Catalyst-Free Template-Synthesis of ZnO Nanopetals at 60 °C

2007 ◽  
Vol 7 (2) ◽  
pp. 696-699 ◽  
Author(s):  
Hui Pan ◽  
Yuan Ping Feng ◽  
Jianyi Lin ◽  
Chuan Jun Liu ◽  
Thye Shen Wee

We report successful growth of a new form of ZnO nanostructures, ZnO nanopetals at low temperature. This two-dimensional nanostructure is morphologically different from nanowalls. The flat and circularly edged nanopetals intersect each other. The thickness of nanopetals is uniform and about 30 nm. The nanostructure was produced using a simple catalyst-free chemical method based on anodic aluminum oxide (AAO) template. The growth temperature was 60 °C which is much lower than that required for growing ZnO nanowalls. The formation of the nanopetal network was induced by the porous alumina network on the surface of the AAO template.

2008 ◽  
Vol 8 (9) ◽  
pp. 4488-4493 ◽  
Author(s):  
Feng Chen ◽  
Adrian H. Kitai

Indium nanowires with diameters approximately 300 nm have been synthesized by a hydraulic pressure technique using anodic aluminum oxide (AAO) templates. The indium melt is injected into the AAO template and solidified to form nanostructures. The nanowires are dense, continuous and uniformly run through the entire ∼60 μm thickness of the AAO template. X-ray diffraction (XRD) reveals that the nanowires are polycrystalline with a preferred orientation. SEM is performed to characterize the morphology of the nanowires.


2012 ◽  
Vol 184-185 ◽  
pp. 924-927
Author(s):  
Lei Shan Chen ◽  
Cun Jing Wang ◽  
Gai Rong Chen

The reactions were carried out by decomposing acetylene at 1000 °C in a two-stage furnace system for 10 min. In the first furnace no catalyst was placed and an AAO template with the average diameter about 50 nm was placed in the second furnace whose temperature was designed to be 500 °C, 600 °C and 700 °C. The samples were characterized by scanning electron microscopy and high resolution transmission electron microscopy. The results show that carbon spheres with average diameter about 50 nm on the AAO template surface were obtained when the temperature of the second furnace was designed to be 700 °C. These carbon spheres are composed of unclosed graphene layers with an interlayer distance of 0.33–0.35 nm between the layers.


2011 ◽  
Vol 393-395 ◽  
pp. 32-35
Author(s):  
Cun Jing Wang ◽  
Peng Yao ◽  
Gai Rong Chen

The reactions were carried out by decomposing acetylene at 1000 °C in a two-stage furnace system for 10 min. In the first furnace no catalyst was placed and an AAO template with average diameter about 50 nm was placed in the second furnace whose temperature was designed to be 700 °C. The samples were characterized by scanning electron microscopy and high resolution transmission electron microscopy. The results show that carbon spheres with average diameter about 50 nm on the AAO template surface were obtained and these carbon spheres are composed of unclosed graphene layers with an interlayer distance of 0.33–0.35 nm between the layers.


2009 ◽  
Vol 469 (1-2) ◽  
pp. 332-335 ◽  
Author(s):  
Xiaofei Qu ◽  
Jinhui Dai ◽  
Jintao Tian ◽  
Xiang Huang ◽  
Zhongfang Liu ◽  
...  

2018 ◽  
Vol 29 (34) ◽  
pp. 345401 ◽  
Author(s):  
Gu Young Cho ◽  
Yusung Kim ◽  
Soon Wook Hong ◽  
Wonjong Yu ◽  
Young-Beom Kim ◽  
...  

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