scholarly journals Effect of Freeze-Thaw Cycles on the Internal Structure and Performance of Semirigid Base Materials

2017 ◽  
Vol 2017 ◽  
pp. 1-18 ◽  
Author(s):  
Yiqi Wang ◽  
Yiqiu Tan ◽  
Meng Guo ◽  
Xinglong Wang
Keyword(s):  
Cement Content ◽  
Strength Loss ◽  
Spatial Distributions ◽  
Loss Ratio ◽  
Curing Time ◽  
X Ray ◽  
Freeze Thaw ◽  
Base Materials ◽  
Internal Structures ◽  
Void Area

In this study, we investigate the spatial distributions of the internal structures in semirigid base materials (SRBMs) and explore their effect on the service performance of the SRBMs. X-ray computed tomography (X-ray CT) was used to conduct a spatial voids structure analysis. Three variates were selected to study the factors influencing the spatial distributions of the internal structures, including freeze-thaw cycles, curing time, and cement content. The results show that, with the increase in the number of freezing and thawing cycles, the average porosity, void area, and void number of the SRBM samples increased, and the average void diameters of all samples initially increased and then decreased. These trends led to an increase in the mass loss ratio and strength loss ratio. Increasing the cement content and extending the curing time decreased the average number of voids, average void area, and average void diameter and decreased the mass loss ratio and strength loss ratio of the SRBMs. The top and bottom of the SRBM samples were more porous than the middle of the samples, whereas the maximum value of the average void diameter was observed in the middle of the samples.

scholarly journals Standardization of Fatigue Characteristics of Cement-Treated Aggregate Base Materials under Different Stress States

2018 ◽  
Vol 8 (9) ◽  
pp. 1500 ◽  
Author(s):  
Jiawei Xie ◽  
Limin Tang ◽  
Songtao Lv ◽  
Naitian Zhang ◽  
Tuo Huang ◽  
...  
Keyword(s):  
Fatigue Life ◽  
Weibull Distribution ◽  
Interval Analysis ◽  
Cement Content ◽  
Curing Time ◽  
Base Materials ◽  
Test Conditions ◽  
Fatigue Characteristics ◽  
Stress States ◽  
Aggregate Base

In this study, to decrease the evaluation uncertainty of the fatigue characteristics of cement-treated aggregate base materials under different test conditions, unconfined compressive, indirect tensile, flexural tensile strength tests and fatigue tests of these base materials with different cement content and at different curing times were carried out. The Weibull distribution was employed to analyze fatigue test results. The standardization model of fatigue characteristics for cement-treated aggregate base materials under different stress states was established. Based on the interval analysis theory, the fatigue characteristic model under different stress states was established using interval parameters. Results revealed that the curing time and cement content considerably affect the strength and fatigue characteristics of cement-treated aggregate base materials, and with increasing cement content and curing time, the fatigue resistance of cement-treated aggregate base materials can be improved. Clear differences between the fitting parameters a and b of the S-N fatigue equation of cement-treated aggregate base materials under different stress states were observed, which can be eliminated by using the analysis method based on the Weibull distribution and the standardization model, and a unified expression for the cement-treated aggregate base materials under different test conditions was realized. A Standardization model of fatigue characteristics based on the interval analysis new method could solve several problems such as inadequate sampling representation, low precision, and insufficient stability of test equipment; thus, the errors caused by materials, structures, the environment, and loads can be reduced, making the fatigue life interval more reasonable and scientific compared to the point numerical fatigue life. Regression parameters a and be were in intervals [9.0, 10.6] and [9.9, 11.3], respectively, and parameters a and b were similar, which improve the test accuracy and reduce the data error.

scholarly journals Principles of Different X-ray Phase-Contrast Imaging: A Review

2021 ◽  
Vol 11 (7) ◽  
pp. 2971
Author(s):  
Siwei Tao ◽  
Congxiao He ◽  
Xiang Hao ◽  
Cuifang Kuang ◽  
Xu Liu
Keyword(s):  
Biological Samples ◽  
Phase Contrast ◽  
Recent Progress ◽  
Phase Contrast Imaging ◽  
Contrast Imaging ◽  
X Ray ◽  
X Ray Imaging ◽  
Internal Structures ◽  
X Ray Absorption ◽  
Made In

Numerous advances have been made in X-ray technology in recent years. X-ray imaging plays an important role in the nondestructive exploration of the internal structures of objects. However, the contrast of X-ray absorption images remains low, especially for materials with low atomic numbers, such as biological samples. X-ray phase-contrast images have an intrinsically higher contrast than absorption images. In this review, the principles, milestones, and recent progress of X-ray phase-contrast imaging methods are demonstrated. In addition, prospective applications are presented.

scholarly journals Freeze–Thaw Resistance and Air-Void Analysis of Concrete with Recycled Glass–Pozzolan Using X-ray Micro-Tomography

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 154
Author(s):  
Marija Krstic ◽  
Julio F. Davalos ◽  
Emanuele Rossi ◽  
Stefan C. Figueiredo ◽  
Oguzhan Copuroglu
Keyword(s):  
Fly Ash ◽  
Pore Structure ◽  
The United States ◽  
Adsorption Method ◽  
X Ray ◽  
Freeze Thaw ◽  
Void System ◽  
Spatial Parameters ◽  
Micro Tomography ◽  
Air Void

Recent studies have shown promising potential for using Glass Pozzolan (GP) as an alternative supplementary cementitious material (SCM) due to the scarcity of fly ash and slag in the United States. However, comprehensive studies on the freeze–thaw (FT) resistance and air void system of mixtures containing GP are lacking. Therefore, this study aimed to evaluate GP’s effect on FT resistance and characterize mixtures with different GP contents, both macro- and microscopically. In this study, six concrete mixes were considered: Three mixes with 20%, 30% and 40% GP as cement replacements and two other comparable mixes with 30% fly ash and 40% slag, as well as a mix with 100% Ordinary Portland cement (OPC) as a reference. Concrete samples were prepared, cured and tested according to the ASTM standards for accelerated FT resistance for 1000 cycles and corresponding dynamic modulus of elasticity (Ed). All the samples showed minimal deterioration and scaling and high F/T resistance with a durability factor of over 90%. The relationships among FT resistance parameters, air-pressured method measurements of fresh concretes and air void analysis parameters of hardened concretes were examined in this study. X-ray micro-tomography (micro-CT scan) was used to evaluate micro-cracks development after 1000 freeze–thaw cycles and to determine spatial parameters of air voids in the concretes. Pore structure properties obtained from mercury intrusion porosimetry (MIP) and N2 adsorption method showed refined pore structure for higher cement replacement with GP, indicating more gel formation (C-S-H) which was verified by thermogravimetric analysis (TGA).

Twin memory and twin amnesia in anorthoclase

2000 ◽  
Vol 64 (2) ◽  
pp. 195-200 ◽  
Author(s):  
S. A. Hayward ◽  
E. K. H. Salje
Keyword(s):  
Phase Transitions ◽  
Transition Temperature ◽  
Alkali Feldspar ◽  
Spatial Distributions ◽  
X Ray Diffraction ◽  
Alkali Cations ◽  
X Ray ◽  
Natural Minerals ◽  
Synthetic Materials ◽  
Before And After

AbstractMany natural minerals and synthetic materials display twin microstructures resulting from displacive phase transitions. These microstructures may be removed temporarily from the sample by heating above the relevant transition temperature, though the twinning generally returns on subsequent cooling.In anorthoclase, the spatial distributions of twins before and after brief annealing above TC are often identical. This property appears to be a common feature in many materials which undergo ferroelastic phase transitions, and is known as ‘twin memory’. The atomic mechanisms responsible for this twin memory may be investigated by studying the annealing regimes required to remove the memory effect; how long must a sample be annealed, and at what temperature, to induce ‘twin amnesia’.High-resolution X-ray diffraction (XRD) has been used to investigate twin memory and twin amnesia in anorthoclase. In anorthoclase, the primary constraint on twin amnesia is thermodynamic, rather than kinetic. The critical temperature to induce amnesia correlates well with the top of the (Na, K) solvus in disordered alkali feldspar. For this reason, the proposed mechanism for twin memory involves the segregation of alkali cations in thin lamellae at the twin boundaries.

The Limitation of Evaluating Thermal Shock Resistance of Al2O3-SiO2 Refractory by Measuring Strength Loss Rate

2011 ◽  
Vol 295-297 ◽  
pp. 2309-2313
Author(s):  
Xin Liu ◽  
Dian Li Qu ◽  
Zhi Jian Li
Keyword(s):  
Thermal Shock ◽  
Thermal Shock Resistance ◽  
Loss Rate ◽  
Strength Loss ◽  
X Ray Diffraction ◽  
Initial State ◽  
X Ray ◽  
Cold Crushing Strength ◽  
Shock Experiment ◽  
Shock Resistance

This paper deeply studied the limitation of evaluating the thermal shock resistance of Al2O3-SiO2 refractory by measuring Strength Loss Rate (SLR). By means of supersonic, X-ray diffraction (XRD), the results were drawn as followed.1)After the thermal shock experiment for mullite based A-S refractory, which were composed by mullite and corundum, the supersonic velocity slowed down as it going through the sample while the cold crushing strength abnormally increased at initial state.2) The strength increased remarkably with the ascending of mullite fraction.3)It is inadequate to evaluate the thermal shock resistance of mullite based A-S refractory by strength loss rate.

scholarly journals Volume change behaviour and microstructure of stabilized loess under cyclic freeze–thaw conditions

2016 ◽  
Vol 43 (10) ◽  
pp. 865-874 ◽  
Author(s):  
Sheng-lin Wang ◽  
Qing-feng Lv ◽  
Hassan Baaj ◽  
Xiao-yuan Li ◽  
Yan-xu Zhao
Keyword(s):  
Fly Ash ◽  
Volume Change ◽  
Cement Content ◽  
Frost Heave ◽  
Equivalent Diameter ◽  
Surface Porosity ◽  
Change Rate ◽  
Freeze Thaw ◽  
Significant Damage ◽  
The Impact

Freeze–thaw action is considered to be one of the most destructive actions that can induce significant damage in stabilized subgrades in seasonally frozen loess areas. Laboratory tests including frost heave – thaw shrinkage and microstructure change during freeze–thaw cycles were conducted to evaluate the volume change rate of loess stabilized with cement, lime, and fly ash under the impact of cyclic freeze–thaw conditions. The loess specimens collapsed after eight freeze–thaw cycles (192 h), but most stabilized loess specimens had no visible damage after all freeze–thaw cycles were completed. All of the stabilized loess samples underwent a much smaller volume change than the loess alone after the freeze–thaw cycles. Although surface porosity and equivalent diameter of stabilized loess samples increased, the stabilized loess can retain its microstructure during freeze–thaw cycles when the cement content was less than 6%. To ensure freeze–thaw resistance of stabilized loess subgrades, the mix proportions of the three additives was recommended to be 4 to 5% cement, 6% lime, and 10% fly ash.

Surface Reactions of Metal Catalysts for Carbon Nanotubes on an Oxide Thin Layer/Si Substrates Studied by in-situ Micro X-ray Adsorption Spectroscopy using SPELEEM

2006 ◽  
Vol 967 ◽  
Author(s):  
Fumihiko Maeda ◽  
Hiroki Hibino ◽  
Satoru Suzuki ◽  
FangZhun Guo ◽  
Yoshio Watanabe
Keyword(s):  
Electron Microscopy ◽  
Oxide Layer ◽  
X Ray ◽  
Si Substrates ◽  
Microscopy Image ◽  
Special Surface ◽  
Void Area ◽  
Low Energy Electron ◽  
Photoemission Electron

ABSTRACTTo clarify the reaction process of Co and Fe with a oxide layer on Si substrates, the annealing processes were analyzed using spectroscopic photoemission and low-energy electron microscopy for a special surface where oxide areas and clean substrate areas (voids) coexist closely in a micrometer-order view. From analyses of XAS spectra and edge jump ratios obtained from the photoemission electron microscopy image, we clarified that Co atoms in the void area remain because of the formation of silicides, but that those on the oxide layer disappear because metallic Co atoms easily diffuse. In contrast, in the case of Fe, we found the formation of various silicides and their gradual diffusion into Si substrate even in the form of silicides.

scholarly journals Effect of Polypropylene Fiber on Frost Resistance of Cemented Soil

2019 ◽  
Vol 57 (2) ◽  
pp. 78-86
Author(s):  
Lina Xu ◽  
Lei Niu
Keyword(s):  
Frost Resistance ◽  
Polypropylene Fiber ◽  
High Strength ◽  
Strength Loss ◽  
Curing Time ◽  
Freezing And Thawing ◽  
Cemented Soil ◽  
Small Cracks ◽  
The Impact ◽  
Engineering Projects

Polypropylene fiber is widely used as a reinforcing material in composite materials of various engineering projects, because it has high strength and corrosion resistance. In this study, with the purpose of examine the impact of discrete polypropylene fiber on frost resistance of cemented soil, cemented soil treated with polypropylene fiber is used as the research sample. Firstly, the impact of curing time, fiber content and length on the strength of cemented soil has been considered. And then, the frost resistance characteristics of cemented soil reinforced by polypropylene fiber with the content of 0.5% have been investigated. The results show that with the development of curing time, the strength of cemented soil increases logarithmically. By adding an appropriate amount of polypropylene fiber, the strength of the specimen may be improved. In this study, cemented soil reinforced by polypropylene fiber 0.1% in content and 3 mm in length has the best reinforcement effect. After 21 cycles of freezing and thawing processes, a sharp decline in strength of cemented soil without fiber, and the strength loss ratio is up to 45%. There are cracks in the specimens, and some of the specimens have broken off. Differently, after 21 freeze-thaw cycles, the strength of the cemented soil with fiber decreased less, and the strength loss ratios are between 1 and 13%, and there are only small cracks on the surface of specimens. The results show that adding discrete polypropylene fiber is a suitable method to prevent the generation and development of internal cracks in the cemented soil during freezing and thawing, thereby improving the frost resistance. These results can be used as a reference for the application of cemented soil reinforced with fiber in seasonal frozen regions.

scholarly journals Synchrotron radiation X-ray tomographic microscopy (SRXTM) of brachiopod shell interiors for taxonomy: Preliminary report

2010 ◽  
pp. 109-117 ◽  
Author(s):  
Neda Motchurova-Dekova ◽  
David Harper
Keyword(s):  
Synchrotron Radiation ◽  
Three Dimensional ◽  
X Rays ◽  
X Ray ◽  
Fine Grained ◽  
Internal Structures ◽  
Efficient Alternative ◽  
Micro Tomography ◽  
Light Beams ◽  
Non Destructive

Synchrotron radiation X-ray tomographic microscopy (SRXTM) is a non-destructive technique for the investigation and visualization of the internal features of solid opaque objects, which allows reconstruction of a complete three-dimensional image of internal structures by recording of the differences in the effects on the passage of waves of energy reacting with those structures. Contrary to X-rays, produced in a conventional X-ray tube, the intense synchrotron light beams are sharply focused like a laser beam. We report encouraging results from the use of SRXTM for purely taxonomic purposes in brachiopods: an attempt to find a non-destructive and more efficient alternative to serial sectioning and several other methods of dissection together with the non-destructive method of X-ray computerised micro-tomography. Two brachiopod samples were investigated using SRXTM. In ?Rhynchonella? flustracea it was possible to visualise the 3D shape of the crura and dental plates. In Terebratulina imbricata it was possible to reveal the form of the brachidium. It is encouraging that we have obtained such promising results using SRXTM with our very first two fortuitous samples, which had respectively fine-grained limestone and marl as infilling sediment, in contrast to the discouraging results communicated to us by some colleagues who have tested specimens with such infillings using X-ray micro-tomography. In future the holotypes, rare museum specimens or delicate Recent material may be preferentially subjected to this mode of analysis.

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