Quantitative Analysis of Carbon Steel with Multi-Line Internal Standard Calibration Method Using Laser-Induced Breakdown Spectroscopy

2016 ◽  
Vol 70 (4) ◽  
pp. 702-708 ◽  
Author(s):  
Congyuan Pan ◽  
Xuewei Du ◽  
Ning An ◽  
Qiang Zeng ◽  
Shengbo Wang ◽  
...  
Author(s):  
Raquel C Machado ◽  
Diego Victor Babos ◽  
Daniel Fernandes Andrade ◽  
Edenir Rodrigues Pereira-Filho

Quantitative analysis requires several efforts to obtain an adequate calibration method to overcome matrix effects employing direct solid analysis by laser-induced breakdown spectroscopy (LIBS). To this end, in this study,...


2018 ◽  
Vol 246 ◽  
pp. 01114
Author(s):  
C. P. Chen ◽  
L. Hei ◽  
S. C. Yu ◽  
W. L. Chen ◽  
M. X. Cai

With the rapid development of spectroscopy technology, laser induced breakdown spectroscopy (LIBS) has become the focus of elemental analysis technology in recent years. With its advantages of non-destructive testing, rapid and multi-element detection, LIBS has been successfully applied to the analysis of geochemical characteristics of soil elements in river basins. The application of LIBS technology in soil elemental analysis of watershed is reviewed in detail. The accuracy of LIBS technology in soil element analysis is studied with the Masha River Basin as the research area. On this basis, the key problems in the process of soil element analysis, such as spectral enhancement methods and quantitative analysis methods, were analyzed. The analysis results show that the accuracy of elemental analysis between LIBS and traditional chemical methods is not much different, but the analysis time of LIBS method is shorter. Methods such as MLR, PLSR, and internal standard methods can improve the fit of the calibration curve and reduce the quantitative analysis error. By changing parameters such as laser energy and delay time, the spectral intensity can be enhanced to reduce the effects of matrix effects. In the process of elemental analysis, the effects of soil physical and chemical parameters should be considered comprehensively, and appropriate quantitative analysis methods should be adopted to improve the accuracy of the analysis results.


2021 ◽  
Author(s):  
Jiujiang Yan ◽  
Yating Shi ◽  
Ke Liu ◽  
Hongjun Li ◽  
Zhiyang Tang ◽  
...  

Internal standard line plays a crucial role in the univariate quantitative analysis in portable laser-induced breakdown spectroscopy (LIBS) technology. To overcome the uncertainty of the conventional internal standard method, the...


Sign in / Sign up

Export Citation Format

Share Document