scholarly journals An Adiabatic Calorimeter for High-resolution Heat Capacity Measurements in the Temperature Range from 12 to 300 K

1975 ◽  
Vol 48 (11) ◽  
pp. 3060-3066 ◽  
Author(s):  
Masami Tatsumi ◽  
Takasuke Matsuo ◽  
Hiroshi Suga ◽  
Syûzô Seki
1988 ◽  
Vol 123 ◽  
pp. 105-111 ◽  
Author(s):  
Tan Zhicheng ◽  
Yin Anxue ◽  
Chen Shuxia ◽  
Zhou Lixing ◽  
Li Fuxue ◽  
...  

2000 ◽  
Vol 352-353 ◽  
pp. 247-253 ◽  
Author(s):  
Zhi-Cheng Tan ◽  
Guang-Yu Sun ◽  
Yong-Ji Song ◽  
Lan Wang ◽  
Jian-Ru Han ◽  
...  

2014 ◽  
Vol 525 ◽  
pp. 141-145
Author(s):  
Qing Fen Meng ◽  
Xiao San Xia

A new complex [Na (H2O)2]6[MoCo6O12(H2O)12]·4.3H2O(s) was synthesized and determined by X-ray crystallography. Low-temperature heat capacities of the compound was measured by a precision automated adiabatic calorimeter over the temperature range from 78 to 380 K. An obvious dehydration process was found in the heat capacity curve of the title compound. The temperature, enthalpy and entropy of the dehydration process were determined to be (370.266±0.292) K, (187.455±0.354) kJ·mol-1, (50.627±0.078) J·K-1·mol-1 by three series of repeated heat capacity measurements in the region of thermal decomposition.


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