scholarly journals The Synthesis of Crystalline Zirconium Phosphate with Large Particle Size by the Direct-precipitation Method

1979 ◽  
Vol 52 (12) ◽  
pp. 3528-3531 ◽  
Author(s):  
Yasushi Inoue ◽  
Yoshimune Yamada
2018 ◽  
Vol 32 (19) ◽  
pp. 1850215
Author(s):  
Yu-Shan Qin ◽  
Qi Shi ◽  
Yu-Guang Lv ◽  
Chen-Xi Shi ◽  
Ya-Xin Zhao ◽  
...  

In this paper, Ag–Ce–ZnO nanocomposites with average particle size of about 50 nm were prepared by direct precipitation method. In order to solve the problem of agglomeration, the nanocomposites with the average particle size of about 30 nm were obtained by treating the nanocomposites with surfactant sodium polyacrylate (PAAS). The effect of surfactant PAAS on the content of hydroxyl radicals produced by nanocomposites was determined by UV spectrophotometry and fluorescence spectrophotometry, and the effect of PAAS on the dispersion effect was obtained indirectly. The experimental results showed that the addition of surfactants’ PAAS effectively reduced the average particle size of nanocomposites, increased the content of hydroxyl radicals, and made the nanocomposites have good dispersing effect.


1939 ◽  
Vol 31 (12) ◽  
pp. 1509-1512 ◽  
Author(s):  
J. McGavack

2010 ◽  
Vol 113-116 ◽  
pp. 1770-1773 ◽  
Author(s):  
Xi Hua Zhao ◽  
Min Xu

Cu(OH)2 precursor was synthesized by direct precipitation method and CuSO4 and NaOH were used as raw materials. Then, Cu(OH)2 precursor was calcined in muffle furnace at 400°C for 2h in order that CuO particle was obtained. Through the analysis of the factors affecting the CuO, the paper determined the optimum conditions for the synthesis of nano-CuO with the direct-precipitation method. Then the paper analyzed phase composition and crystal structure of samples using XRD and calculated the average grain size of samples by Scherrer formula, and observed and analyzed by TEM to characterize the morphology and particle size of samples. The optimum precipitation conditions are as follows: when the precipitation agent is 3.2:1, reaction time 40min and precipitant concentration 0.6mol.L-1. The average size of CuO particle prepared under the conditions is 18nm and the yield is 96%.


RSC Advances ◽  
2015 ◽  
Vol 5 (20) ◽  
pp. 15198-15204 ◽  
Author(s):  
R. R. Ozer ◽  
J. P. Hinestroza

A series of isoreticular lanthanide metal–organic frameworks, Ln-MOFs (Ln = Eu, Gd, and Tb), were directly grown on cotton fibers using a room temperature water-based direct precipitation method.


2013 ◽  
Vol 666 ◽  
pp. 93-102 ◽  
Author(s):  
Chang Jun Li ◽  
Zhi Wei Huang ◽  
Yu Jie He ◽  
Dong Zhou ◽  
Cheng Du ◽  
...  

An direct precipitation method of Calcium glyceroxide Ca(C3H7O3)2 was proposed. The prepared Ca(C3H7O3)2 was effective in transesterification of Jatropha oil into fatty acid methyl esters (FAME). The Ca(C3H7O3)2 catalysts were characterized by using XRD, solid state 13C-NMR, FTIR, and Hammett indicator. The influence of various reaction variables on the conversion was investigated. Under a condition of methanol/oil molar ratio of 9:1, a catalyst amount of 4 wt %, reaction time of 1.5 h, and reaction temperature of 65 °C, over 95% of biodiesel yield was obtained.


Fuel ◽  
2021 ◽  
Vol 289 ◽  
pp. 119838
Author(s):  
Xiaogang Mu ◽  
Jinfang Liu ◽  
Fei Gao ◽  
Cunbao Deng ◽  
Zhixin Jin ◽  
...  

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