Synthesis and Characterization of S-Doped TiO2Made by Anodic Oxidation of Titanium in Sulfuric Acid

2007 ◽  
Vol 36 (11) ◽  
pp. 1318-1319 ◽  
Author(s):  
Atsushi Nakahira ◽  
Koji Yokota ◽  
Takashi Kubo ◽  
Masahide Takahashi
Keyword(s):  
Sulfuric Acid ◽  
Anodic Oxidation ◽  
Synthesis And Characterization

scholarly journals Synthesis and Characterization of TiO2 Doped with P Ions by Anodic Oxidation of Titanium in Acid Solution

2006 ◽  
Vol 114 (1325) ◽  
pp. 46-50 ◽  
Author(s):  
Atsushi NAKAHIRA ◽  
Koichi KONISHI ◽  
Koji YOKOTA ◽  
Tetsuo HONMA ◽  
Hirofumi ARITANI ◽  
...  
Keyword(s):  
Acid Solution ◽  
Anodic Oxidation ◽  
Synthesis And Characterization

scholarly journals Synthesis and characterization of Taurine

2014 ◽  
Vol 14 ◽  
pp. 57-60
Author(s):  
B Bayarmaa ◽  
D Otgonsuren ◽  
P Odonmajig
Keyword(s):  
Sulfuric Acid ◽  
Laboratory Condition ◽  
1H Nmr ◽  
Intermediate Product ◽  
Sodium Sulfite ◽  
Synthesis And Characterization ◽  
Second Step ◽  
Ms Analysis

Have been obtained 2-aminoethanesulfonic acid (taurine) from ethanolamine, sulfuric acid and sodium sulfite during the synthesis in laboratory condition. The process involves two steps of reactions, the first was esterification of ethanolamine with sulfuric acid to produce the intermediate product of 2-aminoethyl ester which than was extended to the second step by sulfonation with sodium sulfite to produce 2-aminoethanesulfonic acid. Resulting product was analyzed using 1H-NMR, IR, FAB-MS analysis and examined purity characterizations of the synthesized products. DOI: http://dx.doi.org/10.5564/mjc.v14i0.200 Mongolian Journal of Chemistry 14 (40), 2013, p57-60

scholarly journals Synthesis and Characterization of New Thioxanthone Derivatives

2013 ◽  
Vol 10 (3) ◽  
pp. 724-735
Author(s):  
Baghdad Science Journal
Keyword(s):  
Sulfuric Acid ◽  
Benzoic Acid ◽  
Sodium Azide ◽  
Aromatic Amines ◽  
Chlorosulfonic Acid ◽  
Starting Material ◽  
Phosphorus Compounds ◽  
Synthesis And Characterization

This work comprises the synthesis of new thioxanthone derivatives containing C-substituted thioxanthone. To obtain these derivatives, the o-mercapto benzoic acid was chosen as the starting material, which was reacted with dry benzene in sulfuric acid (98 %) to produce the thioxanthone (1). The 2,7-(disulfonyl phosphine imine) thioxanthone (4-8) were prepared from reaction of compound (1) with chlorosulfonic acid gave 2,7-(disulfonyl chloride) thioxanthone (2). Treatment of (2) with sodium azide to produce 2,7-(disulfonyl azide) thioxanthone (3). Condensation of (3) with phosphorus compounds afforded compounds (4-8). The 2,7-(disulfonamide) thioxanthone (9-21) was obtained when compound (2) condensed with different aromatic amines, it gave the expected amides (9-21).

Synthesis and Characterization of Rutile TiO2 Powder by the Sulfuric Acid Method

2012 ◽  
Vol 50 (7) ◽  
pp. 523-530 ◽  
Author(s):  
Sung Hwan Lim ◽  
Soon Ok Choi ◽  
Jee Hee Cho ◽  
Won Yon Kim
Keyword(s):  
Sulfuric Acid ◽  
Synthesis And Characterization ◽  
Tio2 Powder ◽  
Rutile Tio2 ◽  
Acid Method ◽  
Sulfuric Acid Method

scholarly journals Synthesis and Characterization of Fe Nanofiber using Alumina with Nanoholes by Anodic Oxidation

2007 ◽  
Vol 115 (1348) ◽  
pp. 905-908 ◽  
Author(s):  
Astushi NAKAHIRA ◽  
Kouji YOKOTA ◽  
Seiichi KATO ◽  
Noriyuki HIROTA ◽  
Hidehiko OKADA ◽  
...  
Keyword(s):  
Anodic Oxidation ◽  
Synthesis And Characterization

scholarly journals Sintesis dan Karakterisasi Selulosa Asetat (CA)

2018 ◽  
Vol 5 (2) ◽  
pp. 58-62
Author(s):  
Fensia Analda Souhoka ◽  
Jolantje Latupeirissa
Keyword(s):  
Acetic Acid ◽  
Sulfuric Acid ◽  
Cellulose Acetate ◽  
Acid Anhydride ◽  
Degree Of Substitution ◽  
Synthesis And Characterization ◽  
Cellulose Content

Synthesis and characterization of cellulose acetate (CA) has been conducted. The cellulose used in this study was commecial a-cellulose in 92% content. All the CA products were analyzed by FTIR spectrometers. The determination of cellulose content was done using standart method of TAPPI T-203, while the determination of the degree of substitution (DS) was based on SNI 0444:2009 method. Conventional acetylation of cellulose was performed using gacial acetic acid, anhydride acetic acid, and sulfuric acid. The acetylation at 25 °C for 2.5 hours gave the DS of 1.482 and at 40 °C for 5 hours gave the higher DS 2.295.

Sign in / Sign up

Export Citation Format

Share Document