scholarly journals A Procedure of Separation and Preconcentration for Titanium Determination in Sawater Samples by ICP-OES

2007 ◽  
Vol 2 (1) ◽  
pp. 1-11 ◽  
Author(s):  
Sérgio Rocha ◽  
Sérgio Ferreira
Keyword(s):  
Icp Oes ◽  
Titanium Determination ◽  
Separation And Preconcentration

An on-line matrix separation and preconcentration procedure for ICP-OES determination of Cd, Co, Cu, Mn and Pb traces in Zr and Zr-Nb alloys using a cation-exchange resin microcolumn

2021 ◽  
Author(s):  
Masoud Aghahoseini ◽  
Gholamhassan Azimi ◽  
M. K. Amini
Keyword(s):  
Inductively Coupled Plasma ◽  
Cation Exchange Resin ◽  
Optical Emission ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Inductively Coupled ◽  
Separation And Preconcentration ◽  
On Line ◽  
Plasma Optical Emission Spectrometry

Determination of traces of Cd, Co, Cu, Mn and Pb elements in zirconium and its alloys by inductively coupled plasma optical emission spectrometry (ICP OES) suffers from severe spectral interferences...

Determination of traces of palladium in stream sediment and auto catalyst by FI-ICP-OES using on-line separation and preconcentration with QuadraSil TA

Talanta ◽  
2009 ◽  
Vol 79 (4) ◽  
pp. 1050-1054 ◽  
Author(s):  
Junichi Nakajima ◽  
Masashi Ohno ◽  
Katsumi Chikama ◽  
Tatsuya Seki ◽  
Koichi Oguma
Keyword(s):  
Stream Sediment ◽  
Icp Oes ◽  
Separation And Preconcentration ◽  
On Line ◽  
Line Separation

scholarly journals ICP-OES Determination of Trace Metal Ions after Preconcentration Using Silica Gel Modified with 1,2-Dihydroxyanthraquinone

2012 ◽  
Vol 9 (2) ◽  
pp. 1007-1016 ◽  
Author(s):  
Reem M. Alghanmi
Keyword(s):  
Trace Metal ◽  
Metal Ions ◽  
Silica Gel ◽  
Inductively Coupled Plasma ◽  
Emission Spectrometry ◽  
Icp Oes ◽  
Trace Metal Ions ◽  
Relative Standard ◽  
Separation And Preconcentration

A new chelating matrix was prepared by immobilizing 1,2-dihydr-oxyanthraquinone, or alizarin (AZ), on silica gel modified with (3-aminopropyl)trimethoxysilane. The matrix was characterized by FTIR spectroscopy and elemental analysis. The new matrix was used to preconcentrate Cd(II), Cu(II), Ni(II), Pb(II) and Zn(II) prior to their determination by inductively coupled plasma optical emission spectrometry (ICP-OES). The optimum pH was 5 and the optimum extraction time was approximately 15 minutes using the batch method. Common electrolytes and metal ions did not interfere with the separation and determination of the analytes. The adsorption capacity of the new sorbent was 67.4, 163.5, 212.8, 76.4 and 180.3 μmol/g for Cd(II), Cu(II), Ni(II), Pb(II) and Zn(II), respectively. The relative standard deviations (RSD) were less than 3.0%. This method allowed for successful separation and preconcentration of trace metal ions in different water samples with satisfactory results.

Thiol-rich polyhedral oligomeric silsesquioxane-modified magnetic nanoparticles for the highly efficient separation and preconcentration of Cd(ii) and Pb(ii) in food and water prior to ICP-OES determination

2018 ◽  
Vol 33 (11) ◽  
pp. 1974-1980 ◽  
Author(s):  
Peng Li ◽  
Jing Wang ◽  
Fei Pei ◽  
Qin Liu ◽  
Yong Fang ◽  
...  
Keyword(s):  
Magnetic Nanoparticles ◽  
Polyhedral Oligomeric Silsesquioxane ◽  
Icp Oes ◽  
Efficient Separation ◽  
Highly Efficient ◽  
Separation And Preconcentration ◽  
Modified Magnetic Nanoparticles ◽  
Oligomeric Silsesquioxane

Thiol-rich polyhedral oligomeric silsesquioxane modified magnetic nanoparticles as a novel adsorbent for the extraction of Cd(ii) and Pb(ii) in foods.

scholarly journals Separation of 44Sc from Natural Calcium Carbonate Targets for Synthesis of 44Sc-DOTATATE

Molecules ◽  
2018 ◽  
Vol 23 (7) ◽  
pp. 1787 ◽  
Author(s):  
Krzysztof Kilian ◽  
Łukasz Cheda ◽  
Mateusz Sitarz ◽  
Katarzyna Szkliniarz ◽  
Jarosław Choiński ◽  
...  
Keyword(s):  
Calcium Concentration ◽  
Small Volume ◽  
Isotope Separation ◽  
Efficient Production ◽  
Icp Oes ◽  
Wide Range ◽  
Separation And Preconcentration ◽  
Metallic Impurities ◽  
Automatic Systems

The rapid increase in applications of scandium isotopes in nuclear medicine requires new efficient production routes for these radioisotopes. Recently, irradiations of calcium in cyclotrons by α, deuteron, and proton beams have been used. Therefore, effective post-irradiation separation and preconcentration of the radioactive scandium from the calcium matrix are important to obtain the pure final product in a relatively small volume. Nobias resin was used as a sorbent for effective separation of 44Sc from calcium targets. Separation was performed at pH 3 using a column containing 10 mg of resin. Scandium was eluted with 100 μL of 2 mol L−1 HCl. Particular attention was paid to the reduction of calcium concentration, presence of metallic impurities, robustness and simple automation. 44Sc was separated with 94.9 ± 2.8% yield, with results in the range of 91.7–99.0%. Purity of the eluate was confirmed with ICP-OES determination of metallic impurities and >99% chelation efficiency with DOTATATE, followed by >36 h radiochemical stability of the complex. A wide range of optimal conditions and robustness to target variability and suspended matter facilitates the proposed method in automatic systems for scandium isotope separation and synthesis of scandium-labeled radiopharmaceuticals.

scholarly journals Separation and preconcentration followed by ICP-OES and ICP-MS determination of precious metals using silica gel chemically modified with dithiocarbamate groups

2019 ◽  
Vol 55 (15) ◽  
pp. 2659-2669 ◽  
Author(s):  
Vladimir N. Losev ◽  
Victoriya V. Parfenova ◽  
Evgeney V. Elsuf’ev ◽  
Elena V. Borodina ◽  
Segey I. Metelitsa ◽  
...  
Keyword(s):  
Silica Gel ◽  
Precious Metals ◽  
Icp Oes ◽  
Chemically Modified ◽  
Icp Ms ◽  
Separation And Preconcentration

Titanium determination in human blood plasma by ICP-OES, longitudinally, and transversally heated Zeeman ETAAS

1998 ◽  
Vol 13 (10) ◽  
pp. 1173-1176 ◽  
Author(s):  
Thorsten J. Einhäuser ◽  
Thomas G. Pieper ◽  
Bernhard K. Keppler
Keyword(s):  
Blood Plasma ◽  
Human Blood ◽  
Human Blood Plasma ◽  
Icp Oes ◽  
Titanium Determination
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