scholarly journals Ultrasonic welding of epoxy- to polyetheretherketone- based composites: Investigation on the material of the energy director and the thickness of the coupling layer

2020 ◽  
Vol 54 (22) ◽  
pp. 3081-3098 ◽  
Author(s):  
Eirini Tsiangou ◽  
Sofia Teixeira de Freitas ◽  
Irene Fernandez Villegas ◽  
Rinze Benedictus

Ultrasonic welding is a highly promising technique for joining thermoplastic to thermoset composites. A neat thermoplastic coupling layer is co-cured on the surface to be welded to make the thermoset composite ‘weldable’. A reliable bond is attained when miscible thermoplastic and thermoset materials are chosen. For welding carbon fibre/polyetheretherketone (PEEK) to thermoset composite samples, a PEEK film is not preferable due to its immiscibility with epoxy resins. On the other hand, polyetherimide is an excellent candidate, since it is known to be miscible to most epoxy systems at high temperatures and PEEK polymers. This study focusses on two main subjects; firstly, the nature of the material of the energy director, i.e. a flat thermoplastic film used to promote heat generation at the interface. In this case, the energy director can be either polyetherimide, as in the coupling layer or PEEK material, as in the matrix of the thermoplastic composite adherend. It was found that both materials can produce welds with similar mechanical performance. This study focusses secondly on the thickness of the coupling layer. Due to the high melting temperature of the PEEK matrix, a 60-µm-thick coupling layer was seemingly too thin to act as a thermal barrier for the epoxy resin for heating times long enough to produce fully welded joints. Such an issue was found to be overcome by increasing the thickness of the coupling layer to 250 µm, which resulted in high-strength welds.

2007 ◽  
Vol 353-358 ◽  
pp. 2007-2010 ◽  
Author(s):  
Jiu Chun Yan ◽  
Xiao Lin Wang ◽  
Rui Qi Li ◽  
Hui Bin Xu ◽  
Shi Qin Yang

The ultrasonic welding process of thermoplastic composite with different shapes of energy director (ED) was simulated using finite element model. The results show that the highest temperature zone locates at the tip for the semicircular and triangular ones, and locates at the middle height for the trapezoid one. But it does not locate at the body of ED for the rectangular one. Energy director with different shapes lead to the temperature rising rate at different order of amplitude. The welding amplitude has same influence on the four shapes of ED. The temperature distributing profiles of semicircular, triangular and trapezoid ED keep constant from the initial welding time to that when the highest temperature on joints arrives the temperature of glass transformation (Tg), but the profile for rectangular ED changes greatly.


Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 473
Author(s):  
Tamer A. Sebaey ◽  
Mohamed Bouhrara ◽  
Noel O’Dowd

Automated Tape Placement (ATP) technology is one of the processes that is used for the production of the thermoplastic composite materials. The ATP process is complex, requiring multiple melting/crystallization cycles. In the current paper, laser-assisted ATP was used to manufacture two thermoplastic composites (IM7/PEEK and AS4/PA12). Those specimens were compared to specimens that were made of thermoset polymeric composites (IM7/8552) manufactured while using a standard autoclave cycle. In order assess the quality, void content, fibre distribution, and fibre misalignment were measured. After manufacturing, specimens from the three materials were assessed using optical microscopy and computed tomography (CT) scans. The results showed that, as compared to the thermoset composites, thermoplastics that are manufactured by the ATP have a higher amount of voids. On the other hand, manufacturing using the ATP showed an improvement in both the fibre distribution inside the matrix and the fibre misalignment.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Tsuyoshi Okumura ◽  
Riku Takahashi ◽  
Katsumi Hagita ◽  
Daniel R. King ◽  
Jian Ping Gong

AbstractWe propose a new concept that utilizes the difference in Poisson's ratio between component materials as a strengthening mechanism that increases the effectiveness of the sacrificial bond toughening mechanism in macroscale double-network (Macro-DN) materials. These Macro-DN composites consist of a macroscopic skeleton imbedded within a soft elastic matrix. We varied the Poisson's ratio of the reinforcing skeleton by introducing auxetic or honeycomb functional structures that results in Poisson’s ratio mismatch between the skeleton and matrix. During uniaxial tensile experiments, high strength and toughness were achieved due to two events: (1) multiple internal bond fractures of the skeleton (like sacrificial bonds in classic DN gels) and (2) significant, biaxial deformation of the matrix imposed by the functional skeleton. The Macro-DN composite with auxetic skeleton exhibits up to 4.2 times higher stiffness and 4.4 times higher yield force than the sum of the component materials. The significant improvement in mechanical performance is correlated to the large mismatch in Poisson's ratio between component materials, and the enhancement is especially noticeable in the low-stretch regime. The strengthening mechanism reported here based on Poisson's ratio mismatch can be widely used for soft materials regardless of chemical composition and will improve the mechanical properties of elastomer and hydrogel systems.


Crystals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 702
Author(s):  
Suxia Guo ◽  
Weiwei Zhou ◽  
Zhenxing Zhou ◽  
Yuchi Fan ◽  
Wei Luo ◽  
...  

Raw powders are processed in water during the freeze-dry pulsated orifice ejection method (FD-POEM), leading to the inclusion of oxygen impurities. This study proposes a strategy for removing the oxygen content and enhancing the mechanical performance of laser powder bed fusion (L-PBF) builds from powders using carbon nanotubes (CNTs) and H2 reduction. Spherical 1.5 wt.% CNT/Mo composite powders with uniform dispersion were fabricated via FD-POEM. The quantity of MoO2 decreased significantly, and a hexagonally structured Mo2C phase was simultaneously formed in the L-PBF build. The Mo2C with network structure was distributed along the boundaries of equiaxed Mo grains, leading to an increased Vickers hardness of the matrix. This study demonstrates the feasibility of fabricating oxygen-free and high-strength refractory parts during L-PBF for ultrahigh-temperature applications.


Polymers ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 1124
Author(s):  
Zhifang Liang ◽  
Hongwu Wu ◽  
Ruipu Liu ◽  
Caiquan Wu

Green biodegradable plastics have come into focus as an alternative to restricted plastic products. In this paper, continuous long sisal fiber (SF)/polylactic acid (PLA) premixes were prepared by an extrusion-rolling blending process, and then unidirectional continuous long sisal fiber-reinforced PLA composites (LSFCs) were prepared by compression molding to explore the effect of long fiber on the mechanical properties of sisal fiber-reinforced composites. As a comparison, random short sisal fiber-reinforced PLA composites (SSFCs) were prepared by open milling and molding. The experimental results show that continuous long sisal fiber/PLA premixes could be successfully obtained from this pre-blending process. It was found that the presence of long sisal fibers could greatly improve the tensile strength of LSFC material along the fiber extension direction and slightly increase its tensile elongation. Continuous long fibers in LSFCs could greatly participate in supporting the load applied to the composite material. However, when comparing the mechanical properties of the two composite materials, the poor compatibility between the fiber and the matrix made fiber’s reinforcement effect not well reflected in SSFCs. Similarly, the flexural performance and impact performance of LSFCs had been improved considerably versus SSFCs.


Author(s):  
Mohamad Alsaadi ◽  
Bashar Younus ◽  
Ahmet Erklig ◽  
Mehmet Bulut ◽  
Omer Bozkurt ◽  
...  

The influence of various graphene nano-platelets (GNPs) content on the tensile, flexural and Charpy impact characteristics of carbon, Kevlar and hybrid carbon/Kevlar fibers reinforced epoxy matrix composites was investigated. Both of composite configurations as carbon and Kevlar at outer and core skins were experimentally tested. The SEM images for flexural specimens were taken to observe the adhesion mechanism of GnPs particles with fiber/epoxy system. It is found that hybridization with Kevlar layers is contributed a positive effect on the hybrid carbon/Kevlar laminate structures in terms of tensile, flexural and impact behaviour. The incorporation of GnPs particles in hybrid and non-hybrid composite samples results in significant improvements in tensile, flexural and impact properties, and the greatest improvement occurs within the GnPs particle content of 0.1 and 0.25 wt%, indicating that the interfacial bonding between the matrix and the fibers is better due to the large surface area of the GnPs and the good entanglement between the GnPs layers and the matrix chains. The samples of impact test are experimented for edgewise and flatwise directions.


Processes ◽  
2021 ◽  
Vol 9 (6) ◽  
pp. 1021
Author(s):  
Yunzhao Li ◽  
Huaping Tang ◽  
Ruilin Lai

Resistance spot welded 1.2 mm (t)-thick 1400 MPa martensitic steel (MS1400) samples are fabricated and their microstructure, mechanical properties are investigated thoroughly. The mechanical performance and failure modes exhibit a strong dependence on weld-nugget size. The pull-out failure mode for MS1400 steel resistance spot welds does not follow the conventional weld-nugget size recommendation criteria of 4t0.5. Significant softening was observed due to dual phase microstructure of ferrite and martensite in the inter-critical heat affected zone (HAZ) and tempered martensite (TM) structure in sub-critical HAZ. However, the upper-critical HAZ exhibits obvious higher hardness than the nugget zone (NZ). In addition, the mechanical properties show that the cross-tension strength (CTS) is about one quarter of the tension-shear strength (TSS) of MS1400 weld joints, whilst the absorbed energy of cross-tension and tension-shear are almost identical.


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