scholarly journals Effect of Various Veneering Techniques on Bond Strength and Colour Stability of Zirconia / Veneering Ceramic after Hydrothermal Aging

2021 ◽  
Vol 10 (39) ◽  
pp. 3474-3479
Author(s):  
Rafat Sasany ◽  
Duygu Sarac ◽  
Goknil Ergun Kunt
Keyword(s):  
Bond Strength ◽  
In Vitro Study ◽  
Resin Cement ◽  
Colour Stability ◽  
Hydrothermal Aging ◽  
Significant Difference ◽  
Before And After ◽  
Cad Cam ◽  
Ceramic Restorations

BACKGROUND The purpose of this in-vitro study was to compare the colour stability and bond strength of zirconia-based ceramic restorations after hydrothermal aging using conventional layering, heat-pressing, and multilayer veneering techniques. METHODS One hundred twenty specimens’ core (15 x 10 x 0.7) was fabricated from A2-shade zirconia CAD-CAM blocks (IPS e.max ZirCAD). Specimens were divided into 4 groups for veneering (N = 30): [(layering group (L), IPS e.max ceram), (heat – pressing group (P), IPS press), and multilayer group, IPS e max Cad for 2 different types of cement (cemented with RelyX U200 (M1) and PANAVIA SA (M2))]. Aging was performed for (5 - 55°C, 5000). Colour coordinates before and after aging were measured to calculate colour differences (ΔE00). The shear bond strength test was performed with a universal test unit. The data were analysed using the analysis of variance (ANOVA) and Tukey’s Honest Significant Difference test (alpha = 0.05). RESULTS Significant differences were found between the groups in bond strength (P < 0.001). Group M1 had the highest bond strength while Group L had the lowest bond strength. In terms of ΔE00 values, there were significant variations between the groups (P < 0.001). Group M1 had the highest colour stability, while Group M2 had the lowest colour stability. CONCLUSIONS The method of fabrication had an impact on the power of the bond between veneering ceramic and zirconia, as well as its colour stability. The restoration fabricated by a multilayer technique was cemented by resin cement (Rely X U200 Automix) which was found to be more resistant and colour stable. KEY WORDS Veneers, Heat-Press Technique, Bond Strength, Colour Different, Hydrothermal Aging.

scholarly journals Micro-shear bond strength of bioactive cement to translucent zirconia after thermocycyling: a comparative in-vitro study

2020 ◽  
Vol 23 (1) ◽  
Author(s):  
Menna Ahmed ElGendy ◽  
Ihab Mosleh ◽  
Hanaa Zaghloul
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Control Group ◽  
Significant Difference ◽  
Before And After

Objective: the purpose of the study was to evaluate the micro-shear bond strength of different cements to translucent zirconia before and after thermocycling aging. Material and methods: Twelve translucent zirconia ceramic discs were used in the study. Specimens were sandblasted using 50 ‎μm aluminum oxide (Al2O3) particles. The specimens were divided into three groups (n = 4) according to the cement type: Panavia resin cement (control group), resin modified glass ionomer (RMGI), and Activa bioactive cement. Each group was further sub-divided into two equal subgroups (n = 2) according to whether the specimens were subjected to thermocycling or not. Thermocycling was performed in distilled water at 5000 cycles between 5 oC - 55 oC. The micro-shear bond strength test (μSBS) was measured using universal testing machine. Kruskal-Wallis test was used to compare between the three cements. Dunn’s test was used for pair-wise comparisons when Kruskal-Wallis test is significant. Mann-Whitney U test was used to compare between micro-shear bond strength before and after thermocycling P ≤ 0.05. Results: In non-aged subgroups, there was no significant difference between Panavia and Activa; both showed significantly the highest mean μSBS values (22.9 MPa, 31.3 MPa respectively). While, RMGI showed the lowest μSBS values (4.7 MPa).  In thermocycled subgroups, Panavia showed significantly the highest mean μSBS values (32.2 MPa). There was no significant difference between RMGI and Activa; both showed the lowest significant mean μSBS values (3.2 MPa and 8.7 MPa respectively). Conclusions: RMGI and Activa couldn’t be considered long-term reliable materials for cementing zirconia. However, Panavia provided the most durable bond to zirconia.KEYWORDSBioactive cement; Micro-shear bond strength; Resin cement; Translucent zirconia.

scholarly journals In vitro Study of the Effect of Internal Relief Space on the Color of Ceramic Laminate Veneer

2021 ◽  
Vol 9 (D) ◽  
pp. 37-42
Author(s):  
Abd El Azeem Mostafa ◽  
Cherif A. Mohsen
Keyword(s):  
Computer Aided Design ◽  
Color Change ◽  
In Vitro Study ◽  
Resin Cement ◽  
Lithium Silicate ◽  
Standard Design ◽  
Significant Difference ◽  
Computer Aided ◽  
Cad Cam

BACKGROUND: Ceramic laminate veneer restoring is considered a challenging modality in solving various esthetic dental problems. AIM: The purpose of this study was to investigate the effect of digital internal relief space on the color of ceramic laminate veneer. MATERIALS AND METHODS: An acrylic central incisor model was prepared for ceramic laminate veneer with standard measures. The prepared acrylic resin dentotype model was scanned with intraoral computer-aided design/computer-aided manufacturing (CAD/CAM) optical scanner (CEREC Omnicam|Dentsply Sirona). The laminate veneer design was planned on the optically scanned preparation on CAD/CAM system software (CEREC software|Dentsply Sirona). Thirty ceramic laminate veneer specimens were machined from zirconia-reinforced lithium silicate (Celtra Duo blocks, Dentsply/Sirona) according to standard design by CAD/CAM system with the change of the digital internal relief space settings. The specimens were divided into three groups according to their digital internal relief settings (IRS) (20, 60, and 100 μm) (n = 10). Thirty epoxy dies were duplicated from the prepared acrylic model. The ceramic laminate veneer specimens were cemented to epoxy dies with total etch resin cement system according to the manufacture instructions. The color change (ΔE) of the cemented ceramic laminate veneer specimens was measured by spectrophotometer (Vita Easy shade, Ivoclar Vivadent AG, Schaan, Liechtenstein) using the CIELAB scale and L*, a*, b*. Each specimen was measured two times (before and after cementation). The value of color difference (ΔE) was calculated according to the formula: ΔE = [(L*2 - L*1)2 + (a*2 - a*1)2 + (b*2- b*1) 2]½. RESULTS: The highest mean value of ΔE was recorded in G100 group (1.91 ± 0.33), followed by G60 group (1.83 ± 0.09), with the least value recorded in G20 group (1.49 ± 0.49). Analysis of variance test revealed a statistically significant difference between groups (p = 0.024). CONCLUSION: The change of the digital IRS affects the color of ceramic laminate veneers.

scholarly journals Influence of drying time of adhesive systems on the bond strength between resin cement and feldspathic ceramic

2016 ◽  
Vol 19 (1) ◽  
pp. 88
Author(s):  
Sabrina Alves Feitosa ◽  
Isabela Gomes Moura ◽  
Pedro Henrique Corazza ◽  
Cesar Dalmolin Bergolli ◽  
Clóvis Pagani ◽  
...  
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Resin Cement ◽  
Ceramic Surface ◽  
Drying Time ◽  
Ceramic Block ◽  
Significant Difference ◽  
Before And After ◽  
Cad Cam ◽  
Ceramic Blocks

<p><strong>O</strong><span lang="en-US"><strong>bjective: </strong></span><span lang="en-US">This study evaluated the effect of drying times of two total-etch &amp; rinse adhesives on the resin bond strength to a feldsphatic ceramic, before and after aging. </span><span lang="en-US"><strong>Material and Methods: </strong></span><span lang="en-US">Feldsphatic-ceramic CAD-CAM bars were cut into blocks (12×10×4 mm) with a cutting machine (N = 32). </span><span lang="en-US">Impressions were made of each ceramic block with silicone putty material and the negative space was filled with a composite resin.</span><span lang="en-US"> The bonding ceramic surface was etched with hydrofluoric acid, silanized, and the adhesive system (SB- Single Bond 2, 3M-ESPE; or PB- Prime &amp; Bond NT, Dentsply) was applied. The samples were dried at different times (5, 10 and 15 s) before the cementation. The resin and ceramic blocks were cemented by a dual cure resin cement. All samples were stored in distilled water at 37 °C for 24 h. For the μ-TBS test, the samples were sliced into microbars. Half of the bars of each block was tested after 24 h and, the other bars </span><span lang="en-US">were submitted to thermocycling (12,000×) and water storage (150 d)</span><span lang="en-US">. For the 24 h groups, the longer drying time increased (p &lt; 0.05) the bond strength of SB (water/alcohol adhesive), while reduced (p &lt; 0.05) for the PB group (acetone based adhesive). </span><span lang="en-US"><strong>Results: </strong></span><span lang="en-US">For the aged groups, the bond strength for the different drying times had no significant difference, for the both adhesives. </span><span lang="en-US"><strong>Conclusion:</strong></span><span lang="en-US"> Longer drying times increased the bond strength values of SB. Smaller drying times increased the bond strength values of PB. The aging protocol influenced the bond strength of SB groups.</span></p><p class="western"> </p><p class="western" lang="pt-BR"><span><span><span lang="en-US"><strong>Keywords:</strong></span></span></span><span><span><span lang="en-US"><span> Microtensile; Adhesion; Feldspar ceramic; Drying time; Adhesive system.</span></span></span></span></p>

Effects of Desensitizers, Temporary Cements, and Dentin Cleaning Methods on the Bond Strength of Self-Etch/ Adhesive Resin Cements to Dentin: An In Vitro Study

2021 ◽  
pp. 232020682110527
Author(s):  
Mehmet Uğur ◽  
I˙dris Kavut ◽  
Şafak Külünk ◽  
Mehmet Şerif Akdeniz ◽  
Özgür Ozan Tanrıkut
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Cleaning Methods ◽  
Self Etch

Aim: The aim of this study was to evaluate the effect of desensitizer, temporary cements, dentin cleaning methods on shear bond strength (SBS) of self-etch and self-adhesive resin cements to dentin. Materials and Methods: Four hundred eighty buccal or lingual/palatine coronal portions of human molar teeth were mounted in the acrylic blocks. Teeth surfaces were prepared until the dentin was exposed. Specimens were divided into four groups. One group separated as control and three groups of teeth were treated with a desensitizing agent containing calcium-phosphate desensitizer (Teethmate Desensitizer, TMD), resin-based self-reinforcing monomer (Shield Force Plus, SFP) and 2-hydroxyethyl methacrylate and glutaraldehyde (Gluma Desensitizer). Two different temporary cement containing calcium hydroxide (Dycall) and zinc oxide based (Rely X Temp NE) temporary cement were applied to the dentin surfaces. Temporary cement was removed with one of three cleansing techniques: 2% chlorhexidine digluconate and glass particles containing agent (Consepsis Scrub), cleansing bur (OptiClean), and ıntra/extracoronal rotary brush (Starbrush). All groups were further divided into two cementation subgroups (Panavia V5 and Panavia SA). The SBS (MPa) was measured using a universal testing machine at 0.5 mm/min crosshead speed. The data were analyzed statistically with a four-way analysis of variance and Tukey’s Honest Significant Difference test ( α = 0.05). Results: Although SFP showed higher SBS, there was no statistically significant difference between other groups ( P > .05). There were no significant differences between temporary cements ( P > .05). OptiClean rotary bur showed higher mean SBS values in all groups. The dual-polymerized Panavia V5 showed the highest SBS values in all groups ( P <.05). Conclusion: Cleaning of dentin surface from temporary cement remnants with a silicon bur and dual-cure resin cement showed the highest bond strength values.

scholarly journals Bond Strength Stability of Different Dual-Curing Adhesive Cements towards CAD-CAM Resin Nanoceramic: An In Vitro Study

2021 ◽  
Vol 11 (9) ◽  
pp. 3971
Author(s):  
Vergano Edoardo Alberto ◽  
Baldi Andrea ◽  
Comba Allegra ◽  
Italia Edoardo ◽  
Ferrero Giorgio ◽  
...  
Keyword(s):  
Bond Strength ◽  
Artificial Saliva ◽  
In Vitro Study ◽  
Test Technique ◽  
Adhesive Luting ◽  
Luting Cement ◽  
Significant Difference ◽  
Cad Cam ◽  
Diamond Saw

Background: To evaluate different adhesive luting procedures on coronal dentin bond-strength of Cerasmart CAD-CAM blocks with μTBS test. Methods: 36 molar crowns were flattened in order to expose sound dentin and a standardized smear layer was created with 600 grit paper. Specimens were divided into six groups according to the luting cement employed (n = 12 each): G1: Panavia V5 (Kuraray, Japan); G2: Bifix QM (Voco, Germany); G3: Estecem (Tokuyama, Japan). CAD-CAM blocks (Cerasmart, GC), shade A2LT, size 14, were sectioned with a diamond saw to obtain 4 mm high specimens, which were then luted on the coronal dentin, following the manufacturer instructions. Specimens were serially sectioned to obtain 1 mm thick beams in accordance with the μTBS test technique. Half of the beams were stressed to failure after 24 h (t = 0), while the other half were stored in artificial saliva for 12 months, at 37 °C, for ageing before stressing to failure (t = 12). Results: two-way ANOVA test showed significant difference for the factor “luting cement” (p = 0.0002), while the factor “time of storage” (p = 0.0991) had no significant effect on µTBS. Conclusions: PanaviaV5 seems to have better µTBS values at T0 than QM and ES and 1 year aging doesn’t seem to affect the bonding strength of tested systems.

scholarly journals Marginal and Internal Fit of Ceramic Prostheses Fabricated from Different Chairside CAD/CAM Systems: An In Vitro Study

2021 ◽  
Vol 11 (2) ◽  
pp. 857
Author(s):  
Keunbada Son ◽  
Kyu-Bok Lee
Keyword(s):  
Computer Aided Design ◽  
In Vitro Study ◽  
Vitro Study ◽  
Marginal Gap ◽  
Significant Difference ◽  
Cad Cam ◽  
Ceramic Crowns ◽  
Internal Fit ◽  
Cam Systems

The purpose of this in vitro study was to evaluate marginal and internal fits of ceramic crowns fabricated with chairside computer-aided design and manufacturing (CAD/CAM) systems. An experimental model based on ISO 12836:2015 was digitally scanned with different intraoral scanners (Omnicam (CEREC), EZIS PO (DDS), and CS3500 (Carestream)). Ceramic crowns were fabricated using the CAD/CAM process recommended by each system (CEREC, EZIS, and Carestream systems; N = 15). The 3-dimensional (3D) marginal and internal fit of each ceramic crown was measured using a 3D inspection software (Geomagic control X). Differences among the systems and various measurements were evaluated using the Kruskal–Wallis test. Statistically significant differences were validated using pairwise comparisons (α = 0.05). Occlusal gaps in the CEREC, EZIS, and Carestream groups were 113.0, 161.3, and 438.2 µm, respectively (p < 0.001). The axial gaps were 83.4, 78.0, and 107.9 µm, respectively. The marginal gaps were 77.8, 99.3, and 60.6 µm, respectively, and the whole gaps were 85.9, 107.3, and 214.0 µm, respectively. Significant differences were observed with the EZIS system compared with the other two systems in terms of the marginal gap sizes. The CEREC system showed no significant differences among the four measured regions. However, the EZIS and Carestream systems did show a statistically significant difference (p < 0.05). All three systems were judged to be capable of fabricating clinically acceptable prostheses, because the marginal gap, which is the most important factor in the marginal fit of prostheses, was recorded to be below 100 µm in all three systems.

Development of a Cavity Disinfectant Containing Antibacterial Monomer MDPB

2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  
Keyword(s):  
Antibacterial Activity ◽  
Bond Strength ◽  
Bacterial Species ◽  
Oral Bacteria ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Adhesive Resin Cement

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.

scholarly journals Efficacy of Fiber Post Bonding To Root Dentin after Different Obturation Techniques and Cementation Timings: In Vitro Study

2018 ◽  
Vol 6 (9) ◽  
pp. 1707-1711
Author(s):  
Rami M. Atia ◽  
Nada Omar ◽  
Haidy Nabil ◽  
Yousra Aly
Keyword(s):  
Bond Strength ◽  
Statistical Significance ◽  
Testing Machine ◽  
In Vitro Study ◽  
Resin Cement ◽  
Vitro Study ◽  
Endodontically Treated Teeth ◽  
Root Dentin ◽  
Push Out

OBJECTIVE: The aim of this in vitro study was to assess the effect of obturation technique and cementation timings on the bonding of fibre-reinforced posts to the root canal walls. METHODS: Twenty extracted teeth were randomly allocated to two groups according to the obturation technique and cementation timing. Central incisors with single canals were used after being decoronated. Every extracted tooth of the {vertical compaction group} (VC) group (n = 10) had been obturated using the {E & Q plus obturation system} with posts cemented in the same day; The other (CO) conventional group (n = 10) teeth were obturated using the conventional lateral compaction technique and posts cemented after one week. “SF“ Fiber posts were used after bonding and cementation using Rely X ARC resin cement with all the endodontically treated teeth. The push-out test was performed in a universal testing machine. Data were analysed by 2 way analysis of variance with Statistical significance was set to 0.05. RESULTS: Heat softened gutta percha group showed more push out the bond strength of the bonded posts than the conventional obturation group (p < 0.05). In the middle region, there was no statistical significance between the two groups while there was significance in the coronal and apical thirds. CONCLUSION: The vertical compaction technique and early cementation improved the bond strength of the resin posts in comparison to the conventional obturation technique with late cementation.

scholarly journals Effects of Universal Adhesive on Shear Bond Strength of Resin Cement to Zirconia Ceramic with Different Surface Treatments

2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Surface Treatments ◽  
Resin Cement ◽  
Zirconia Ceramic ◽  
Single Bond ◽  
Universal Adhesive

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.

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