scholarly journals Smart Starch-Gelatin Films Incorporated with Curcumin

2020 ◽  
Vol 36 (6) ◽  
pp. 1088-1095
Author(s):  
Le Thi Bich Nguyet ◽  
Vinh Tien Nguyen
Keyword(s):  
Acetic Acid ◽  
Food Packaging ◽  
Gelatin Film ◽  
Film Properties ◽  
Elongation At Break ◽  
Independent Variables ◽  
Gelatin Films ◽  
Film Forming ◽  
Central Composite Experimental Design ◽  
Central Composite

In this study, we developed a starch-gelatin film incorporated with synthesized curcumin to be used as a pH-sensitive smart material for food packaging. The film-forming mixture contained five components: starch, gelatin, glycerol, acetic acid and curcumin. The interactions of the components and their effects on the film properties were investigated by using response surface methodology with central composite experimental design. The results showed impacts of the contents of these components as independent variables on tensile strength, elongation at break, Young’s modulus and solubility of the films. The contents of starch, gelatin and glycerol significantly affect these properties, while acetic acid and curcumin do not (p<0.05). Also, it was shown that the incorporation of curcumin provided the film with the capacity to sense pH changes from neutral to basic (yellow at pH ≤ 8 and orange-red at pH ≥ 9).

Physicochemical Properties of Biodegradable Tilapia Skin Gelatin Film and Gelatin-Polysaccharide Based Composite Films

2014 ◽  
Vol 941-944 ◽  
pp. 1133-1140 ◽  
Author(s):  
Shuai Peng ◽  
Li Hong Niu ◽  
Ke Qiang Lai ◽  
Yi Qun Huang
Keyword(s):  
Tensile Strength ◽  
Composite Film ◽  
Composite Films ◽  
Water Vapor Permeability ◽  
Gelatin Film ◽  
Vapor Permeability ◽  
Film Properties ◽  
Arabic Gum ◽  
Gelatin Films ◽  
Film Forming

The present study was to investigate the film forming properties of tilapia skin gelatin as affected by the addition of 2%, 5% Arabic gum or pectin (g/g gelatin), as well as 1%, 2% glutaraldehyde (GTA) (g/g gelatin) in an attempt to improve gelatin film properties. Tensile strength (TS) and transparency of gelatin film were improved 36.6% and 30.3% by the addition of Arabic gum, respectively, while the water vapor permeability (WVP) was not affected. The addition of pectin had less effect on the film tensile strength and transparency, but led to 41.7% of increase in WVP. Tensile strength and WVP of gelatin-arabic gum composite film cross-linked with 2% GTA were better than those of 1% GTA cross-linked composite film, though the extensibility and transparency were slightly weak. The FTIR spectra of gelatin films showed that both Arabic gum and pectin formed cross-linkages with gelatin protein molecules, while GTA facilitated the formation of intermolecular bonds, resulting in more stable films.

Fish gelatin films laminated with emulsified gelatin film or poly(lactic) acid film: Properties and their use as bags for storage of fried salmon skin

2021 ◽  
Vol 111 ◽  
pp. 106199 ◽  
Author(s):  
Krisana Nilsuwan ◽  
Pedro Guerrero ◽  
Koro de la Caba ◽  
Soottawat Benjakul ◽  
Thummanoon Prodpran
Keyword(s):  
Lactic Acid ◽  
Gelatin Film ◽  
Poly Lactic Acid ◽  
Fish Gelatin ◽  
Film Properties ◽  
Gelatin Films

Gelatin Films and its Pregelatinized Starch Blends: Effect of Plasticizers

2017 ◽  
Vol 751 ◽  
pp. 230-235 ◽  
Author(s):  
Suchipha Wannaphatchaiyong ◽  
Prapaporn Boonme ◽  
Wiwat Pichayakorn
Keyword(s):  
Tensile Strength ◽  
Gelatin Solution ◽  
Film Properties ◽  
Polyethylene Glycol 400 ◽  
Elongation At Break ◽  
Gelatin Films ◽  
Gel Film ◽  
Starch Gel ◽  
Pregelatinized Starch ◽  
Starch Blends

This study aimed to develop gelatin (GEL) and gelatin/Alpha starch (GEL/αSt) dissolving films as drug delivery by casting method. Because these films were brittle and lack of elasticity, therefore, glycerin (GLY), propylene glycol (PG) or polyethylene glycol 400 (PEG) in various amounts (5-30 part per hundred of gelatin; phg) was used as plasticizer. It was found that all types and amounts of plasticizer could be blended into gelatin solution and the transparent GEL films were formed, except the GEL/PEG films presented in opaque characteristics. However, 30 phg GLY blended film was too softy. Increasing amount of plasticizer caused a decrease in tensile strength and increase in elongation at break (EAB) of films. These GEL films swelled, dissolved and eroded in 2 hours. The αSt was also blended, and the effects of αSt amounts (5-30 phg) and plasticizer types (at 25 phg) on GEL film properties were studied. The αSt dispersions mixed well in gelatin solution and gave homogenous films. The swelling and erosion of GEL/αSt films in water were faster than those of GEL films. Increasing αSt amount prolonged the swelling time and decreased the degradation rate of GEL/αSt films. The tensile strength of GEL/αSt/GLY films slightly increased when the αSt amount increased but those of PEG and PG blended films were not different. The EAB of all plasticizer blended films decreased when the amount of αSt increased. Either lidociane or lidociane hydrochloride was mixed in GEL/αSt/GLY dissolving films to use as local anesthetic. The morphology, Fourier Transform Infrared Spectroscopy confirmed their compatibilities in these films, but Differential Scanning Calorimeter showed some changes that should be further evaluated.

scholarly journals Antioxidant, Antibacterial, Water Binding Capacity and Mechanical Behavior of Gelatin-Ferula Oil Film as a Wound Dressing Material

2015 ◽  
Vol 4 (2) ◽  
pp. 103-14
Author(s):  
Gholamreza Kavoosi ◽  
Amin Shakiba ◽  
Mahmood Ghorbani ◽  
Seyed Mohammad Mahdi Dadfar ◽  
Amin Mohammadi Purfard
Keyword(s):  
Water Vapor ◽  
Wound Dressing ◽  
Water Solubility ◽  
Water Vapor Permeability ◽  
Antibacterial Activities ◽  
Gelatin Film ◽  
Vapor Permeability ◽  
Elongation At Break ◽  
Gelatin Films ◽  
Water Swelling

Background: Development of biodegradable and biocompatible films based on protein polymer with strong antioxidant and antibacterial activities has gradually obtained extensive concern in the world. In this study, the improvement of gelatin film properties incorporated with Ferula assa-foetida essential oil (FAO) as a potential antioxidant/antibacterial wound dressing film was investigated. Materials and Methods: Gelatin films were prepared from gelatin solutions (10% w/v) containing different concentration of FAO. The effect of FAO addition on water solubility, water swelling, water vapor permeability, mechanical behavior, light barrier properties as well as antioxidant and antibacterial activities of the films were examined. Results: Water solubility, water swelling and water vapor permeability for pure gelatin films were 29 ± 1.6%, 396 ± 8%, 0.23 ± 0.018 g.mm/m2.h, respectively. Incorporation of FAO into gelatin films caused a significant decrease in swelling and increase in solubility and water vapor permeability. Tensile strength, elastic modulus and elongation at break for pure gelatin films were 4.2 ± 0.4 MPa, 5.8 ± 4.2 MPa, 128 ± 8 %, respectively. Incorporation of FAO into gelatin films caused a significant decrease in tensile strength and elastic modulus and increase in elongation at break of the films. Gelatin film showed UV-visible light absorbance ranging from 280 to 480 nm with maximum absorbance at 420 nm. Gelatin/FAO films also exhibited excellent antioxidant ad antimicrobial activities. Conclusions: Our results suggested that gelatin/FAO films could be used as active films due to their excellent antioxidant and antimicrobial features for different biomedical applications including wound-dressing materials.[GMJ.2015;4(2):103-14]

scholarly journals Gelatin Films Modified with Acidic and Polyelectrolyte Polymers—Material Selection for Soft Gastroresistant Capsules

Polymers ◽  
2019 ◽  
Vol 11 (2) ◽  
pp. 338 ◽  
Author(s):  
Bartosz Maciejewski ◽  
Małgorzata Sznitowska
Keyword(s):  
Material Selection ◽  
Continuous Phase ◽  
Gelatin Film ◽  
Scanning Calorimetry ◽  
Adhesive Properties ◽  
Polyelectrolyte Complexes ◽  
Gelatin Films ◽  
Film Forming ◽  
Anionic Polysaccharides ◽  
Insoluble Polymers

The following investigation comprised the formation of acid-resistant gelatin-based films, intended for future use in soft-capsule technology. Such film compositions were obtained by including nonionized forms of acid-insoluble polymers in a gelatin-based film-forming mixture. The selected films were additionally modified with small amounts of anionic polysaccharides that have potential to interact with gelatin, forming polyelectrolyte complexes. The obtained film compositions were subjected to, e.g., disintegration tests, adhesiveness tests, differential scanning calorimetry (DSC), and a transparency study. As a result of the performed study, some commercial enteric polymers (acrylates), as well as cellulose acetate phthalate, were selected as components that have the ability to coalesce and form a continuous phase within a gelatin film. The use of a small amount (1.5%) of additional gelling polymers improved the rheological characteristics and adhesive properties of the obtained films, with ί-carrageenan and gellan gum appearing to be the most beneficial.

scholarly journals Prototype Gastro-Resistant Soft Gelatin Films and Capsules—Imaging and Performance In Vitro

Materials ◽  
2020 ◽  
Vol 13 (7) ◽  
pp. 1771
Author(s):  
Bartosz Maciejewski ◽  
Vishnu Arumughan ◽  
Anette Larsson ◽  
Małgorzata Sznitowska
Keyword(s):  
Drug Release ◽  
Acidic Medium ◽  
Diclofenac Sodium ◽  
Gelatin Film ◽  
Cellulose Acetate Phthalate ◽  
Critical Feature ◽  
Gelatin Films ◽  
Film Forming ◽  
And Performance

The following study is a continuation of the previous work on preparation of gastro-resistant films by incorporation of cellulose acetate phthalate (CAP) into the soft gelatin film. An extended investigation on the previously described binary Gelatin-CAP and ternary Gelatin-CAP-carrageenan polymer films was performed. The results suggest that the critical feature behind formation of the acid-resistant films is a spinodal decomposition in the film-forming mixture. In the obtained films, upon submersion in an acidic medium, gelatin swells and dissolves, exposing a CAP-based acid-insoluble skeleton, partially coated by a residue of other ingredients. The dissolution-hindering effect appears to be stronger when iota-carrageenan is added to the film-forming mixture. The drug release study performed in enhancer cells confirmed that diclofenac sodium is not released in the acidic medium, however, at pH 6.8 the drug release occurs. The capsules prepared with a simple lab-scale process appear to be resistant to disintegration of the shell structure in acid, although imperfections of the sealing have been noticed.

scholarly journals Physicochemical and Antimicrobial Properties of Whey Protein-Based Films Functionalized with Palestinian Satureja capitata Essential Oil

Coatings ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1364
Author(s):  
Manar Abdalrazeq ◽  
Nidal Jaradat ◽  
Mohammad Qadi ◽  
C. Valeria L. Giosafatto ◽  
Eliana Dell’Olmo ◽  
...  
Keyword(s):  
Antimicrobial Activity ◽  
Essential Oil ◽  
Food Packaging ◽  
Pathogenic Bacteria ◽  
Whey Proteins ◽  
Antimicrobial Properties ◽  
Wild Plants ◽  
Gram Negative Bacteria ◽  
Elongation At Break ◽  
Film Forming

The present study aimed to produce bio-active packaging materials made of whey proteins (WPs) and essential oil (EO) extracted from Thymbra (Satureja capitata, L.), one of the most popular Palestinian wild plants. In this study, two different Thymbra leaves from Nablus and Qabatiya in Palestine were collected and analyzed for EOs by gas chromatography and mass spectrometry. Based on the analysis, two EOs, namely, TEO1 and TEO2, were extracted, and it was found that both samples primarily contain γ-terpinene and carvacrol, whereas p-cymene was detected only in TEO1. The antimicrobial activity of TEO1 and TEO2 was evaluated by microbroth microdilution assays against pathogenic bacteria and yeast. Based on the results, TEO1 exhibited potent antimicrobial activity against the test strains. Besides, TEO1 was chosen to functionalize WP-based films at different concentrations (0.1%, 0.4%, and 0.8% v/v of Film Forming Solutions). Film mechanical property investigation showed a marked reduction in the tensile strength and Young’s modulus at 0.8% TEO1. In contrast, its elongation at break value was significantly (p < 0.05) increased due to the plasticizing effect of the EO. Moreover, the film transparency was found to be significantly (p < 0.05) reduced by increasing TEO1 concentrations. Finally, microbiological investigations indicated that film antimicrobial activity against both gram-positive and gram-negative bacteria increased dose-dependently. The overall results open interesting perspectives for employing these films as preservative materials in food packaging.

scholarly journals Preparation and Characterization of Ginger Essential Oil Microcapsule Composite Films

Foods ◽  
2021 ◽  
Vol 10 (10) ◽  
pp. 2268
Author(s):  
Huahua Wang ◽  
Mengyao Li ◽  
Zhouyong Dong ◽  
Tiehua Zhang ◽  
Qingyu Yu
Keyword(s):  
Essential Oil ◽  
Food Packaging ◽  
Composite Films ◽  
Storage Period ◽  
Gelatin Film ◽  
Scanning Calorimetry ◽  
Application Range ◽  
Gelatin Films ◽  
Entire Storage Period ◽  
High Level

New food packaging has shown research significance in the face of increasing demand for high-quality foods and growing attention paid to food safety. In this study, ginger essential oil microcapsule composite films were prepared by combining microcapsules prepared by a complex coacervation method with gelatin films, and the mechanical properties and active functions of the composite films were analyzed. Fourier-transform infrared spectroscopy and differential scanning calorimetry confirmed the successful encapsulation of ginger essential oil. The scanning electron microscopy of the composite films showed the microcapsules and gelatin film matrix were highly compatible. During the entire storage period, the antioxidant capacity of the ginger essential oil microcapsule films weakened more slowly than ginger essential oil microcapsules and could be maintained at a relatively high level for a long time. The microcapsule films had excellent inhibitory effects on Escherichia coli, Staphylococcus aureus, and Bacillus subtilis. Therefore, the direct addition of microcapsules to a film matrix can broaden the application range of microcapsules and increase the duration of the release of active ingredients. Ginger essential oil microcapsule films are potential biodegradable food packaging films with long-lasting activity.

scholarly journals EFFECT OF PREPARING CONDITIONS ON PROPERTIES OF GELATIN FILM FROM HORSE MACKEREL SCALE

2015 ◽  
Vol 2 (1) ◽  
pp. 32
Author(s):  
Le Thi Minh Thuy ◽  
Emiko Okazaki ◽  
Kazufumi Osako
Keyword(s):  
Protein Content ◽  
Protein Concentration ◽  
Gelatin Film ◽  
Edible Film ◽  
Horse Mackerel ◽  
Protein Patterns ◽  
Film Property ◽  
Gelatin Films ◽  
Film Forming ◽  
Sds Page

In this study, the effect of preparing conditions, such as protein concentrations and glycerol concentrations of film forming solution (FFS) on properties of gelatin film from horse mackerel scale were investigated. Properties of edible film from gelatin was extracted at 70oC for 1 h at various protein concentrations (1, 2, and 3%) in film-forming solution (FFS) were examined.. Films from FFS containing higher protein content showed the higher TS and EAB. WVP of film increased with increasing protein concentration of FFS. The study about the effect of glycerol in FFS on the film property showed that addition of glycerol as a plasticizer into FFS at the concentrations of 0, 10, 15, 20 and 25 % of protein lead to the decline of TS of gelatin film, while both EAB and WVP of film increased. The SDS-PAGE patterns showed that all gelatin films consisted of two different α chains, α1 and α2, as well as a β component and no differences in protein patterns among the protein concentrations and glycerol concentrations of FFS.Keywords: gelatin, films, horse mackerel, scales.

Preparation and Characterization of β-glucosidase Films for Stabilization and Handling in Dry Configurations

2020 ◽  
Vol 21 (8) ◽  
pp. 741-747
Author(s):  
Liguang Zhang ◽  
Yanan Shen ◽  
Wenjing Lu ◽  
Lengqiu Guo ◽  
Min Xiang ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Protein Function ◽  
Protein Stabilization ◽  
Functional Protein ◽  
Elongation At Break ◽  
Gelatin Films ◽  
The Stability ◽  
And Function ◽  
General Method

Background: Although the stability of proteins is of significance to maintain protein function for therapeutical applications, this remains a challenge. Herein, a general method of preserving protein stability and function was developed using gelatin films. Method: Enzymes immobilized onto films composed of gelatin and Ethylene Glycol (EG) were developed to study their ability to stabilize proteins. As a model functional protein, β-glucosidase was selected. The tensile properties, microstructure, and crystallization behavior of the gelatin films were assessed. Result: Our results indicated that film configurations can preserve the activity of β-glucosidase under rigorous conditions (75% relative humidity and 37°C for 47 days). In both control films and films containing 1.8 % β-glucosidase, tensile strength increased with increased EG content, whilst the elongation at break increased initially, then decreased over time. The presence of β-glucosidase had a negligible influence on tensile strength and elongation at break. Scanning electron-microscopy (SEM) revealed that with increasing EG content or decreasing enzyme concentrations, a denser microstructure was observed. Conclusion: In conclusion, the dry film is a promising candidate to maintain protein stabilization and handling. The configuration is convenient and cheap, and thus applicable to protein storage and transportation processes in the future.

Sign in / Sign up

Export Citation Format

Share Document