scholarly journals Energy Dispersive Diffractometry for Quantitative Texture Studies

1990 ◽  
Vol 12 (4) ◽  
pp. 243-247 ◽  
Author(s):  
J. A. Szpunar

Energy dispersive diffractometry is becoming a useful tool for texture measurements. In this work we demonstrated that the intensity measured at points in four inverse pole figures for cold-rolled steel can be used to calculate the orientation distribution function (ODF) with an accuracy sufficient for the determination of about 12 series expansion coefficients. A pole figure generated from such a selective experiment agrees with the pole figure measured by neutron diffraction.

1989 ◽  
Vol 22 (6) ◽  
pp. 559-561 ◽  
Author(s):  
J. A. Szpunar ◽  
P. Blandford ◽  
D. C. Hinz

Series-expansion coefficients for an orientation distribution function (ODF) of cold-rolled aluminium sheet were calculated from the intensity of Debye–Scherrer rings obtained in an experiment using synchrotron radiation. Calculated and observed pole figures demonstrate that a sufficiently good approximation to the ODF is obtained from coefficients calculated to l = 8.


1986 ◽  
Vol 6 (4) ◽  
pp. 289-313 ◽  
Author(s):  
H. P. Lee ◽  
H. J. Bunge ◽  
C. Esling

Because of the superposition of pole figures corresponding to symmetrically equivalent crystal directions, only the reduced orientation distribution function f∼(g) can be obtained directly by pole figure inversion. The additional information contained in the positivity condition of the ODF allows, however, the determination of an approximation to the “indeterminable” part and hence of the complete ODF f(g), if the texture has sufficiently large zero-ranges. The application of the method and the accuracy of the results was tested using two theoretical and one experimental textures. The accuracy of the complete ODF depends on the size of the zero-range, the errors in its determination, and on the errors, experimental and truncational, of the reduced ODF. The “physical zero” used in order to determine the zero-range is defined according to the statistical error of the pole figure measurement.


1999 ◽  
Vol 31 (4) ◽  
pp. 239-248 ◽  
Author(s):  
H. Ghildiyal ◽  
E. Jansen ◽  
A. Kirfel

The volume texture of a naturally deformed quartzite from the Kaoko belt, North-West Namibia, has been analysed by both universal stage microscopy and neutron diffraction. Universal stage microscopy is restricted to the determination of the base pinacoid preferred orientation in quartzite. For a more complete description of the texture, the orientations of additional crystal planes, such as first and second order prisms as well as positive and negative rhombs, must be known. Neutron methods allow the evaluation of pole figures of all Bragg reflecting planes, of which those of the first order prisms being considered to be the most active slip planes, are of particular interest. Drawbacks of neutron diffraction, i.e. the faking of an eventually absent inversion centre and lack of resolution, can be overcome by pole figure inversion and subsequent calculation of desired pole figures. Both, universal stage microscopy and neutron diffraction yield well comparable results, of course only with respect to the pole figure of the c-axis.


1993 ◽  
Vol 21 (2-3) ◽  
pp. 71-78
Author(s):  
H.-G. Brokmeier

This paper describes the application of neutron diffraction to investigate the texture of a zinc layer 8 μm in thickness. In a nondestructive way both the texture of the zinc layer as well as the texture of the steel substrate were studied. Therefore, pole figures of iron ((110), (200) and (211)) and of zinc ((0002), (101¯0), (101¯1); and (101¯3)/(112¯0)) were measured; additionally the orientation distribution function of iron and zinc were calculated.


1978 ◽  
Vol 3 (1) ◽  
pp. 1-25 ◽  
Author(s):  
Jerzy Jura ◽  
Jan Pospiech

The use of incomplete pole figure data for defining the orientation distribution function (ODF) in a polycrystalline material is of great practical importance, because it enables the use of experimental data from a simplified measurement. The present paper provides the source text of a computer program for calculating the coefficients of ODF series expansion, Cℓμυ. The data for computations are in the incomplete pole figures of rhombic symmetry as determined by the back reflection or transmission technique for crystalline solids of the cubic system. Also described is the numerical method of determining the coefficients Cℓμυ, and the results so obtained are discussed.


1995 ◽  
Vol 28 (5) ◽  
pp. 532-533 ◽  
Author(s):  
L.-G. Yu ◽  
H. Guo ◽  
B. C. Hendrix ◽  
K.-W. Xu ◽  
J.-W. He

A new simple method is proposed for determining the orientation distribution function (ODF) for three-dimensional texture analysis in a polycrystal based on the reality that the accuracy of an ODF is dependent on both the accuracy of each measured pole figure and the number of pole figures.


Sign in / Sign up

Export Citation Format

Share Document