scholarly journals Physical and Biological Properties of a High-Plasticity Tricalcium Silicate Cement

2018 ◽  
Vol 2018 ◽  
pp. 1-6 ◽  
Author(s):  
Arthur Dias Galarça ◽  
Wellington Luiz de Oliveira Da Rosa ◽  
Tiago Machado Da Silva ◽  
Giana da Silveira Lima ◽  
Neftalí Lenin Villarreal Carreño ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Film Thickness ◽  
Cell Viability ◽  
Water Solubility ◽  
Setting Time ◽  
Mineral Trioxide Aggregate ◽  
Biological Properties ◽  
High Plasticity ◽  
Silicate Matrix ◽  
Time Flow

Introduction. Mineral Trioxide Aggregate (MTA) is a tricalcium-based silicate, dicalcium silicate matrix. Despite its good biologic properties, some clinicians still claim to have difficulties in handling MTA after its preparation due to its sandy consistency. The aim of the present study was to evaluate the physicochemical properties and cytotoxicity of MTA Repair HP (Angelus, Londrina, PR, Brazil) compared with MTA Angelus (Angelus, Londrina, PR, Brazil). Materials and Method. The properties assessed were particle size, setting time, flow, film thickness, radiopacity, water solubility, compressive strength, and cytotoxicity. Statistical analysis was performed considering p < 0.05 as statistically significant. Results. For radiopacity, water absorption and solubility MTA Repair HP were statistically similar to MTA Angelus. The MTA Angelus had statistically different film thickness values, higher than MTA Repair HP (p < 0.05). Besides, MTA Angelus showed a lower and statistically different compressive strength after 28 days than MTA Repair HP (p<0.05). Additionally, MTA Repair HP set more slowly (p < 0.05). Relative to cell viability, MTA Repair HP was statistically similar to MTA Angelus after 24 and 48 h in cell viability. Conclusions. The MTA Repair HP presented similar cell viability, lower film thickness, higher flow, setting time, and compressive strength values after 28 days than MTA Angelus. In general, the MTA Repair HP presented physicochemical and biological properties similar to the MTA Angelus.

scholarly journals Ytterbium Oxide as Radiopacifier of Calcium Silicate-Based Cements. Physicochemical and Biological Properties

2018 ◽  
Vol 29 (5) ◽  
pp. 452-458 ◽  
Author(s):  
Bernardo Cesar Costa ◽  
Juliane Maria Guerreiro-Tanomaru ◽  
Roberta Bosso-Martelo ◽  
Elisandra Márcia Rodrigues ◽  
Idomeo Bonetti-Filho ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Cell Viability ◽  
Calcium Silicate ◽  
Setting Time ◽  
Neutral Red ◽  
Biological Properties ◽  
Alizarin Red ◽  
Ytterbium Oxide ◽  
Physicochemical And Biological Properties ◽  
Bioactive Potential

Abstract This study evaluated physicochemical properties, cytotoxicity and bioactivity of MTA Angelus (MTA), calcium silicate-based cement (CSC) and CSC with 30% Ytterbium oxide (CSC/Yb2O3). Setting time was evaluated using Gilmore needles. Compressive strength was evaluated in a mechanical machine. Radiopacity was evaluated using radiographs of materials and an aluminum scale. Solubility was evaluated after immersion in water. Cell viability was evaluated by means of MTT assay and neutral red staining, and the mineralization activity by using alkaline phosphatase activity and Alizarin Red staining. The data were submitted to ANOVA, Tukey and Bonferroni tests (5% significance). The bioactive potential was evaluated by scanning electron microscopy. The materials presented similar setting time. MTA showed the lowest compressive strength. MTA and CSC/Yb2O3 presented similar radiopacity. CSC/Yb2O3 showed low solubility. Saos-2 cell viability tests showed no cytotoxic effect, except to 1:1 dilution in NR assay which had lower cell viability when compared to the control. ALP at 1 and 7 days was similar to the control. MTA and CSC had greater ALP activity at 3 days when compared to control. All the materials present higher mineralized nodules when compared with the control. SEM analysis showed structures suggesting the presence of calcium phosphate on the surface of materials demonstrating bioactivity. Ytterbium oxide proved to be a properly radiopacifying agent for calcium silicate-based cement since it did not affected the physicochemical and biological properties besides preserving the bioactive potential of this material.

scholarly journals Effect of Silver Nanoparticles on Physicochemical and Antibacterial Properties of Calcium Silicate Cements

2016 ◽  
Vol 27 (5) ◽  
pp. 508-514 ◽  
Author(s):  
Fernando Vazquez-Garcia ◽  
◽  
Mário Tanomaru-Filho ◽  
Gisselle Moraima Chávez-Andrade ◽  
Roberta Bosso-Martelo ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Silver Nanoparticles ◽  
Compressive Strength ◽  
Antibacterial Activity ◽  
Calcium Silicate ◽  
Setting Time ◽  
Antibacterial Properties ◽  
Mineral Trioxide Aggregate ◽  
Biological Properties ◽  
Calcium Silicate Cements

Abstract Mineral trioxide aggregate (MTA) and Portland cement (PC) are calcium silicate cements. They have similar physicochemical, mechanical and biological properties. The addition of zirconium oxide (ZrO2) to PC provides radiopacity. Silver nanoparticles (AgNPs) may improve some properties of cements. The aim of this study was to evaluate the effect of AgNPs on physicochemical/mechanical properties and antibacterial activity of white MTA (WMTA) and PC associated with ZrO2. The following materials were evaluated: WMTA; PC 70% + ZrO2 30%; WMTA+ AgNPs; and PC 70% + ZrO2 30% + AgNPs. The study evaluated radiopacity, setting time, pH, compressive strength and solubility. For radiopacity analysis, radiographs were made alongside an aluminum (Al) step wedge. To evaluate the antibacterial activity, direct contact test was performed on planktonic cells and Enterococcus faecalis biofilm induced on bovine root dentin for 14 days. The experimental periods were 5 and 15 h. Data were obtained as CFU mL-1. The obtained data were submitted to ANOVA and Tukey tests (p<0.05). The addition of AgNPs to WMTA increased the pH, lowered the solubility and the initial and final setting times. The addition of AgNPs to PC/ZrO2 maintained the pH, lowered the solubility, and increased the setting time and compressive strength. The radiopacity of all materials was higher than 4 mmAl. The addition of AgNPs promoted an increase in antibacterial activity for calcium silicate cements and favored the physicochemical and mechanical properties of the materials.

scholarly journals Preparation and Physicochemical Evaluation of Paste-Paste Calcium Hydroxide Based Dental Cement and the Effect of Replacement of Glycol Disalicylate by Methyl Salicylate on its Basic Properties

2012 ◽  
Vol 21 (3) ◽  
pp. 096369351202100
Author(s):  
Nader Nezafati ◽  
Saeed Hesaraki ◽  
Mostafa Shahrezaee
Keyword(s):  
Compressive Strength ◽  
Calcium Hydroxide ◽  
Methyl Salicylate ◽  
Water Solubility ◽  
Setting Time ◽  
Barium Sulphate ◽  
Biological Properties ◽  
Zinc Stearate ◽  
Dental Cement ◽  
Reparative Dentin

Dycal® is a paste-paste calcium hydroxide dental cement uses as pulp capping and liner in dentistry. First paste (base paste) contains titanium dioxide and barium sulphate in glycol disalicylate and second paste (catalyst paste) contains calcium hydroxide, zinc oxide and zinc stearate in ethyl toluene sulphonamide. Equal amounts of base and catalyst paste were mixed together and a hard mass is obtained after a certain time. The set material consists of TiO2, ZnO (fillers), BaSO4 (radiopacifier) and free unreacted Ca(OH)2 dispersed in an amorphous calcium phenolate matrix. This unreacted calcium hydroxide is responsible for biological properties of Dycal® (antibacterial and formation of reparative dentin). In this research Dycal® has been fabricated and furthermore glycol disalicylate was gradually replaced by methyl salicylate up to 20 % in base paste. Cements were characterized by X-ray diffraction (XRD) and Fourier transform infra-red (FTIR) and scanning electron microscopy (SEM). Also effect of the replacement was investigated on setting time, water solubility, pH and compressive strength of the cement. Results showed that unreacted calcium hydroxide decreased in set cement when methyl salicylate increase in base paste and therefore, and pH of distilled water containing cement decrease by this replacement. Setting time and water solubility also decreased when methyl salicylate increased in base paste (from 5.5 to 3 min and 4.5% to 2.5% respectively). The compressive strength showed no changes by this replacement.

scholarly journals Physico-Chemical Investigation of Endodontic Sealers Exposed to Simulated Intracanal Heat Application: Hydraulic Calcium Silicate-Based Sealers

Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 728
Author(s):  
David Donnermeyer ◽  
Magdalena Ibing ◽  
Sebastian Bürklein ◽  
Iris Weber ◽  
Maximilian P. Reitze ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Thermal Treatment ◽  
Film Thickness ◽  
Physical Properties ◽  
Calcium Silicate ◽  
Setting Time ◽  
Chemical Properties ◽  
Chemical Changes ◽  
Time Flow ◽  
Heat Application

The aim of this study was to gain information about the effect of thermal treatment of calcium silicate-based sealers. BioRoot RCS (BR), Total Fill BC Sealer (TFBC), and Total Fill BC Sealer HiFlow (TFHF) were exposed to thermal treatment at 37 °C, 47 °C, 57 °C, 67 °C, 77 °C, 87 °C and 97 °C for 30 s. Heat treatment at 97 °C was performed for 60 and 180 s to simulate inappropriate application of warm obturation techniques. Thereafter, specimens were cooled to 37 °C and physical properties (setting time/flow/film thickness according to ISO 6876) were evaluated. Chemical properties (Fourier-transform infrared spectroscopy) were assessed after incubation of the specimens in an incubator at 37 °C and 100% humidity for 8 weeks. Statistical analysis of physical properties was performed using the Kruskal-Wallis-Test (P = 0.05). The setting time, flow, and film thickness of TFBC and TFHF were not relevantly influenced by thermal treatment. Setting time of BR decreased slightly when temperature of heat application increased from 37 °C to 77 °C (P < 0.05). Further heat treatment of BR above 77 °C led to an immediate setting. FT-IR spectroscopy did not reveal any chemical changes for either sealers. Thermal treatment did not lead to any substantial chemical changes at all temperature levels, while physical properties of BR were compromised by heating. TFBC and TFHF can be considered suitable for warm obturation techniques.

scholarly journals Development of a Zero-Cement Binder Using Slag, Fly Ash, and Rice Husk Ash with Chemical Activator

2015 ◽  
Vol 2015 ◽  
pp. 1-14 ◽  
Author(s):  
M. R. Karim ◽  
M. F. M. Zain ◽  
M. Jamil ◽  
F. C. Lai
Keyword(s):  
Compressive Strength ◽  
Fly Ash ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Setting Time ◽  
Time Flow ◽  
Alumina Gel ◽  
Cement Binder ◽  
Increasing Demand ◽  
Chemical Activator

The increasing demand and consumption of cement have necessitated the use of slag, fly ash, rice husk ash (RHA), and so forth as a supplement of cement in concrete construction. The aim of the study is to develop a zero-cement binder (Z-Cem) using slag, fly ash, and RHA combined with chemical activator. NaOH, Ca(OH)2, and KOH were used in varying weights and molar concentrations. Z-Cem was tested for its consistency, setting time, flow, compressive strength, XRD, SEM, and FTIR. The consistency and setting time of the Z-Cem paste increase with increasing RHA content. The Z-Cem mortar requires more superplasticizer to maintain a constant flow of110±5% compared with OPC. The compressive strength of the Z-Cem mortar is significantly influenced by the amounts, types, and molar concentration of the activators. The Z-Cem mortar achieves a compressive strength of 42–44 MPa at 28 days with 5% NaOH or at 2.5 molar concentrations. The FTIR results reveal that molecules in the Z-Cem mortar have a silica-hydrate (Si-H) bond with sodium or other inorganic metals (i.e., sodium/calcium-silica-hydrate-alumina gel). Therefore, Z-Cem could be developed using the aforementioned materials with the chemical activator.

scholarly journals Brushite cement containing gelatin: evaluation of mechanical strength and in vitro degradation

Cerâmica ◽  
2019 ◽  
Vol 65 (374) ◽  
pp. 261-266 ◽  
Author(s):  
L. P. Silva ◽  
M. D. P. Ribeiro ◽  
E. S. Trichês ◽  
M. Motisuke
Keyword(s):  
Mechanical Properties ◽  
Weight Loss ◽  
Compressive Strength ◽  
Solid Phase ◽  
Setting Time ◽  
Biological Properties ◽  
Solubility In Water ◽  
Ringer’S Solution ◽  
Weight Loss Data

Abstract Calcium phosphate cements (CPCs) are potential materials for repairing bone defects, mainly due to their excellent biocompatibility and osteoconductivity. Nevertheless, their low mechanical properties limit their usage in clinical applications. The gelatin addition may improve the mechanical and biological properties of CPCs, but their solubility in water may increase the porosity of the cement during degradation. Thus, the aim of this work was to investigate the influence of gelatin on the setting time, compressive strength and degradation rate of a brushite cement. CPCs were prepared with the addition of 0, 5, 10 and 20 wt% of gelatin powder in the solid phase of the cement. The results indicated that the setting time increased with gelatin. Furthermore, cement with 20 wt% of gelatin had an initial compressive strength of 14.1±1.8 MPa while cement without gelatin had 4.5±1.2 MPa. The weight loss, morphology and compressive strength were evaluated after degradation in Ringer’s solution. According to the weight loss data, gelatin was eliminated of samples during degradation. It was concluded that the presence of gelatin improved CPCs mechanical properties; however, as degradation in Ringer’s solution evolved, cement compressive strength decreased due to gelatin dissolution and, consequently, an increase in sample porosity.

scholarly journals Effect of Rice Husk Ash (RHA) and Slag as Partial Replacement of Cement on Reinforced Concrete Slabs

2021 ◽  
pp. 34-40
Author(s):  
Mohamed Nabil ◽  
Ashraf Essa ◽  
Magdy Mahmoud ◽  
Mohamed Rabah
Keyword(s):  
Compressive Strength ◽  
Rice Husk ◽  
Rice Husk Ash ◽  
Setting Time ◽  
Partial Replacement ◽  
Reinforced Concrete Slabs ◽  
Time Flow ◽  
Increasing Demand ◽  
Relationship Of ◽  
Compressive Tests

The increasing demand and consumption of cement have necessitated the use of slag, fly ash, rice husk ash (RHA), and so forth as a supplement of cement in concrete construction. The aim of the study is to develop a replacement of the cement with rice husk ash and slag combined with chemical activator. NaOH, Ca(OH)2, and KOH were used in varying weights and molar concentrations. Partial replacement of cement was tested for its consistency, setting time, flow, compressive strength, and fire. The consistency and setting time of the Partial Z-Cement (Zero cement) paste increase with increasing RHA content. The replacement of cement mortar achieves a compressive strength of 22–25MPa at  28 days with 5% NaOH or at 2.5or non used activator molar concentrations. The tested slabs were made of concrete and reinforced with bars with 10 mm diameter having and compressive strength evaluated from the compressive tests. The analysis of the slab deflection behavior has been presented after fire of samples. The results show the different character of the load-deflection relationship of a replacement of the cement with rice husk ash and slag reinforced slabs compared to traditionally reinforced slabs.  

scholarly journals Effect of bioactive glass addition on the physical properties of mineral trioxide aggregate

2021 ◽  
Vol 25 (1) ◽  
Author(s):  
Jei Kim ◽  
Hyun-Jung Kim ◽  
Seok Woo Chang ◽  
Soram Oh ◽  
Sun-Young Kim ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Bond Strength ◽  
Physical Properties ◽  
Bioactive Glass ◽  
Body Fluid ◽  
Setting Time ◽  
Mineral Trioxide Aggregate ◽  
Xrd Analysis ◽  
Control Group ◽  
Push Out

Abstract Background The addition of bioactive glass (BG), a highly bioactive material with remineralization potential, might improve the drawback of weakening property of mineral trioxide aggregates (MTA) when it encounters with body fluid. This study aims to evaluate the effect of BG addition on physical properties of MTA. Methods ProRoot (MTA), and MTA with various concentrations of BG (1, 2, 5 and 10% BG/MTA) were prepared. Simulated body fluid (SBF) was used to investigate the effect of the storage solution on dentin remineralization. Prepared specimens were examined as following; the push-out bond strength to dentin, compressive strength, setting time solubility and X-ray diffraction (XRD) analysis. Results The 2% BG/MTA showed higher push-out bond strengths than control group after 7 days of SBF storage. The 2% BG/MTA exhibited the highest compressive strength. Setting times were reduced in the 1 and 2% BG/MTA groups, and solubility of all experimental groups were clinically acceptable. In all groups, precipitates were observed in dentinal tubules via SEM. XRD showed the increased hydroxyapatite peaks in the 2, 5 and 10% BG/MTA groups. Conclusion It was verified that the BG-added MTA increased dentin push-out bond strength and compressive strength under SBF storage. The addition of BG did not negatively affect the MTA maturation reaction; it increased the amount of hydroxyapatite during SBF maturation.

scholarly journals A Silk Fibroin Based Hydration Accelerator for Root Canal Filling Materials

Polymers ◽  
2020 ◽  
Vol 12 (4) ◽  
pp. 994
Author(s):  
Ching-Shuan Huang ◽  
Sung-Chih Hsieh ◽  
Nai-Chia Teng ◽  
Wei-Fang Lee ◽  
Poonam Negi ◽  
...  
Keyword(s):  
Cell Viability ◽  
Silk Fibroin ◽  
Root Canal ◽  
Setting Time ◽  
Testing Machine ◽  
Mineral Trioxide Aggregate ◽  
Filling Material ◽  
Root Canal Filling ◽  
Initial Setting Time

Mineral trioxide aggregate (MTA) is widely used in various dental endodontic applications such as root-end filling, furcal perforation repair, and vital pulp therapy. In spite of many attempts to improve handling properties and reduce the discoloration of MTA, the ideal root canal filling material has yet to be fully developed. The objective of this study was to investigate the setting time, mechanical properties, and biocompatibility of MTA set by a silk fibroin solution. A 5 wt% silk fibroin (SF) solution (a novel hydration accelerant) was used to set SavDen® MTA and ProRoot® white MTA (WMTA). Changes in setting time, diametral tensile strength (DTS), material crystallization, in vitro cell viability, and cell morphology were assessed by Vicat needle measurement, a universal testing machine, scanning electron microscopy (SEM), and WST-1 assay, respectively. The initial setting time of ProRoot® MTA and SavDen® MTA experienced a drastic decrease of 83.9% and 42.1% when deionized water was replaced by 5 wt% SF solution as the liquid phase. The DTS of SavDen® MTA showed a significant increase after set by the SF solution in 24 h. A human osteoblast-like cell (MG-63)-based WST-1 assay revealed that both ProRoot® MTA and SavDen® MTA hydrated using SF solution did not significantly differ (p > 0.05) in cell viability. MG-63 cells with pseudopodia attachments and nuclear protrusions represent a healthier and more adherent status on the surface of MTA when set with SF solution. The results suggest that the 5 wt% SF solution may be used as an alternative hydration accelerant for MTA in endodontic applications.

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