively and used as a prediction of wood strength.

Forests ◽  
2020 ◽  
Vol 11 (9) ◽  
pp. 920 ◽  
Author(s):  
Lin Yang ◽  
Hong-Hai Liu

Wood is an environmentally friendly material, but some natural properties limit its wide application. To study the effect of a combination of heat treatment (HT) and wax impregnation (WI) on wood hygroscopicity, dimensional stability, and mechanical properties, samples of Pterocarpus macrocarpus Kurz wood were subjected to HT at a moderate temperature of 120 °C and a high temperature of 180 °C, for a 4 h duration. Subsequently, half of the 120 °C HT samples were treated with WI at 90 °C. The results showed that 180 °C HT and WI decreased the capacity of adsorption and liquid water uptake and swelled the wood significantly, while WI had the biggest reduction. The effect of 120 °C HT was significant only on decreasing the capacity of adsorption and the swelling of liquid water uptake. The bending strength (MOR) of wood decreased only after 180 °C HT, and 120 °C/4h HT and WI had no significant influence on MOR. The bending stiffness (MOE) increased significantly after 180 °C HT and WI, while 120 °C/4h HT had no significant influence on MOE. Therefore, the combination of moderate-temperature HT can act synergistically in the improvement of certain aspects of wood properties such as capacity of water adsorption and liquid water uptake. WI effectively improved wood hygroscopicity, dimensional stability, and mechanical properties.


Forests ◽  
2019 ◽  
Vol 10 (2) ◽  
pp. 189 ◽  
Author(s):  
Vlastimil Borůvka ◽  
Roman Dudík ◽  
Aleš Zeidler ◽  
Tomáš Holeček

This work deals with the quality of birch (Betula pendula) wood from different sites and the impact of heat treatment on it. Two degrees of heat treatment were used, 170 °C and 190 °C. The resulting property values were compared with reference to untreated wood samples. These values were wood density, compressive strength, modulus of elasticity (MOE), bending strength (MOR), impact bending strength (toughness), hardness, swelling, limit of hygroscopicity, moisture content and color change. It was supposed that an increase in heat-treatment temperature could reduce strength properties and, adversely, lead to better shape and dimensional stability, which was confirmed by experiments. It was also shown that the properties of the wood before treatment affected their condition after heat treatment, and that the characteristic values and variability of birch properties from 4 sites, 8 stems totally, were reflected in the properties of the heat-treated wood. Values of static MOR were the exception, where the quality of the input wood was less significant at a higher temperature, and this was even more significant in impact bending strength, where it manifested at a lower temperature degree. Impact bending strength also proved to be significantly negatively affected by heat treatment, about 48% at 170 °C, and up to 67% at 190 °C. On the contrary, the most positive results were the MOE and hardness increases at 170 °C by about 30% and about 21%, respectively, with a decrease in swelling at 190 °C by about 31%. On the basis of color change and other ascertained properties, there is a possibility that, after suitable heat treatment, birch could replace other woods (e.g., beech) for certain specific purposes, particularly in the furniture industry.


2011 ◽  
Vol 306-307 ◽  
pp. 823-826
Author(s):  
Ming Wen ◽  
Yun Long Yue ◽  
Hai Tao Zhang ◽  
Yang Li

Parameters of processing (heat treatment temperature, holding time) and properties (Bending strength and Microhardness) of Ti2AlC/TiAl compound materials were obtained through mechanical properties examination, the network model was built by BP artificial neural network. The results show that the built model can reflect the relationships between processing and properties very well and has certain accuracy. It can be used for the prediction of the properties of Ti2AlC/TiAl compound materials after heating processing under different experiment conditions. Meanwhile, the model can also serve as a guide for the preparation technology of Ti2AlC/TiAl compound materials.


BioResources ◽  
2017 ◽  
Vol 12 (4) ◽  
pp. 9212-9226
Author(s):  
Qilan Fu ◽  
Alain Cloutier ◽  
Aziz Laghdir

Effects of heat and steam were investigated relative to the mechanical properties and dimensional stability of thermo-hygromechanically-densified sugar maple wood (Acer saccharum Marsh.). The densification process was performed at four temperatures (180 °C, 190 °C, 200 °C, and 210 °C) with and without steam. The hardness, bending strength, bending stiffness, and compression set recovery of the control and densified samples were determined. The effects of heat and steam on the density profile of the samples across thickness were also investigated. The results suggested that the effects of steam on the mechanical properties and dimensional stability of sugar maple wood were more important than that of heat’s influence. Compared to the samples densified without steam, the samples densified with steam showed higher values for hardness, bending strength, bending stiffness, compression set, and density, but much lower compression set recovery when treatment temperature was below 200 °C. High temperature combined with steam contributed to decreased compression set recovery. The lowest compression set recovery was obtained after the first swelling/drying cycle for all of the treatments. A higher weight loss occurred at 210 °C, which resulted in a noticeable decrease of wood density.


2016 ◽  
Vol 850 ◽  
pp. 802-808 ◽  
Author(s):  
Kang Du ◽  
Xiao Kang Liang ◽  
Da Quan Li ◽  
Qiang Zhu

In semi-solid rheocast and thixocast industry, T6 heat treatment was one key factor to improve the mechanical properties of the castings. The microstructure evolution was closely influenced by heat treatment temperature and time. In this paper, the morphology change of eutectic silicon in semi-solid alloy during different heat treatment time was firstly observed. The changes of both roundness and aspect show that the silicon particles underwent fragmentation, coarsening and growing up processes during solution treatment. Then, the mechanical properties after stand T6 and T6 with higher temperature were compared. It may be concluded that the higher temperature doesn’t have obvious effect to increase the mechanical strength, but severe negative effect on the elongation. Finally, the incipient melting defect appeared in higher temperature T6 was proved and its relationship with elongation was analysed.


2011 ◽  
Vol 197-198 ◽  
pp. 90-95 ◽  
Author(s):  
Xian Jun Li ◽  
Zhi Yong Cai ◽  
Qun Ying Mou ◽  
Yi Qiang Wu ◽  
Yuan Liu

In this study the effect of heat treatment on some physical properties of Douglas fir (Pseudotsuga menziesii) was investigated. Wood specimens were subjected to heat treatment at 160, 180, 200 and 220°C for 1, 2, 3 and 4h. The results show that heat treatment resulted in a darkened color, decreased moisture performance and increased dimensional stability of wood. Compared with untreated wood, equilibrium moisture content (EMC), water absorption (WA) and volume swelling (VS) for treated wood decrease up to 42.63%, 34.93% and 67.47%. The higher the treatment temperature and the longer the treatment time, the lower EMC, WA and VS. The VS of treated specimens has a more significant reduction than EMC and WA when the heat treatment temperature is above 180°C. The visual color changes were more distinct after heat treatment above 180°C. Temperature has a greater influence than time on these properties of specimens.


BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 4693-4703
Author(s):  
Alperen Kaymakci ◽  
Bahadır Çağrı Bayram

Effects of the heat treatment parameters were evaluated relative to some physical and mechanical properties of poplar wood (Populus alba L.) with use of two of the prominent multi criteria decision-making (MCDM) techniques: Entropy and The Technique for Order Preference by Similarity to Ideal Solution (TOPSIS). To meet this objective, the test samples were heat-treated at 120, 150, 180, and 210 °C for 2 and 4 h in a laboratory-scale oven. With increasing temperature and duration, the shrinkage and swelling ratios of heat-treated samples were improved. However, the bending strength, modulus of elasticity, and compression strength generally decreased with increasing process temperature and duration. According to (MCDM) analyses, thermal modification definitely improved the physical properties of wood up to a point. Bending strength was found to be the most important determinant of heat treatment success. The other determinants were identified as swelling, compression strength, shrinkage, and modulus of elasticity, respectively. Also, the best results were obtained at 120 °C for 2 h. In general, heat treatment above 150 °C or 4 h is not recommended.


Polymers ◽  
2022 ◽  
Vol 14 (2) ◽  
pp. 222
Author(s):  
Zhenbo Lan ◽  
Jiangang Deng ◽  
You Song ◽  
Zhuolin Xu ◽  
Yu Nie ◽  
...  

Thermal aging of polymer matrix composites exert significant influence on their properties and applications. This paper studied the color changes and mechanical properties of glass fiber reinforced polycarbonate (GF-PC) composites after aging at different temperatures, and the correlation between the trend of color changes and mechanical properties after aging was discussed. The GF-PC composites were aged at 85 °C, 100 °C, 115 °C, 130 °C and 145 °C, respectively. Thereafter, CIELAB colors were used to characterize the color changes of the composites after aging. Tensile and three-point bending tests were carried out to determine the mechanical properties of the composites. According to the values of CIELAB color, the color changes and the color difference (ΔE) of the GF-PC composites after aging were calculated, which showed that color of the GF-PC composite aged at 100 °C changed the most. The color changes of the composites after aging mainly comes from the change of brightness (L value), which was 25.067 for the Raw GF-PC composite. When the aging temperature increased from 85 °C to 100 °C, the brightness of the composites also increased, but decreased when the aging temperature is above 100 °C and continues to rise. Coincidentally, the trend of the mechanical properties of GF-PC composites is closely associated with color changes in the aging temperature range of 85 °C to 145 °C. The tensile and flexural strength of the composites reached the maximum value 72 MPa and 131 MPa, respectively, after aged at 100 °C. It can be speculated that the brightness of the GF-PC composites correlates with trends observed in its tensile strength and bending strength.


2010 ◽  
Vol 150-151 ◽  
pp. 1689-1692 ◽  
Author(s):  
Hai Tao Tao ◽  
Xi Jun Liu ◽  
Tie Ning Ma

In this paper, a series of polyurethane elastomers (PUE) were prepared employing casting method using toluene diisocyanate (TDI), hydroxy-terminated butadiene-acrylonitrile copolymer(HTBN) and polytetrahydrofuran glycol (PTMG) as the main raw materials, and using 2,4- and 2,6- dimethylthioaromatic diamine (DMTDA) as a chain extender. The effects of the content of NCO in PUE (NCO%), mass ratio of HTBN/PTMG, molecular weight of PTMG, dosage of chain extender and heat treatment on the mechanical properties of PUE were studied. The results showed that the lower molecular weight of PTMG and the higher heat treatment temperature were both favorable for increasing the mechanical properties of PUE. When the mass ratio of HTBN/PTMG was 35:65, NCO% was 6.0%, molar ratio of NCO/NH2 was 1.20 and heat treatment time was 2h at 115 , the mechanical properties of PUE were best.


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