X-Ray Absorption of Gold Nanoparticles with Thin Silica Shell

2006 ◽  
Vol 6 (11) ◽  
pp. 3503-3506 ◽  
Author(s):  
Yeon-Su Park ◽  
Luis M. Liz-Marzán ◽  
Atsuo Kasuya ◽  
Yoshio Kobayashi ◽  
Daisuke Nagao ◽  
...  
Nanomaterials ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1898
Author(s):  
Iole Venditti ◽  
Giovanna Iucci ◽  
Ilaria Fratoddi ◽  
Manuela Cipolletti ◽  
Emiliano Montalesi ◽  
...  

Strongly hydrophilic gold nanoparticles (AuNPs), functionalized with citrate and L-cysteine, were synthetized and used as Resveratrol (RSV) vehicle to improve its bioavailability. Two different conjugation procedures were investigated: the first by adding RSV during AuNPs synthesis (1) and the second by adding RSV after AuNPs synthesis (2). The two different conjugated systems, namely AuNPs@RSV1 and AuNPs@RSV2 respectively, showed good loading efficiency (η%): η1 = 80 ± 5% for AuNPs@RSV1 and η2 = 20 ± 3% for AuNPs@RSV2. Both conjugated systems were investigated by means of Dynamic Light Scattering (DLS), confirming hydrophilic behavior and nanodimension (<2RH> 1 = 45 ± 12 nm and <2RH> 2 = 170 ± 30 nm). Fourier Transform Infrared Spectroscopy (FT-IR), Synchrotron Radiation induced X-Ray Photoelectron Spectroscopy (SR-XPS) and Near Edge X-ray Absorption Fine Structure (NEXAFS) techniques were applied to deeply understand the hooking mode of RSV on AuNPs surface in the two differently conjugated systems. Moreover, the biocompatibility of AuNPs and AuNPs@RSV1 was evaluated in the concentration range 1.0–45.5 µg/mL by assessing their effect on breast cancer cell vitality. The obtained data confirmed that, at the concentration used, AuNPs do not induce cell death, whereas AuNPs@RSV1 maintains the same anticancer effects as the unconjugated RSV.


2020 ◽  
Vol 56 (71) ◽  
pp. 10329-10332 ◽  
Author(s):  
Paulo F. M. de Oliveira ◽  
Adam A. L. Michalchuk ◽  
Ana Guilherme Buzanich ◽  
Ralf Bienert ◽  
Roberto M. Torresi ◽  
...  

A new tandem approach combines XRD and XANES for time-resolved in situ monitoring of the mechanochemical synthesis of gold nanoparticles.


2017 ◽  
Vol 520 (1) ◽  
pp. 196-201
Author(s):  
Phakkhananan Pakawanit ◽  
Rattikorn Yimnirun ◽  
Yongyut Laosiritaworn ◽  
Kanokwan Kanchiang

ACS Nano ◽  
2015 ◽  
Vol 9 (4) ◽  
pp. 4036-4042 ◽  
Author(s):  
Samuel T. Chill ◽  
Rachel M. Anderson ◽  
David F. Yancey ◽  
Anatoly I. Frenkel ◽  
Richard M. Crooks ◽  
...  

2015 ◽  
Vol 50 (4) ◽  
pp. 281-285 ◽  
Author(s):  
A. Berrezoug ◽  
A.S. A Dib ◽  
A.H. Belbachir

Langmuir ◽  
2006 ◽  
Vol 22 (9) ◽  
pp. 4310-4314 ◽  
Author(s):  
Bruce G. Anderson ◽  
Juan C. Fierro-Gonzalez ◽  
Kanaparthi Ramesh ◽  
C. P. Vinod ◽  
J. W. Niemantsverdriet ◽  
...  

Small ◽  
2011 ◽  
pp. n/a-n/a ◽  
Author(s):  
Bieke Van de Broek ◽  
Didier Grandjean ◽  
Jesse Trekker ◽  
Jian Ye ◽  
Kris Verstreken ◽  
...  

2014 ◽  
Vol 16 (42) ◽  
pp. 23157-23163 ◽  
Author(s):  
Flavio Zamponi ◽  
Thomas J. Penfold ◽  
Maarten Nachtegaal ◽  
Andrea Lübcke ◽  
Jochen Rittmann ◽  
...  

The onset of disorder 100 ps after optical excitation of small Au NPs was revealed by X-ray absorption spectroscopy.


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