A NEW SYNTHESIS OF β NITRO CARBONYL COMPOUNDS FROM ALKYL VINYL KETONES WITH SODIUM NITRITE-ACETIC ACID IN TETRAHYDROFURAN

1981 ◽  
Vol 10 (12) ◽  
pp. 1677-1678 ◽  
Author(s):  
Tetuo Miyakoshi ◽  
Shojiro Saito ◽  
Ju Kumanotani
Keyword(s):  
Acetic Acid ◽  
Sodium Nitrite ◽  
Carbonyl Compounds ◽  
New Synthesis

scholarly journals Oxidation of Aliphatic Secondary and Benzylic Alcohols to Carbonyl Compounds by Peracetic Acid in the Presence of Sodium Bromide in Acetic Acid

1987 ◽  
Vol 60 (11) ◽  
pp. 4143-4144 ◽  
Author(s):  
Takashi Morimoto ◽  
Masao Hirano ◽  
Hiroyuki Ashiya ◽  
Hidetaka Egashira ◽  
Xiumin Zhuang
Keyword(s):  
Acetic Acid ◽  
Peracetic Acid ◽  
Carbonyl Compounds ◽  
Sodium Bromide ◽  
Benzylic Alcohols

scholarly journals Determination of Diethanolamine in Shampoo Products Containing Fatty Acid Diethanolamides by Liquid Chromatography with a Thermal Energy Analyzer

2005 ◽  
Vol 88 (2) ◽  
pp. 592-594 ◽  
Author(s):  
Hardy J Chou
Keyword(s):  
Acetic Acid ◽  
Liquid Chromatography ◽  
Fatty Acid ◽  
Thermal Energy ◽  
Sodium Nitrite ◽  
Room Temperature ◽  
Energy Analyzer

Abstract A liquid chromatography (LC) method using a thermal energy analyzer (TEA) is described for the determination of diethanolamine (DEA) in shampoo products containing fatty acid diethanolamides. DEA was converted to N-nitrosodiethanolamine (NDELA) by dissolving a portion of the product in 6M acetic acid and mixing with sodium nitrite for 1 h at room temperature. The reaction mixture was dried, dissolved in acetone, and analyzed for NDELA by LC-TEA. The recovery of DEA from 2 shampoo products at fortification levels of 25, 250, and 1000 ppm ranged from 70 to 105%. Twenty shampoo products were analyzed by this method, and 19 were found to contain DEA at levels ranging from 140 to 15 200 ppm.

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