scholarly journals Green Synthesis of Carbon Dots from Grapefruit and Its Fluorescence Enhancement

2020 ◽  
Vol 2020 ◽  
pp. 1-7
Author(s):  
Xinzhu Huo ◽  
Yuxuan He ◽  
Shiqi Ma ◽  
Yingying Jia ◽  
Jiaming Yu ◽  
...  
Keyword(s):  
Carbon Dots ◽  
Carbon Sources ◽  
Carbon Quantum Dots ◽  
One Pot ◽  
Transmission Electron ◽  
Three Samples ◽  
Structure Morphology ◽  
Ir Transmission ◽  
Ft Ir ◽  
Doped Carbon Dots

In this study, undoped carbon quantum dots (UCQDs, UCQDs-peel) and N-doped carbon dots (NCQDs) were prepared by a facile one-pot environmentally friendly hydrothermal method using grapefruit as carbon sources in the absence and presence of area, respectively. The structure, morphology, and fluorescence properties of three samples were characterized by Fourier transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), and photoluminescence (PL). It was found that three types of CQDs could emit blue fluorescence with different intensities when irradiated with ultraviolet light. Compared to the luminescence properties of UCQDs, NCQDs, and UCQDs-peel, it can be seen that the fluorescence intensity of NCQDs was strongest due to the presence of NH and C-N bonds.

scholarly journals One pot three component synthesis of substituted 3,4,6,7-tetrahydro-3,3,6,6-tetramethyl-9,10-diphenylacridine-1,8(2H,5H,9H,10H)-diones catalyzed by efficient In2O3-SiO2

2021 ◽  
Author(s):  
Deepak Totaram Tayde ◽  
Madhukar E. Navgire ◽  
Machhindra K. Lande
Keyword(s):  
High Yield ◽  
Reusable Catalyst ◽  
X Ray Diffraction ◽  
One Pot ◽  
Synthetic Strategy ◽  
Transmission Electron ◽  
Catalytic Material ◽  
Ir Transmission ◽  
Ft Ir ◽  
Temperature Programmed

Abstract A convenient, One pot synthesis of heterocyclic nucleous acridine derivative compound has been achieved those are having very much attention in medicinal chemistry because of their extensive application in biology. The mixture of dimedone, substituted benzaldehyde and aniline were catalyzed by efficient In2O3-SiO2 heterogeneous reusable catalyst in ethanol to obtain the desired acridine derivatives with good yield. Hydrothermal method used to synthesize In2O3-SiO2 catalytic material. This catalytic material were characterized by using X-ray diffraction spectroscopy (XRD), scanning electron microscopy (SEM), Energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FT-IR), Transmission electron microscope (TEM), Temperature-programmed desorption (NH3-TPD) and Brunauer-Emmett-Teller (BET). Our synthetic strategy features high yield, simple work up procedure, non-toxic, clean, and easy recovery and reusability of the catalytic system.

scholarly journals A facile green and one-pot synthesis of grape seed-derived carbon quantum dots as a fluorescence probe for Cu(ii) and ascorbic acid

RSC Advances ◽  
2021 ◽  
Vol 11 (54) ◽  
pp. 34107-34116
Author(s):  
Jiawei Li ◽  
Ouwen Xu ◽  
Xiashi Zhu
Keyword(s):  
Quantum Dots ◽  
Ascorbic Acid ◽  
Carbon Dots ◽  
Fluorescence Probe ◽  
Grape Seed ◽  
Carbon Quantum Dots ◽  
One Pot ◽  
One Pot Synthesis ◽  
Doped Carbon Dots

In this study, an on–off–on fluorescence probe for the detection of trace Cu(ii) and ascorbic acid (AA) based on biomass-derived sulfur and nitrogen double heteroatom-doped carbon dots (N,S-CDs) was designed.

scholarly journals Hydrothermal Synthesis, Characterization and Exploration of Photocatalytic Activities of Polyoxometalate: Ni-CoWO4 Nanoparticles

Crystals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 456
Author(s):  
Fahad A. Alharthi ◽  
Hamdah S. Alanazi ◽  
Amjad Abdullah Alsyahi ◽  
Naushad Ahmad
Keyword(s):  
Electron Microscopy ◽  
Hydrothermal Synthesis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Structure Morphology ◽  
Photocatalytic Activities ◽  
Ft Ir ◽  
Photocatalytic Reactions ◽  
Cobalt Tungstate

This study demonstrated the hydrothermal synthesis of bimetallic nickel-cobalt tungstate nanostructures, Ni-CoWO4 (NCW-NPs), and their phase structure, morphology, porosity, and optical properties were examined using X-ray Diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), Scanning electron microscopy- energy dispersive X-ray spectroscopy (SEM-EDS), high resolution Transmission electron microscopy (HR-TEM), Brunauer-Emmett-Teller (BET) and Raman instruments. It was found that as-calcined NCW-NPs have a monoclinic phase with crystal size ~50–60 nm and is mesoporous. It possessed smooth, spherical, and cubic shape microstructures with defined fringe distance (~0.342 nm). The photocatalytic degradation of methylene blue (MB) and rose bengal (RB) dye in the presence of NCW-NPs was evaluated, and about 49.85% of MB in 150 min and 92.28% of RB in 90 min degraded under visible light. In addition, based on the scavenger’s study, the mechanism for photocatalytic reactions is proposed.

scholarly journals Facile Hydrothermal and Solvothermal Synthesis and Characterization of Nitrogen-Doped Carbon Dots from Palm Kernel Shell Precursor

2021 ◽  
Vol 11 (4) ◽  
pp. 1630
Author(s):  
Yakubu Newman Monday ◽  
Jaafar Abdullah ◽  
Nor Azah Yusof ◽  
Suraya Abdul Rashid ◽  
Rafidah Hanim Shueb
Keyword(s):  
Carbon Dots ◽  
Batch Reactor ◽  
Average Particle Size ◽  
Research Work ◽  
Palm Kernel ◽  
Average Particle ◽  
One Pot ◽  
Palm Kernel Shell ◽  
Doped Carbon Dots ◽  
Nitrogen Doped Carbon

Carbon dots (CDs), a nanomaterial synthesized from organic precursors rich in carbon content with excellent fluorescent property, are in high demand for many purposes, including sensing and biosensing applications. This research focused on preparing CDs from natural and abundant waste, palm kernel shells (PKS) obtained from palm oil biomass, aiming for sensing and biosensing applications. Ethylenediamine and L-phenylalanine doped CDs were produced via the hydrothermal and solvothermal methods using one-pot synthesis techniques in an autoclave batch reactor. The as-prepared N-CDs shows excellent photoluminescence (PL) property and a quantum yield (QY) of 13.7% for ethylenediamine (EDA) doped N-CDs (CDs-EDA) and 8.6% for L-phenylalanine (L-Ph) doped N-CDs (CDs-LPh) with an excitation/emission wavelength of 360 nm/450 nm. The transmission electron microscopy (TEM) images show the N-CDs have an average particle size of 2 nm for both CDs. UV-Visible spectrophotometric results showed C=C and C=O transition. FTIR results show and confirm the presence of functional groups, such as -OH, -C=O, -NH2 on the N-CDs, and the X-ray diffraction pattern showed that the N-CDs were crystalline, depicted with sharp peaks. This research work demonstrated that palm kernel shell biomass often thrown away as waste can produce CDs with excellent physicochemical properties.

A green synthetic route for the surface-passivation of carbon dots as an effective multifunctional fluorescent sensor for the recognition and detection of toxic metal ions from aqueous solution

2019 ◽  
Vol 11 (4) ◽  
pp. 490-506 ◽  
Author(s):  
K. Radhakrishnan ◽  
P. Panneerselvam ◽  
M. Marieeswaran
Keyword(s):  
Aqueous Solution ◽  
Quantum Dots ◽  
Carbon Dots ◽  
Surface Passivation ◽  
Fluorescent Sensor ◽  
Toxic Metal ◽  
Carbon Quantum Dots ◽  
Synthetic Route ◽  
One Pot ◽  
Hydrothermal Methods

In this work, a green synthetic route was used to create a number of surface passivated fluorescent carbon quantum dots, which are explored as promising sensing probes, via facile one-pot hydrothermal methods.

Carbon Nanotube Templated Growth of the Nano-Crystalline NaY Zeolite

2011 ◽  
Vol 194-196 ◽  
pp. 594-597
Author(s):  
Ke Tang ◽  
Xin Hong ◽  
Jin Gang Qi
Keyword(s):  
Structural Characteristics ◽  
Internal Diameter ◽  
X Ray Diffraction ◽  
Nay Zeolite ◽  
Nano Crystalline ◽  
Transmission Electron ◽  
Ir Transmission ◽  
Ft Ir ◽  
Nay Zeolites ◽  
Nanosized Zeolites

FAU-type(NaY) zeolites nanocrystals have been synthesized through crystallization of gel in mesoporous system of carbon nanotubes(CNTS) with a internal diameter of 20~30 nm. Investigation by using X-ray diffraction (XRD), Fourier transform infrared (FT-IR), transmission electron microscope (TEM) shows that the nanocrystals possess the typical nanosized zeolites structural characteristics which is different from those of microsized zeolites.

An “on–off–on” fluorescent nanoprobe for recognition of Cu2+ and GSH based on nitrogen co-doped carbon quantum dots, and its logic gate operation

2019 ◽  
Vol 11 (20) ◽  
pp. 2650-2657 ◽  
Author(s):  
Yifang Gao ◽  
Huilin Zhang ◽  
Shaomin Shuang ◽  
Hui Han ◽  
Chuan Dong
Keyword(s):  
Quantum Dots ◽  
Carbon Dots ◽  
Logic Gate ◽  
Carbon Quantum Dots ◽  
Gate Operation ◽  
Fluorescent Nanoprobe ◽  
Highly Sensitive ◽  
Doped Carbon Dots ◽  
Co Doped

Novel nitrogen co-doped carbon dots (NCDs) were synthesized as a fluorescent “on–off–on” switch for the highly sensitive and selective sensing of Cu2+ and glutathione (GSH) by a straightforward pyrolysis route.

scholarly journals Synthesis, Characterization, and Tribological Behavior of Oleic Acid Capped Graphene Oxide

2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Tiedan Chen ◽  
Yanqiu Xia ◽  
Zhengfeng Jia ◽  
Zhilu Liu ◽  
Haobo Zhang
Keyword(s):  
Graphene Oxide ◽  
Oleic Acid ◽  
Friction And Wear ◽  
Graphite Powder ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
Transmission Electron ◽  
Alpha Olefin ◽  
Ir Transmission ◽  
Ft Ir

Graphene oxide (GO) nanosheets were prepared by modified Hummers and Offeman methods. Furthermore, oleic acid (OA) capped graphene oxide (OACGO) nanosheets were prepared and characterized by means of Fourier transform-infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), and X-ray diffraction (XRD). At the same time, the friction and wear properties of OA capped graphite powder (OACG), OACGO, and oleic acid capped precipitate of graphite (OACPG) as additives in poly-alpha-olefin (PAO) were compared using four-ball tester and SRV-1 reciprocating ball-on-disc friction and wear tester. By the addition of OACGO to PAO, the antiwear ability was improved and the friction coefficient was decreased. Also, the tribological mechanism of the GO was investigated.

Green preparation of carbon dots for Hg2+ detection and cell imaging

2020 ◽  
Vol 10 (11) ◽  
pp. 1777-1787
Author(s):  
Yadian Xie ◽  
Shanshan Wang ◽  
Ning Fu ◽  
Yan Yang ◽  
Xingliang Liu ◽  
...  
Keyword(s):  
Photoelectron Spectroscopy ◽  
Carbon Dots ◽  
High Sensitivity ◽  
Amorphous Structure ◽  
X Ray Diffraction ◽  
X Ray ◽  
Carbon And Nitrogen ◽  
Transmission Electron ◽  
Sensitivity And Selectivity ◽  
Ft Ir

Carbon dots (CDs) also nitrogen-doped CDs (N-CDs) were produced by green hydrothermal synthesis using Pea and ethanediamine as the carbon and nitrogen source, separately. Transmission electron microscopy (TEM) images displayed that the prepared CDs and N-CDs were well dispersed, had a spherical morphology. X-ray diffraction (XRD) figures of CDs and N-CDs presented a graphitic amorphous structure. Fourier transform infrared spectroscopy (FT-IR) verified that CDs and N-CDs carried many different hydrophilic groups (for example hydroxyl, carboxyl/carbonyl, amide, amino groups) on the surface, X-ray photoelectron spectroscopy (XPS) together verified this result. However, the optical properties and fluorescence quantum yield for N-CDs were obviously superior to those of CDs. Furthermore, the prepared N-CDs displayed outstanding advantages including low toxicity, satisfactory biocompatibility, and excellent chemical stability. More prominently, the prepared N-CDs could detect Hg2+ ions with high sensitivity and selectivity in both water samples and HeLa cells.

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