scholarly journals Biocompatibility and Surface Characteristics of Resin-Modified Glass Ionomer Cements with Ammonium Quaternary Compounds or Silver Nanoparticles: AnIn VitroStudy

2018 ◽  
Vol 2018 ◽  
pp. 1-13 ◽  
Author(s):  
Silvia Munguía-Moreno ◽  
Gabriel-Alejandro Martínez-Castañón ◽  
Nuria Patiño-Marín ◽  
Claudio Cabral-Romero ◽  
Norma-Verónica Zavala-Alonso

Glass ionomer cements are materials with diverse clinical applications. Its use is indicated in patients with special needs, pediatric patients, and the elderly; accordingly, it is important to know its properties. The aim of the present study was to determine the cytotoxicity, surface roughness, microhardness, and surface characteristics of GC Fuji ORTHO LC and GC Fuji PLUS resin-modified glass ionomer cements (RMGICs) with 1 and 2% of benzalkonium chloride, cetylpyridinium chloride, hexadecyltrimethylammonium bromide, or silver nanoparticles. All the experimental groups increase or decrease statistically significantly the VHN (P<0.05) compared with the control group, except for GC Fuji PLUS added with hexadecyltrimethylammonium bromide 1 wt%. In the same way, all groups show a statistically significant (P<0.05) increase or decrease in Ra compared with the control group except for GC Fuji ORTHO added with benzalkonium chloride 2 wt%, GC Fuji PLUS added with benzalkonium chloride 2 wt%, and GC Fuji PLUS added with cetylpyridinium chloride 2 wt%. The SEM micrographs show similar surface images between the control and experimental groups. When a dental material is modified, it is important to reevaluate its biological and mechanical characteristics. In the present study, all the additions modified the cytotoxicity and surface characteristics of RMGICs, by increasing or decreasing these properties.

Author(s):  
Marzieh Moradian ◽  
Mohsen Nosrat Abadi ◽  
Dana Jafarpour ◽  
Maryam Saadat

Abstract Objectives The purpose of this study was to evaluate the effect of bacterial cellulose nanocrystals (BCNCs) on the mechanical properties of resin-modified glass ionomer cements (RMGICs) including compressive strength (CS), diametral tensile strength (DTS), and modulus of elasticity (E). Materials and Methods BCNCs were incorporated into RMGIC at various concentrations (0.3, 0.5, and 1 wt%). Unmodified RMGIC was used as the control group. The specimens were stored in distilled water at 37°C for 24 hours. CS and DTS, as well as modulus of elasticity, were evaluated using a universal testing machine. The nanostructure of BCNCs was observed via field emission scanning electron microscopy. Statistical Analysis One-way analysis of variance and post-hoc Tukey tests were used for data analysis. Level of significance was at p < 0.05. Results The addition of BCNCs to RMGIC led to an increase in all of the tested mechanical properties compared with the control group, with a significant increase observed for 1 wt% BCNC. CS and DTS improved up to 23%, and modulus of elasticity increased by 44%. Conclusions The addition of BCNCs to the RMGIC improved the mechanical properties, including CS, elastic modulus, and DTS. Thus, the newly developed RMGICs with BCNCs might represent an ideal and promising novel dental material in restorative dentistry.


2016 ◽  
Vol 10 (1) ◽  
pp. 58-68 ◽  
Author(s):  
Júlio C. M. Souza ◽  
Joel B. Silva ◽  
Andrea Aladim ◽  
Oscar Carvalho ◽  
Rubens M. Nascimento ◽  
...  

Background: Glass-ionomer cements perform a protective effect on the dentin-pulp complex considering the F ions release and chemical bonding to the dental structures. On the other hand, those materials have poor physic-mechanical properties in comparison with the restorative resin composite. The main aim of this work was to evaluate the influence of zirconia and/or alumina fillers on the microstructure and strength of a resin modified glass-ionomer cement after thermal cycling. Methods: An in vitro experimental study was carried out on 9 groups (n = 10) of cylindrical samples (6 x 4 mm) made from resin modified glass-ionomer (Vitremer, 3M, USA) with different contents of alumina and/or zirconia fillers. A nano-hybrid resin composite was tested as a control group. Samples were mechanically characterized by axial compressive tests and electron scanning microscopy (SEM) coupled to energy dispersive X-ray spectrophotometry (EDS), before and after thermal cycling. Thermal cycling procedures were performed at 3000, 6000 and 10000 cycles in Fusayama´s artificial saliva at 5 and 60 oC. Results: An improvement of compressive strength was noticed on glass-ionomer reinforced with alumina fillers in comparison with the commercial glass ionomer. SEM images revealed the morphology and distribution of alumina or zirconia in the microstructure of glass-ionomers. Also, defects such as cracks and pores were detected on the glass-ionomer cements. The materials tested were not affected by thermal cycling in artificial saliva. Conclusion: Addition of inorganic particles at nano-scale such as alumina can increase the mechanical properties of glass-ionomer cements. However, the presence of cracks and pores present in glass-ionomer can negatively affect the mechanical properties of the material because they are areas of stress concentration.


2021 ◽  
Author(s):  
Zuleikha Malik ◽  
Danial Qasim Butt ◽  
Zainab Qasim Butt ◽  
Nawshad Muhammad ◽  
Muhammad Kaleem ◽  
...  

Author(s):  
PC Siqueira ◽  
APR Magalhaes ◽  
WC Carvalho-Pires ◽  
FC Pereira ◽  
EP Silveira-Lacerda ◽  
...  

2015 ◽  
Vol 63 (4) ◽  
pp. 383-388
Author(s):  
Luísa Bandeira Pires Monteiro LOPES ◽  
Andreia Sofia Lopes de ARAÚJO ◽  
Virginia Barreiros MILAGRE

Objective: To quantify the color variation of two glass ionomer cements and a composite resin used in pediatric dentistry, after being immersed in different pigments agents. Methods: Using two glass ionomer cements (Ketac(tm) Molar and Photac(tm) Fil) and a microhybrid composite resin (Filtek(tm) z250), were produced 40 disks of each material (10 mm in diameter and 2 mm thick). The samples were soaked in artificial saliva (control group), coke, peach Ice Tea(r) and chocolate milk, for 72 hours in an oven at 37ºC. After this period, the samples were washed in 50 ml of distilled water. Finally, using the spectrophotometer, it was made the reading of results. The color change was measured according to the CIE L * a * b * system. Color changes were statistically analyzed using parametric one-way ANOVA and ANOVA with Welch correction, the nonparametric Kruskal-Wallis tests and post-hoc Tukey and Dunnet T3 with p≤ 0.05. Results: The immersion of restorative materials in different pigmentation agents caused a significant color variation on the samples. The agent who presented higher results was the Peach Ice Tea(r). The chocolate milk was the fluid with lowest pigmentation capacity of all restorative materials under study. The greater color variation was found on the Ketac(tm) Molar submerged in Coca-Cola(r) and the smallest on the Filtek(tm) z250 in chocolate milk. Conclusion: All restorative materials were shown to be susceptible to pigmentation by all agents. The Filtek(tm) z250 proved to have better color stability, followed by Photac(tm) Fil and finally by Ketac(tm) Molar.


2012 ◽  
Vol 17 (6) ◽  
pp. 154-159 ◽  
Author(s):  
Marcel M. Farret ◽  
Eduardo Martinelli de Lima ◽  
Eduardo Gonçalves Mota ◽  
Hugo Mitsuo S. Oshima ◽  
Gabriela Maguilnik ◽  
...  

OBJECTIVE: To evaluate the mechanical properties of three glass ionomers cements (GICs) used for band cementation in Orthodontics. METHODS: Two conventional glass ionomers (Ketac Cem Easy mix/3M-ESPE and Meron/Voco) and one resin modified glass ionomer (Multi-cure Glass ionomer/3M-Unitek) were selected. For the compressive strength and diametral tensile strength tests, 12 specimens were made of each material. For the microhardness test 15 specimens were made of each material and for the shear bond strength tests 45 bovine permanent incisors were used mounted in a self-cure acrylic resin. Then, band segments with a welded bracket were cemented on the buccal surface of the crowns. For the mechanical tests of compressive and diametral tensile strength and shear bond strength a universal testing machine was used with a crosshead speed of 1,0 mm/min and for the Vickers microhardness analysis tests a Microdurometer was used with 200 g of load during 15 seconds. The results were submitted to statistical analysis through ANOVA complemented by Tukey's test at a significance level of 5%. RESULTS: The results shown that the Multi-Cure Glass Ionomer presented higher diametral tensile strength (p < 0.01) and compressive strength greater than conventional GICs (p = 0.08). Moreover, Ketac Cem showed significant less microhardness (p < 0.01). CONCLUSION: The resin-modified glass ionomer cement showed high mechanical properties, compared to the conventional glass ionomer cements, which had few differences between them.


2004 ◽  
Vol 12 (1) ◽  
pp. 12-17 ◽  
Author(s):  
Linda Wang ◽  
Marília Afonso Rabelo Buzalaf ◽  
Maria Teresa Atta

A dhesive systems associated to resin-modified glass ionomer cements are employed for the achievement of a higher bond strength to dentin. Despite this benefit, other properties should not be damaged. This study aimed at evaluating the short-time fluoride release of a resin-modified glass ionomer cement coated with two one-bottle adhesive systems in a pH cycling system. Four combinations were investigated: G1: Vitremer (V); G2: Vitremer + Primer (VP); G3: Vitremer + Single Bond (VSB) and G4: Vitremer + Prime & Bond 2.1 (VPB). SB is a fluoride-free and PB is a fluoride-containing system. After preparation of the Vitremer specimens, two coats of the selected adhesive system were carefully applied and light-cured. Specimens were immersed in demineralizing solution for 6 hours followed by immersion in remineralizing solution for 18 hours, totalizing the 15-day cycle. All groups released fluoride in a similar pattern, with a greater release in the beginning and decreasing with time. VP showed the greatest fluoride release, followed by V, with no statistical difference. VSB and VPB released less fluoride compared to V and VP, with statistical difference. Regardless the one-bottle adhesive system, application of coating decreased the fluoride release from the resin-modified glass ionomer cements. This suggests that this combination would reduce the beneficial effect of the restorative material to the walls around the restoration.


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