scholarly journals Properties of Sinters Produced from Commercially Available Powder Mixtures

2016 ◽  
Vol 16 (4) ◽  
pp. 37-40 ◽  
Author(s):  
J. Borowiecka-Jamrozek ◽  
J. Lachowski
Keyword(s):  
Static Loading ◽  
Metal Matrix ◽  
Laboratory Testing ◽  
General Purpose ◽  
Powder Mixtures ◽  
Micron Size ◽  
Experimental Laboratory ◽  
Strength And Ductility ◽  
Graphite Mould ◽  
Scanning Electron

Abstract This paper discusses the mechanical properties of a material fabricated from commercially available metal powder mixtures designed for use as a metal matrix of diamond impregnated composites. The mixtures with the catalogue numbers CSA and CSA800 provided by a Chinese producer are suitable for experimental laboratory testing. The specimens were fabricated in a graphite mould using hot pressing. The material was tested for density, porosity, hardness, and tensile strength under static loading. A scanning electron microscope (SEM) was used to analyze the microstructure and cleavage fracture of broken specimens. It was essential to determine how the chemical composition and the fabrication process affected the microstructure and properties of the material. The properties of the sinters were compared with those of hot pressed specimens fabricated from sub-micron size cobalt powder (Cobalt SMS). Although the as-consolidated material is inferior to cobalt, it displays a favourable combination of hardness, yield strength and ductility, and seems to have a great potential for moderate and general purpose applications.

scholarly journals Sintered FeCuRe Alloys Produced from Commercially Available Powders

2017 ◽  
Vol 62 (3) ◽  
pp. 1713-1720
Author(s):  
J. Borowiecka-Jamrozek
Keyword(s):  
Experimental Data ◽  
Mechanical Properties ◽  
Metal Matrix ◽  
General Purpose ◽  
Cobalt Powder ◽  
Static Tensile ◽  
Properties Of Materials ◽  
Sintered Materials ◽  
Graphite Mould ◽  
Scanning Electron

Abstract This paper discusses the mechanical properties of materials fabricated from commercially available powders designed for use as a metal matrix of diamond-impregnated composites. The powders with the catalogue numbers CSA and CSA800 produced in China were tested under laboratory conditions. The specimens were fabricated in a graphite mould using hot pressing. The materials were analysed for density, porosity, hardness and static tensile strength. A scanning electron microscope (SEM) was employed to observe the microstructure and fracture surfaces of the specimens. The experimental data was used to determine how the chemical composition of the powders and the process parameters affected the microstructure and properties of the materials. The properties of the sintered materials produced from the Chinese powders were compared with the properties reported for specimens fabricated from cobalt powder (Co SMS). Even though the hot pressed CSA and CSA800 powders had inferior mechanical properties to their cobalt analogue, they seem well-suited for general-purpose diamond-impregnated tools with less demanding applications.

The Strength of High-Temperature Ag–In Joints Produced Between Copper by Fluxless Low-Temperature Processes

2014 ◽  
Vol 136 (1) ◽  
Author(s):  
Yuan-Yun Wu ◽  
Chin C. Lee
Keyword(s):  
Solid Solution ◽  
Electron Microscope ◽  
Shear Test ◽  
Test Results ◽  
X Ray ◽  
Ductile Mode ◽  
Micron Size ◽  
Cu Substrates ◽  
Strength And Ductility ◽  
Scanning Electron

Two copper (Cu) substrates were bonded using silver (Ag) and indium (In) and annealed at 200–250 °C to convert the joints into the solid solution (Ag) for enhanced strength and ductility. Cu–Cu pair was chosen so that the samples break in the joint during shear test. The upper Cu was electroplated with 15 μm Ag. The lower Cu was plated with 15 μm Ag, followed by In and 0.1 μm Ag to inhibit indium oxidation. Two designs were implemented, using 8 μm and 5 μm In, respectively. The Cu substrates were bonded at 180 °C in 100 mTorr vacuum without flux. Afterwards, samples were annealed at 200 °C for 1000 h (first design) and at 250 °C for 350 h (second design), respectively. Scanning electron microscope with energy dispersive X-ray analysis (SEM and EDX) results indicate that the joint of the first design is an alloy of mostly (Ag) with micron-size Ag2In and (ζ) regions, and that of second design has converted to a single (Ag) phase. Shear test results show that the samples are very strong. The breaking forces far exceed requirements in MIL-STD-883 H standards. Fracture incurs inside the joint and is a mix of brittle and ductile modes or only ductile mode. The joint solidus temperatures are 600 °C and 900 °C for the first and second designs, respectively.

Effect of Small Iron, Chromium and Boron Additions as Alloying Elements on Microstructure and Mechanical Properties of Ni3Al

2007 ◽  
Vol 23 ◽  
pp. 123-126
Author(s):  
Radu L. Orban ◽  
Mariana Lucaci
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Room Temperature ◽  
Alloying Elements ◽  
Alloyed Powder ◽  
Mechanically Alloyed ◽  
Powder Mixtures ◽  
B Additions ◽  
Strength And Ductility ◽  
Iron Chromium

This paper investigates the effect of Fe, Cr and B additions, in small proportions, as alloying elements in Ni3Al with the purpose to reduce its intrinsic fragility and extrinsic embrittlement and to enhance, in the same time, its mechanical properties. It represents a development of some previous research works of the authors, proving that Ni3Al-Fe-Cr-B alloys obtained by reactive synthesis (SHS) starting from Mechanically Alloyed powder mixtures have superior both room temperature tensile strength and ductility, and compression ones at temperatures up to 800 °C, than pure Ni3Al. These create premises for their using as superalloys substitutes.

scholarly journals Achieving high strength and ductility in ODS-W alloy by employing oxide@W core-shell nanopowder as precursor

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Zhi Dong ◽  
Zongqing Ma ◽  
Liming Yu ◽  
Yongchang Liu
Keyword(s):  
High Temperature ◽  
Metal Matrix ◽  
High Performance ◽  
High Energy ◽  
Core Shell ◽  
Microstructural Stability ◽  
Oxide Particles ◽  
Ods Alloy ◽  
Prepared Alloy ◽  
Strength And Ductility

AbstractWith excellent creep resistance, good high-temperature microstructural stability and good irradiation resistance, oxide dispersion strengthened (ODS) alloys are a class of important alloys that are promising for high-temperature applications. However, plagued by a nerve-wracking fact that the oxide particles tend to aggregate at grain boundary of metal matrix, their improvement effect on the mechanical properties of metal matrix tends to be limited. In this work, we employ a unique in-house synthesized oxide@W core-shell nanopowder as precursor to prepare W-based ODS alloy. After low-temperature sintering and high-energy-rate forging, high-density oxide nanoparticles are dispersed homogeneously within W grains in the prepared alloy, accompanying with the intergranular oxide particles completely disappearing. As a result, our prepared alloy achieves a great enhancement of strength and ductility at room temperature. Our strategy using core-shell powder as precursor to prepare high-performance ODS alloy has potential to be applied to other dispersion-strengthened alloy systems.

Alumina Reinforced EP648 Metal Matrix Composite Produced by Selective Laser Melting Powder Bed Fusion Additive Technology

2021 ◽  
Vol 316 ◽  
pp. 181-186
Author(s):  
P.A. Lykov ◽  
L. V. Radionova
Keyword(s):  
Selective Laser Melting ◽  
Matrix Composite ◽  
Metal Matrix ◽  
Composite Powder ◽  
Additive Technology ◽  
Ceramic Powders ◽  
Laser Melting ◽  
Two Phase ◽  
Powder Bed ◽  
Scanning Electron

This paper is devoted to fabrication of alumina reinforced EP648 matrix composite material, using selective laser melting. of two-phase composite powder, prepared by ball milling of metal and ceramic powders. Five 10x10x5 mm bulk specimens were successfully manufactured using different process parameters. The obtained MMC specimens were characterized by scanning electron microscopy.

scholarly journals Chemical Stability of Ti3C2 MXene with Al in the Temperature Range 500–700 °C

Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1979 ◽  
Author(s):  
Jing Zhang ◽  
Shibo Li ◽  
Shujun Hu ◽  
Yang Zhou
Keyword(s):  
Electron Microscopy ◽  
Chemical Stability ◽  
Metal Matrix ◽  
Matrix Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Temperature Range ◽  
Transmission Electron ◽  
Work First ◽  
Scanning Electron

Ti3C2Tx MXene, a new 2D nanosheet material, is expected to be an attractive reinforcement of metal matrix composites because its surfaces are terminated with Ti and/or functional groups of –OH, –O, and –F which improve its wettability with metals. Thus, new Ti3C2Tx/Al composites with strong interfaces and novel properties are desired. To prepare such composites, the chemical stability of Ti3C2Tx with Al at high temperatures should be investigated. This work first reports on the chemical stability of Ti3C2Tx MXene with Al in the temperature range 500–700 °C. Ti3C2Tx is thermally stable with Al at temperatures below 700 °C, but it reacts with Al to form Al3Ti and TiC at temperatures above 700 °C. The chemical stability and microstructure of the Ti3C2Tx/Al samples were investigated by differential scanning calorimeter, X-ray diffraction analysis, scanning electron microscopy, and transmission electron microscopy.

Obtention of an Al-Based Composite Material by Direct Fusion of Used Beverage Cans

2012 ◽  
Vol 706-709 ◽  
pp. 271-276 ◽  
Author(s):  
Claudia Carrasco ◽  
C. Montalba ◽  
Carlos Camurri
Keyword(s):  
Composite Material ◽  
Aluminium Alloys ◽  
Metal Matrix ◽  
Mechanical Analysis ◽  
Heat Treated ◽  
Structural Applications ◽  
Metal Matrix Composite Material ◽  
Direct Fusion ◽  
Scanning Electron

In the present study, the fabrication of an Al-based metal matrix composite material obtained directly from the melting of the aluminium used beverage cans in a modified rheocasting process is presented. The analysed operational condition is the shear rate applied to the bath and its influence on the properties of the obtained samples. Additionally, samples were heat treated at two different times. The characterization of the phases obtained in Al-based MMC was made by means of metallography, scanning electron microscopy with energy dispersive spectroscopy and electron microprobe with wavelength dispersion spectroscopy. The results show that some constituents were formed during the fabrication process of the MMC, mainly Al6(Fe, Mn), which are partially transformed during the heat treatment. Additionally, samples were evaluated using dynamic mechanical analysis, and the results suggest that the obtained MMC could have very good mechanical properties, similar or superior to the aluminium alloys commonly used for structural applications such as 6XXX family.

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