Large-scale Synthesis of Crystalline Tellurium Nanowires with Controlled-Diameters via a Hydrothermal-reduction Process

2004 ◽  
Vol 33 (5) ◽  
pp. 592-593 ◽  
Author(s):  
Liqiang Xu ◽  
Yanwei Ding ◽  
Guangcheng Xi ◽  
Wanqun Zhang ◽  
Yiya Peng ◽  
...  
Keyword(s):  
Large Scale ◽  
Reduction Process ◽  
Large Scale Synthesis ◽  
Tellurium Nanowires ◽  
Hydrothermal Reduction

Large-scale synthesis of high-content Fe nanotubes/nanorings with high magnetization by H2 reduction process

2013 ◽  
Vol 48 (12) ◽  
pp. 5003-5007 ◽  
Author(s):  
Xiaoli Liu ◽  
Minrui Zheng ◽  
Yunbo Lv ◽  
Jie Fang ◽  
Chorng Haur Sow ◽  
...  
Keyword(s):  
Large Scale ◽  
Reduction Process ◽  
Large Scale Synthesis

scholarly journals Catalytic reduction of dimeric acetylated 2-deoxy-2-nitroso-α-D-glycopyranosyl chlorides

1980 ◽  
Vol 58 (23) ◽  
pp. 2720-2723 ◽  
Author(s):  
T. L. Nagabhushan
Keyword(s):  
Large Scale ◽  
Catalytic Reduction ◽  
Reduction Process ◽  
Platinum Oxide ◽  
Large Scale Synthesis

Reduction of tri-O-acetyl-2-deoxy-2-nitroso-α-D-glucopyranosyl chloride dimer with hydrogen and platinum oxide in the presence of methanol or ethanol afforded the corresponding alkyl tri-O-acetyl-2-amino-2-deoxy-β-D-glucopyranoside hydrochloride. In the absence of an alcohol the product was tri-O-acetyl-2-amino-1,5-anhydro-2-deoxy-D-glucitol hydrochloride. The glycosylation/reduction process gave similar results with the galacto isomer.A method is described for the ready and large-scale synthesis of D-galactosamine hydrochloride.

Large-Scale Synthesis of Carbon Nanotubes by an Ethanol Thermal Reduction Process

2003 ◽  
Vol 125 (27) ◽  
pp. 8088-8089 ◽  
Author(s):  
Jianwei Liu ◽  
Mingwang Shao ◽  
Xiangying Chen ◽  
Weichao Yu ◽  
Xianming Liu ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Large Scale ◽  
Reduction Process ◽  
Thermal Reduction ◽  
Large Scale Synthesis ◽  
Synthesis Of Carbon Nanotubes

Exogenous Directing Group Free, Ligand-Enabled gamma-C(sp3)–H Arylation of Free Primary Aliphatic Amines and α-Amino Esters

2019 ◽  
Author(s):  
Yongzheng Ding ◽  
Shuai Fan ◽  
Xiaoxi Chen ◽  
yuzhen gao ◽  
Gang Li
Keyword(s):  
Amino Acids ◽  
Large Scale ◽  
Free Ligand ◽  
Aliphatic Amines ◽  
Rapid Synthesis ◽  
Amino Esters ◽  
Directing Group ◽  
Large Scale Synthesis ◽  
Primary Aliphatic Amines

A Pdᴵᴵ-catalyzed, ligand-enabled gamma-C(sp3)–H arylation of free primary aliphatic amines and amino esters without using an exogenous directing group is reported. This reaction is compatible with unhindered free aliphatic amines, and it is also be applicable to the rapid synthesis of biologically and synthetically valuable unnatural α-amino acids. Large scale synthesis is also feasible using this method.<br>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

Improved and Large-Scale Synthesis of N-methyl-D-aspartic Acid

2015 ◽  
Vol 12 (2) ◽  
pp. 197-201 ◽  
Author(s):  
Liang Xi ◽  
Di Wu ◽  
Hong-You Zhu ◽  
Cong-Hai Zhang ◽  
Yi Jin ◽  
...  
Keyword(s):  
Aspartic Acid ◽  
Large Scale ◽  
Large Scale Synthesis

Large-scale synthesis of copper nanoparticles by chemically controlled reduction for applications of inkjet-printed electronics

2008 ◽  
Vol 19 (41) ◽  
pp. 415604 ◽  
Author(s):  
Youngil Lee ◽  
Jun-rak Choi ◽  
Kwi Jong Lee ◽  
Nathan E Stott ◽  
Donghoon Kim
Keyword(s):  
Copper Nanoparticles ◽  
Large Scale ◽  
Printed Electronics ◽  
Large Scale Synthesis

Large-scale synthesis of ionic liquid [BMIM]Br in a microbore tube

2021 ◽  
Author(s):  
Nirvik Sen ◽  
Sameer Ekhande ◽  
K.K. Singh ◽  
S. Mukhopadhyay ◽  
R.S. Sirsam ◽  
...  
Keyword(s):  
Ionic Liquid ◽  
Large Scale ◽  
Large Scale Synthesis
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