scholarly journals In Situ Synthesis of Reduced Graphene Oxide-Reinforced Silicone-Acrylate Resin Composite Films Applied in Erosion Resistance

2015 ◽  
Vol 2015 ◽  
pp. 1-8 ◽  
Author(s):  
Yang Cao ◽  
Xiaoyong Tian ◽  
Yan Wang ◽  
Youyi Sun ◽  
Hailin Yu ◽  
...  

The reduced graphene oxide reinforced silicone-acrylate resin composite films (rGO/SAR composite films) were prepared by in situ synthesis method. The structure of rGO/SAR composite films was characterized by Raman spectrum, atomic force microscope, scanning electron microscopy, and thermogravimetric analyzer. The results showed that the rGO were uniformly dispersed in silicone-acrylate resin matrix. Furthermore, the effect of rGO loading on mechanical properties of composite films was investigated by bulge test. A significant enhancement (ca. 290% and 320%) in Young’s modulus and yield stress was obtained by adding the rGO to silicone-acrylate resin. At the same time, the adhesive energy between the composite films and metal substrate was also improved to be about 200%. Moreover, the erosion resistance of the composite films was also investigated as function of rGO loading. The rGO had great effect on the erosion resistance of the composite films, in which theRcorr(ca. 0.8 mm/year) of composite film was far lower than that (28.7 mm/year) of pure silicone-acrylate resin film. Thus, this approach provides a novel route to investigate mechanical stability of polymer composite films and improve erosion resistance of polymer coating, which are very important to be used in mechanical-corrosion coupling environments.

2020 ◽  
Vol 59 (1) ◽  
pp. 477-487 ◽  
Author(s):  
Zhuang Liu ◽  
Haiyang Fu ◽  
Bo Gao ◽  
Yixuan Wang ◽  
Kui Li ◽  
...  

AbstractThis paper studies in-situ synthesis of Fe2O3/reduced graphene oxide (rGO) anode materials by different hydrothermal process.Scanning Electron Microscopy (SEM) analysis has found that different processes can control the morphology of graphene and Fe2O3. The morphologies of Fe2O3 prepared by the hydrothermal in-situ and oleic acid-assisted hydrothermal in-situ methods are mainly composed of fine spheres, while PVP assists The thermal in-situ law presents porous ellipsoids. Graphene exhibits typical folds and small lumps. X-ray diffraction analysis (XRD) analysis results show that Fe2O3/reduced graphene oxide (rGO) is generated in different ways. Also, the material has good crystallinity, and the crystal form of the iron oxide has not been changed after adding GO. It has been reduced, and a characteristic peak appears around 25°, indicating that a large amount of reduced graphene exists. The results of the electrochemical performance tests have found that the active materials prepared in different processes have different effects on the cycle performance of lithium ion batteries. By comprehensive comparison for these three processes, the electro-chemical performance of the Fe2O3/rGO prepared by the oleic acid-assisted hydrothermal method is best.


2018 ◽  
Vol 3 (43) ◽  
pp. 12108-12112 ◽  
Author(s):  
Xiaoqing Liu ◽  
Dan Zhang ◽  
Guangshe Li ◽  
Chenglin Xue ◽  
Junfang Ding ◽  
...  

2021 ◽  
Vol 264 ◽  
pp. 114924
Author(s):  
Periyasami Gnanaprakasam ◽  
Aruchamy Gowrisankar ◽  
Shanmugam Senthilkumar ◽  
Arumugam Murugadoss ◽  
Thangavelu Selvaraju ◽  
...  

2016 ◽  
Vol 22 (7) ◽  
pp. 2247-2252 ◽  
Author(s):  
Sai Sun ◽  
Xiaodong Zhuang ◽  
Bo Liu ◽  
Luxing Wang ◽  
Linfeng Gu ◽  
...  

RSC Advances ◽  
2016 ◽  
Vol 6 (47) ◽  
pp. 40911-40915 ◽  
Author(s):  
Rakesh Kumar Gupta ◽  
Vinod Kumar ◽  
Anchal Srivastava ◽  
Daya Shankar Pandey

Applicability of a novel heteroleptic dipyrrin complex exhibiting dual functionality (reducing and capping agent) in rapid synthesis of small sized AuNPs has been described.


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