X-ray and SEM Observations of Smectic A Phase and Dried Gel Fibers Formed in a Fine Capillary

2005 ◽  
Vol 34 (12) ◽  
pp. 1650-1651 ◽  
Author(s):  
Yuki Morita ◽  
Kosuke Kawabe ◽  
Fusheng Zhang ◽  
Hiroaki Okamoto ◽  
Shunsuke Takenaka ◽  
...  
1998 ◽  
Vol 10 (1) ◽  
pp. 147-153 ◽  
Author(s):  
M Tanaka ◽  
M Konda ◽  
M Miyamoto ◽  
Y Kimura ◽  
A Yamaguchi

Anomalous solid structures formed by a thermotropic liquid crystalline polyimide (PI-LC) were investigated by thermal analysis, polarized light microscopy and x-ray analysis. It was revealed that PI-LC should undergo a phase transition from the crystalline to the isotropic phase through the smectic or nematic phase in the temperature range 277–300 °C. The PI-LC filament extruded at 280 °C, at which temperature the polymer was in liquid crystalline phase, was formed to have a structure similar to the smectic C phase, while that extruded and melt-drawn at 310 °C, at which temperature the polymer was in the isotropic phase, had a structure similar to the smectic A phase.


1988 ◽  
Vol 105 (2) ◽  
pp. K107-K110 ◽  
Author(s):  
B. Pura ◽  
J. Przedmojski ◽  
K. Wentowska ◽  
R. D??browski ◽  
K. Czupryński

Author(s):  
B. I. Ostrovskii ◽  
M. A. Saidachmetov
Keyword(s):  
X Ray ◽  

1987 ◽  
Vol 149 (1) ◽  
pp. 49-60 ◽  
Author(s):  
Hirofumi Sakashita ◽  
Shigeki Komori ◽  
Kazuya Kazuya Kamon ◽  
Hikaru Terauchi ◽  
Yo Shimizu ◽  
...  

2007 ◽  
Vol 15 (1) ◽  
Author(s):  
R. Dąbrowski ◽  
W. Drzewiński ◽  
J. Dziaduszek ◽  
J. Gąsowska ◽  
P. Henderson ◽  
...  

AbstractThree homologous series of orthoconic (45 degree tilt) antiferroelectric liquid crystals containing either naphthyl or terphenyl groups as mesogenic unit have been synthesized and their mesomorphic behaviour investigated by DSC and polarized light microscopy, and their properties discussed. X-ray diffraction studies have shown the presence of a de Vries-type smectic A phase which does not exhibit a layer shrinkage on transition to the ferroelectric smectic C phase. Mixtures of the new materials have been formulated and their electro-optical properties investigated for their use in surface stabilized orthoconic antiferroelectric liquid crystal (SSOAFLC) devices


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