Quantitative Calibration Models for the Determination of Azithromycin and Decladinosylazithromycin in Azithromycin Injection Powder by Using Diffuse Reflectance near Infrared Spectroscopy

2011 ◽  
Vol 19 (4) ◽  
pp. 265-275 ◽  
Author(s):  
Ji-Xiong Dong ◽  
Wen-Bo Zhou ◽  
Yan-Chun Feng ◽  
Dan-Qing Song ◽  
Chang-Qin Hu
2017 ◽  
Vol 63 (No. 5) ◽  
pp. 226-230 ◽  
Author(s):  
Zbíral Jiří ◽  
Čižmár David ◽  
Malý Stanislav ◽  
Obdržálková Elena

Determining and characterizing soil organic matter (SOM) cheaply and reliably can help to support decisions concerning sustainable land management and climate policy. Glomalin was recommended as one of possible indicators of SOM quality. Extracting glomalin from and determining it in soils using classical chemical methods is too complicated and therefore near-infrared spectroscopy (NIRS) was studied as a method of choice for the determination of glomalin. Representative sets of 84 different soil samples from arable land and grasslands and 75 forest soils were used to develop NIRS calibration models. The parameters of the NIRS calibration model (R = 0.90 for soils from arable land and grasslands and R = 0.94 for forest soils) proved that glomalin can be determined in air-dried soils by NIRS with adequate trueness and precision simultaneously with determination of nitrogen and oxidizable carbon.


1994 ◽  
Vol 2 (1) ◽  
pp. 49-57 ◽  
Author(s):  
James B. Reeves

The objective of this work was to explore the relative value of near- and mid-infrared diffused reflectance spectroscopy in determining the composition of forages and by-products. Sixty-seven samples consisting of 15 alfalfa, 16 tall fescue and 15 orchard grass hays, 10 corn stovers and 11 wheat straws at various stages of maturity were examined by diffuse reflectance using a scanning monochromator (1100–2500 nm), a Fourier near infrared spectrometer (10,000–4000 cm−1, 4 and 16 cm−1 resolution, neat and 5% sample in KBr) and a Fourier mid-infrared spectrometer (4000–400 cm−1, 4 and 16 cm−1 resolution, neat and 5% sample in KBr). Samples were analysed chemically and spectroscopically for fibres, in vitro digestibility, crude protein, nitrobenzene oxidation products and various measures of lignin content. The results showed that diffuse mid-infrared reflectance spectroscopy can perform as well as, and sometimes better than, diffuse near infrared spectroscopy in determining the composition of forages and by-products. In addition, Fourier near infrared spectroscopy did not perform as well as either near infrared using a scanning monochromator or the Fourier mid-infrared spectrometer. Finally, diluting samples with KBr was not beneficial for either Fourier based determinations. Additional work with more diverse data sets and various Fourier instrument configurations will be needed to further define the limits and usefulness of Fourier transform near- and mid-infrared spectroscopy in the determination of forage and by-product composition.


2008 ◽  
Vol 80 (19) ◽  
pp. 7257-7265 ◽  
Author(s):  
Javier Moros ◽  
Nieves Galipienso ◽  
Rocío Vilches ◽  
Salvador Garrigues ◽  
Miguel de la Guardia

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