Isotope Ratio Analysis of Individual Plutonium and Uranium–Plutonium Mixed Oxide Particles by Thermal Ionization Mass Spectrometry with a Continuous Heating Method

2012 ◽  
Vol 41 (1) ◽  
pp. 90-91 ◽  
Author(s):  
Daisuke Suzuki ◽  
Yoko Saito-Kokubu ◽  
Chi-Gyu Lee ◽  
Fumitaka Esaka ◽  
Masaaki Magara ◽  
...  
Keyword(s):  
Isotope Ratio ◽  
Thermal Ionization Mass Spectrometry ◽  
Continuous Heating ◽  
Ionization Mass ◽  
Ratio Analysis ◽  
Heating Method ◽  
Isotope Ratio Analysis ◽  
Oxide Particles ◽  
Thermal Ionization Mass ◽  
Uranium Plutonium

scholarly journals Feasibility Study of Isotope Ratio Analysis of Individual Uranium-Plutonium Mixed Oxide Particles with SIMS and ICP-MS

2011 ◽  
Vol 2 (4) ◽  
pp. 80-83 ◽  
Author(s):  
Fumitaka Esaka ◽  
Masaaki Magara ◽  
Daisuke Suzuki ◽  
Yutaka Miyamoto ◽  
Chi-Gyu Lee ◽  
...  
Keyword(s):  
Feasibility Study ◽  
Mixed Oxide ◽  
Isotope Ratio ◽  
Ratio Analysis ◽  
Icp Ms ◽  
Isotope Ratio Analysis ◽  
Oxide Particles ◽  
Uranium Plutonium

High Precision Pb Isotope Determination by Using 207Pb-204Pb Double Spike Revisited

2012 ◽  
Vol 518-523 ◽  
pp. 1669-1676 ◽  
Author(s):  
Xi Jun Liu ◽  
Shuai Liao
Keyword(s):  
Thermal Ionization Mass Spectrometry ◽  
Isotopic Analysis ◽  
Ionization Mass ◽  
Ratio Analysis ◽  
Pb Isotope ◽  
Mass Fractionation ◽  
Isotope Ratio Analysis ◽  
Isotope Determination ◽  
Thermal Ionization Mass ◽  
Isotope Analyses

A method for getting high quality Pb isotope ratio analysis using207Pb-204Pb double spike method has been developed at Scripps Institution of Oceanography (SIO), which corrected the mass fractionation effects during small amount Pb loading isotopic analysis by thermal ionization mass spectrometry (TIMS), with the minimum amount of 8×10-9g Pb per load. The double spike method effectively improves in both precision and accuracy without recourse to excessively rigorous loading or run conditions. Over a period of fifteen months accuracy double spike tested for Pb standard SRM981 in SIO isotope laboratory, an external precision of ±0.0038、±0.0040、±0.0122 (2σ, n=53) was obtained for206Pb/204Pb,207Pb/204Pb and208Pb/204Pb rations, although the small amount Pb loading, which present a same excellent accuracy and external precision as other laboratories reported. Therefore, this method is superior to precise and accurate isotope analyses of low level Pb concentration geological and environmental samples, and will be a highly powerful tool in the future of earth sciences and environmental sciences.

scholarly journals Application of automated particle screening for effective analysis of individual uranium particles by thermal ionization mass spectrometry

2016 ◽  
Vol 8 (7) ◽  
pp. 1543-1548 ◽  
Author(s):  
Fumitaka Esaka ◽  
Daisuke Suzuki ◽  
Takumi Yomogida ◽  
Masaaki Magara
Keyword(s):  
Mass Spectrometry ◽  
Thermal Ionization Mass Spectrometry ◽  
Thermal Ionization ◽  
Ionization Mass Spectrometry ◽  
Ionization Mass ◽  
Ratio Analysis ◽  
Isotope Ratio Analysis ◽  
Thermal Ionization Mass ◽  
Effective Analysis ◽  
Particle Screening

Automated particle screening was combined with isotope ratio analysis of individual uranium particles using thermal ionization mass spectrometry.

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