scholarly journals Identification and Comparative Determination of Senkyunolide A in Traditional Chinese Medicinal Plants Ligusticum chuanxiong and Angelica sinensis by HPLC Coupled with DAD and ESI-MS

2005 ◽  
Vol 53 (11) ◽  
pp. 1480-1483 ◽  
Author(s):  
Tao Yi ◽  
Kelvin Sze-Yin Leung ◽  
Guang-Hua Lu ◽  
Hao Zhang ◽  
Kelvin Chan
Molecules ◽  
2020 ◽  
Vol 25 (15) ◽  
pp. 3356
Author(s):  
Hongwei Wu ◽  
Qianqian Huang ◽  
Shujun Chao ◽  
Jie Yu ◽  
Shengrui Xu ◽  
...  

Hydrophilic ionic liquids are often used to extract the active ingredients of medicinal plants, while hydrophobic ionic liquids are rarely used to directly extract solid samples. In this paper, a simple, novel and efficient temperature-controlled hydrophobic ionic liquids-based ultrasound/heating-assisted extraction (TC-ILs-UHAE) procedure coupled with high-performance liquid chromatography (HPLC) was developed and applied to the determination of ferulic acid (FA) in Chinese herbal medicine Angelica sinensis. During the extraction procedure, hydrophobic ionic liquids (ILs) were dispersed into water to form cloudy solution (fine droplets) with the aid of ultrasound and heating simultaneous. After extraction, phase separation was easily achieved by centrifuging at 0 °C. Among all ILs used, 1-butyl-3-methylimidazolium bis(trifluoromethanesulphonyl)imide ([C4mim]NTf2) exhibited the highest extraction ability and the possible extraction mechanism was discussed. Additionally, the synergistic effect of heating and ultrasound on the extraction efficiency was investigated. Under the optimized conditions, a good linearity was observed with correlation coefficient (r) of 0.9995. The limit of detection of FA (LOD, S/N = 3) was 9.6 µg/L and the spiked recoveries of FA for real samples were in the range of 91.67 to 102.00% with relative standard deviation (RSD) lower than 3.87%. Compared with the traditional extraction methods, the proposed method gave the highest yield of FA and had the shortest extraction time. Therefore, this method is a potential simple, green and highly efficient technique and expected to be applied to the extraction of other bioactive ingredients in medicinal plants.


2011 ◽  
Vol 28 (7) ◽  
pp. 885-893 ◽  
Author(s):  
Xiaofei Zhang ◽  
Wenkun Liu ◽  
Antonio F. Logrieco ◽  
Meihua Yang ◽  
Zhen Ou-yang ◽  
...  

2010 ◽  
Vol 27 (7) ◽  
pp. 989-997 ◽  
Author(s):  
Lei Yang ◽  
Linan Wang ◽  
Jianyu Pan ◽  
Lan Xiang ◽  
Meihua Yang ◽  
...  

2013 ◽  
Vol 9 (36) ◽  
pp. 19 ◽  
Author(s):  
Yong Zhang ◽  
Kunpeng Xue ◽  
EugeneYuexing Zhao ◽  
Yin Li ◽  
Lixin Yao ◽  
...  

2020 ◽  
Vol 2020 ◽  
Author(s):  
Firew Admasu

Abstract: The study were conducted at Dilla University, College of Natural Sciences, Biological Sciences laboratories. Background: Ethiopia is a country with many ethnic groups, cultures and beliefs which in turn have contributed to the high diversity of traditional health care knowledge and practices of traditional medicine from local growth plants, animals and minerals for various physical and mental disorders of human and livestock population that passed from generation to generation for centuries. Medicinal plants contributors to pharmaceutical, agricultural and food industries in the world. The use of medicinal plants in the industrialized societies has been traced to extraction and development of several drugs used in order to heel some diseases having inhibiting effect against pathogenic microorganism. Objective: The main objective of this study was Extraction and Phytochemicals determination of traditional medicinal plants for anti microbial susceptibility test. Methodology: The extraction and identification of some phytochemicals crude compound which used for antimicrobial susceptibility test from plant sample such as Ocimum lamiifolium (OL), Croton maerosth (Cm) and Ruta chalepesis (RC) were conducted. Plant samples are collected, powdered using mortal and pistil and extracted using ethanol and some susceptibility tests were performed to identify some phytochemicals compound. Result: The main result of Antimicrobial activity test showed that the crude extract of OL has the highest zone of inhibition. The highest yield of crude extract (38.21%) was obtained from Croton maerosth (CM) which followed by Ruta chalepesis (RC) (32.43%). However, the lowest yield (28.37%) was obtained from Oscpmum lamifolium (OL). Conclusion: Traditional Medicine is used by many people to managing numerous conditions; it’s accessible and effective on antimicrobial activity. Therefore, it plays a significant role by reducing life-threatening ailments of people and other animals.


Sign in / Sign up

Export Citation Format

Share Document