Electrical impedance analysis of carbon nanotube/epoxy nanocomposite-based piezoresistive strain sensors under uniaxial cyclic static tensile loading

2019 ◽  
Vol 54 (6) ◽  
pp. 845-855 ◽  
Author(s):  
Abdulkadir Sanli ◽  
Olfa Kanoun

Carbon nanotubes-based nanocomposites have gained a great amount of attraction and play a key role in the realization of strain sensors owing to their remarkable physical properties. In this study, the piezoresistivity of multi-walled carbon nanotubes (MWCNTs)/epoxy-based nanocomposite-based strain sensor under static tensile load is examined using electrochemical impedance spectroscopy. Morphological examinations show that MWCNTs are randomly and homogeneously distributed in the epoxy polymer matrix. A simplified resistance constant phase element model is proposed and validated by impedance spectrum to fit the impedance spectra and the equivalent circuit parameters are extracted under uniaxial static load. Impedance results suggest that depending on the frequency regions, the sensor exhibits different responses under loading. Moreover, the proposed sensor gives high sensitivity, linearity and low hysteresis under cyclic quasi-static loading and unloading that makes the sensor a promising candidate for practical strain sensor applications.

Nanoscale ◽  
2018 ◽  
Vol 10 (28) ◽  
pp. 13599-13606 ◽  
Author(s):  
Binghao Liang ◽  
Zhiqiang Lin ◽  
Wenjun Chen ◽  
Zhongfu He ◽  
Jing Zhong ◽  
...  

A highly stretchable and sensitive strain sensor based on a gradient carbon nanotube was developed. The strain sensors show an unprecedented combination of both high sensitivity (gauge factor = 13.5) and ultra-stretchability (>550%).


Author(s):  
Ryohei Nakagawa ◽  
Zhi Wang ◽  
Ken Suzuki

Health monitoring devices using a strain sensor, which shows high sensitivity and large deformability, are strongly demanded due to further aging of society with fewer children. Conventional strain sensors, such as metallic strain gauges and semiconductive strain sensors, however, aren’t applicable to health monitoring because of their low sensitivity and deformability. In this study, fundamental design of area-arrayed graphene nano-ribbon (GNR) strain senor was proposed in order to fabricate next-generation strain sensor. The sensor was consisted of two sections, which are stress concentration section and stress detecting section. This structure can take full advantage of GNR’s properties. Moreover, high quality GNR fabrication process, which is one of the important process in the sensor, was developed by applying CVD (Chemical Vapor Deposition) method. Top-down approach was applied to fabricate the GNR. At first, in order to synthesize a high-quality graphene sheet, acetylene-based LPCVD (low pressure chemical vapor deposition) using a closed Cu foil was employed. After that, graphene was transferred silicon substrate and the quality was evaluated. The high quality graphene was transferred on the soft PDMS substrate and metallic electrodes were fabricated by applying MEMS technology. Area-arrayed fine pin structure was fabricated by using hard PDMS as a stress-concentration section. Finally, both sections were integrated to form a highly sensitive and large deformable pressure sensor. The strain sensitivity of the GNR-base sensor was also evaluated.


2018 ◽  
Vol 4 (2) ◽  
pp. 1 ◽  
Author(s):  
Angelica Campigotto ◽  
Stephane Leahy ◽  
Ayan Choudhury ◽  
Guowei Zhao ◽  
Yongjun Lai

A novel, inexpensive, and easy-to-use strain sensor using polydimethylsiloxane (PDMS)  was developed. The sensor consists of a microchannel that is partially filled with a coloured liquid and embedded in a piece of PDMS. A finite element model was developed to optimize the geometry of the microchannel to achieve higher sensitivity. The highest gauge factor that was measured experimentally was 41. The gauge factor was affected by the microchannel’s square cross-sectional area, the number of basic units in the microchannel, and the inlet and outlet configuration. As a case study, the developed strain sensors were used to measure the rotation angle of the wrist and finger joints.


Coatings ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 792 ◽  
Author(s):  
Hsuan-Ling Kao ◽  
Cheng-Lin Cho ◽  
Li-Chun Chang ◽  
Chun-Bing Chen ◽  
Wen-Hung Chung ◽  
...  

A fully inkjet-printed strain sensor based on carbon nanotubes (CNTs) was fabricated in this study for microstrain and microcrack detection. Carbon nanotubes and silver films were used as the sensing layer and conductive layer, respectively. Inkjet-printed CNTs easily undergo agglomeration due to van der Waals forces between CNTs, resulting in uneven films. The uniformity of CNT film affects the electrical and mechanical properties. Multi-pass printing and pattern rotation provided precise quantities of sensing materials, enabling the realization of uniform CNT films and stable resistance. Three strain sensors printed eight-layer CNT film by unidirectional printing, rotated by 180° and 90° were compared. The low density on one side of eight-layer CNT film by unidirectional printing results in more disconnection and poor connectivity with the silver film, thereby, significantly increasing the resistance. For 180° rotation eight-layer strain sensors, lower sensitivity and smaller measured range were found because strain was applied to the uneven CNT film resulting in non-uniform strain distribution. Lower resistance and better strain sensitivity was obtained for eight-layer strain sensor with 90° rotation because of uniform film. Given the uniform surface morphology and saturated sheet resistance of the 20-layer CNT film, the strain performance of the 20-layer CNT strain sensor was also examined. Excluding the permanent destruction of the first strain, 0.76% and 1.05% responses were obtained for the 8- and 20-layer strain sensors under strain between 0% and 3128 µε, respectively, which demonstrates the high reproducibility and recoverability of the sensor. The gauge factor (GF) of 20-layer strain sensor was found to be 2.77 under strain from 71 to 3128 µε, which is higher than eight-layer strain sensor (GF = 1.93) due to the uniform surface morphology and stable resistance. The strain sensors exhibited a highly linear and reversible behavior under strain of 71 to 3128 µε, so that the microstrain level could be clearly distinguished. The technology of the fully inkjet-printed CNT-based microstrain sensor provides high reproducibility, stability, and rapid hardness detection.


2014 ◽  
Vol 2014 ◽  
pp. 1-9
Author(s):  
Wei Qiu ◽  
Shi-Lei Li ◽  
Wei-lin Deng ◽  
Di Gao ◽  
Yi-Lan Kang

A strain sensor composed of carbon nanotubes with Raman spectroscopy can achieve measurement of the three in-plane strain components in microscale. Based on previous work on the mathematic model of carbon nanotube strain sensors, this paper presents a detailed study on the optimization, diversification, and standardization of a CNT strain sensor from the viewpoint of metrology. A new miniaccessory for polarization control is designed, and two different preparing methods for CNT films as sensing media are introduced to provide diversified choices for applications. Then, the standard procedure of creating CNT strain sensors is proposed. Application experiments confirmed the effectiveness of the above improvement, which is helpful in developing this method for convenient metrology.


2018 ◽  
Vol 2 (2) ◽  
pp. 355-361 ◽  
Author(s):  
Xi Fan ◽  
Naixiang Wang ◽  
Jinzhao Wang ◽  
Bingang Xu ◽  
Feng Yan

A stretchable plastic strain sensor was fabricated, showing high sensitivity and a broad strain-sensing region with good durability.


Author(s):  
Tarun Singla ◽  
Amrinder Pal Singh ◽  
Suresh Kumar ◽  
Gagandeep Singh ◽  
Navin Kumar

The usage of nano phase materials for strain sensing applications has attracted attention due to their unique electromechanical properties. The nanocomposite as piezo-resistive films provides an alternative for the realization of strain sensors with high sensitivity than the conventional sensors based on metal and semiconductor strain gauges. In this work, polymer based nano-composite with carbon nanotubes as filler were developed. The multi-walled carbon nanotubes/polystyrene (MWCNTs/PS) nano-composite films were prepared with different wt.% of CNTs using solution mixing method. Field emission scanning electron microscopy technique was carried out to investigate the morphology and dispersion of CNTs in the nano-composite sample. Fourier transform infrared spectroscopy technique was employed to characterize the bonds present in the prepared nano-composite. The electrical response of the composite films was recorded in the form of current-voltage (I-V) characteristics using source meter. The electromechanical response of the nano-composite films with different wt.% of filler CNTs was recorded by applying uni-axial tensile load. The electromechanical responses were then analyzed to obtain gauge factor for the strain sensitivity. The highest gauge factor of 133 was recorded during tensile testing of the nano-composite with 3 wt.% of CNTs fillers.


Micromachines ◽  
2021 ◽  
Vol 12 (6) ◽  
pp. 716
Author(s):  
Rong Dong ◽  
Jianbing Xie

In this paper, stretchable strain sensors with a controllable negative resistance sensitivity coefficient are firstly proposed. In order to realize the sensor with a negative resistance sensitivity coefficient, a stretchable stress sensor with sandwich structure is designed in this paper. Carbon nanotubes are added between two layers of silica gel. When the sensor is stretched, carbon nanotubes will be squeezed at the same time, so the sensor will show a resistance sensitivity coefficient that the resistance becomes smaller after stretching. First, nanomaterials are coated on soft elastomer, then a layer of silica gel is wrapped on the outside of the nanomaterials. In this way, similar to sandwich biscuits, a stretchable strain sensor with controllable negative resistance sensitivity coefficient has been obtained. Because the carbon nanotubes are wrapped between two layers of silica gel, when the silica gel is stretched, the carbon nanotubes will be squeezed longitudinally, which increases their density and resistance. Thus, a stretchable strain sensor with negative resistance sensitivity coefficient can be realized, and the resistivity can be controlled and adjusted from 12.7 Ω·m to 403.2 Ω·m. The sensor can be used for various tensile testing such as human motion monitoring, which can effectively expand the application range of conventional tensile strain sensor.


Nanomaterials ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 2333
Author(s):  
Huiying Shen ◽  
Huizhen Ke ◽  
Jingdong Feng ◽  
Chenyu Jiang ◽  
Qufu Wei ◽  
...  

Owing to the multi-dimensional complexity of human motions, traditional uniaxial strain sensors lack the accuracy in monitoring dynamic body motions working in different directions, thus multidirectional strain sensors with excellent electromechanical performance are urgently in need. Towards this goal, in this work, a stretchable biaxial strain sensor based on double elastic fabric (DEF) was developed by incorporating carboxylic multi-walled carbon nanotubes(c-MWCNTs) and polypyrrole (PPy) into fabric through simple, scalable soaking and adsorption-oxidizing methods. The fabricated DEF/c-MWCNTs/PPy strain sensor exhibited outstanding anisotropic strain sensing performance, including relatively high sensitivity with the maximum gauge factor (GF) of 5.2, good stretchability of over 80%, fast response time < 100 ms, favorable electromechanical stability, and durability for over 800 stretching–releasing cycles. Moreover, applications of DEF/c-MWCNTs/PPy strain sensor for wearable devices were also reported, which were used for detecting human subtle motions and dynamic large-scale motions. The unconventional applications of DEF/c-MWCNTs/PPy strain sensor were also demonstrated by monitoring complex multi-degrees-of-freedom synovial joint motions of human body, such as neck and shoulder movements, suggesting that such materials showed a great potential to be applied in wearable electronics and personal healthcare monitoring.


Nanomaterials ◽  
2021 ◽  
Vol 12 (1) ◽  
pp. 120
Author(s):  
Rui Wang ◽  
Xiaoyang Zhu ◽  
Luanfa Sun ◽  
Shuai Shang ◽  
Hongke Li ◽  
...  

The development of strain sensors with high sensitivity and stretchability is essential for health monitoring, electronic skin, wearable devices, and human-computer interactions. However, sensors that combine high sensitivity and ultra-wide detection generally require complex preparation processes. Here, a novel flexible strain sensor with high sensitivity and transparency was proposed by filling a multiwalled carbon nanotube (MWCNT) solution into polydimethylsiloxane (PDMS) channel films fabricated via an electric field-driven (EFD) 3D printing and molding hybrid process. The fabricated flexible strain sensor with embedded MWCNT networks had superior gauge factors of 90, 285, and 1500 at strains of 6.6%, 14%, and 20%, respectively. In addition, the flexible strain sensors with an optical transparency of 84% offered good stability and durability with no significant change in resistance after 8000 stretch-release cycles. Finally, the fabricated flexible strain sensors with embedded MWCNT networks showed good practical performance and could be attached to the skin to monitor various human movements such as wrist flexion, finger flexion, neck flexion, blinking activity, food swallowing, and facial expression recognition. These are good application strategies for wearable devices and health monitoring.


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