scholarly journals Application of fluorescent triazoles to analytical chemistry. I. Determination of aromatic primary amine with 2,4,6-triaminopyrimidine as a reagent.

1985 ◽  
Vol 33 (11) ◽  
pp. 4928-4934 ◽  
Author(s):  
SHIGERU NARITA ◽  
TAKAYASU KITAGAWA ◽  
EIZO HIRAI
Keyword(s):  
Analytical Chemistry ◽  
Primary Amine ◽  
Aromatic Primary Amine

Green synthesis of gold nanoparticles and its application for the trace level determination of painter's colic

RSC Advances ◽  
2015 ◽  
Vol 5 (21) ◽  
pp. 16284-16291 ◽  
Author(s):  
Chelladurai Karuppiah ◽  
Selvakumar Palanisamy ◽  
Shen-Ming Chen ◽  
R. Emmanuel ◽  
K. Muthupandi ◽  
...  
Keyword(s):  
Analytical Chemistry ◽  
Heavy Metal ◽  
Green Synthesis ◽  
Metal Ion ◽  
Trace Level ◽  
Ion Sensing ◽  
Metal Ion Sensing ◽  
Heavy Metal Ion Sensing ◽  
Trace Level Determination

The green synthesis of metal nanoparticles is found to be more attractive in various disciplines, including in analytical chemistry for heavy metal ion sensing.

scholarly journals NEW, GREEN AND MINIATURIZED ANALYTICAL METHOD FOR DETERMINATION OF CEFADROXIL MONOHYDRATE IN CAPSULES

2019 ◽  
Vol 3 (1) ◽  
pp. 23-28 ◽  
Author(s):  
Bianca Marco ◽  
Ana Kogawa ◽  
Hérida Salgado
Keyword(s):  
Analytical Chemistry ◽  
Standard Sample ◽  
Low Cost ◽  
Visible Region ◽  
Hplc Method ◽  
Minimal Amount ◽  
Green Analytical Chemistry ◽  
Color Reagent ◽  
Routine Quality Control

Cefadroxil, an oral antimicrobial, presents few techniques optimized for the reduction of solvents and toxic residues and/or non-use of them. So, a quantitative, new and miniaturized method for determination of cefadroxil monohydrate in capsules has been developed and validated by spectrophotometric method in the visible region according to the international guidelines. The analyzes were performed using microplates containing 96 wells, 1 % of phenolphthalein and sodium hydroxide 0.1 M as reagent at 552 nm. The method was (i) linear in the range of 15-115 µg mL-1, (ii) selective when comparing standard, sample, adjuvants and color reagent, (iii) precise with deviations below 4 %, (iv) accurate when comparing the proposed method with the HPLC method, (v) robusts by making small and deliberate modifications to the method, (vi) besides being fast, low cost, eco-friendly and generates minimal amount of waste. The method can be applied to the routine quality control of cefadroxil monohydrate in capsules and an effective and accessible alternative that contemplates the concepts of current and sustainable green analytical chemistry.

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