scholarly journals A Green and Efficient Method for the Preparation of 3,4-Dihydropyrimidin-2(1H)-ones Using Quaternary Ammonium-Treated Clay in Water

2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Soheil Sayyahi ◽  
Sedigheh Jahanbakhshi ◽  
Zahra Dehghani

A variety of 3,4-dihydropyrimidin-2(1H)-ones derivatives were synthesized via three-component Biginelli reaction. The quaternary ammonium-treated clay-catalyzed process proved to be simple, efficient, and environmentally friendly.

2021 ◽  
Author(s):  
Pakin Noppawan ◽  
Suwiwat Sangon ◽  
Nontipa Supanchaiyamat ◽  
Andrew J. Hunt

Multicomponent one-pot Biginelli reactions have been successfully performed using vegetable oil as bio-based, non-toxic, and environmentally friendly solvents. Palm oil was demonstrated to be a highly effective greener solvent as...


2020 ◽  
pp. 174751982092575
Author(s):  
Meng Yao ◽  
Xia Chen ◽  
Yuling Lu ◽  
Zhenhua Guan ◽  
Zengwei Luo ◽  
...  

An efficient method for N-acylation of amides is described using a pyridine ring as the internal nucleophilic catalyst to give imides in moderate to excellent yields. The methodology provides a facile, air insensitive, and environmentally friendly route to form diversified imide scaffolds, which exist widely in natural products and biologically active materials.


Synlett ◽  
2019 ◽  
Vol 30 (17) ◽  
pp. 1981-1987 ◽  
Author(s):  
Michał Patrzałek ◽  
Jakub Piątkowski ◽  
Anna Kajetanowicz ◽  
Karol Grela

Easy and efficient method for preparation of all-chloro ruthenium catalysts bearing a quaternary ammonium tag was developed. The key anion metathesis reaction was made with AgCl, and the facile recycling of silver wastes was demonstrated. The developed method transforms more accessible, yet poorly characterised mixed chloro/iodo Ru complexes into valuable all-chloro catalysts, useful in aqueous metathesis. Practical utility of the developed anion metathesis reaction was demonstrated by preparation of a commercial Ru catalyst, StickyCat™, on a 5 gram scale.


2020 ◽  
Vol 44 (19) ◽  
pp. 7987-7997
Author(s):  
Diana Peña-Solórzano ◽  
Vladimir V. Kouznetsov ◽  
Cristian Ochoa-Puentes

An environmentally friendly and efficient method for the synthesis of indeno[2,1-c]quinolines is developed using a urea/zinc chloride eutectic mixture as a green mildly acidic medium.


2003 ◽  
Vol 46 (19) ◽  
pp. 4173-4181 ◽  
Author(s):  
Thorsteinn Thorsteinsson ◽  
Már Másson ◽  
Karl G. Kristinsson ◽  
Martha A. Hjálmarsdóttir ◽  
Hilmar Hilmarsson ◽  
...  

RSC Advances ◽  
2016 ◽  
Vol 6 (38) ◽  
pp. 31698-31704 ◽  
Author(s):  
Kai Liu ◽  
Zhiguo Su ◽  
Shida Miao ◽  
Guanghui Ma ◽  
Songping Zhang

A simple, green, robust and efficient method has been developed for the preparation of an anti-biofouling coating by directly mixing antifouling enzymes with a castor oil-based waterborne polyurethane (WPU) dispersion.


2020 ◽  
Vol 57 (6) ◽  
pp. 2466-2479
Author(s):  
Vakhid A. Mamedov ◽  
Nataliya A. Zhukova ◽  
Milyausha S. Kadyrova ◽  
Rezeda R. Fazleeva ◽  
Olga B. Bazanova ◽  
...  

2016 ◽  
Vol 13 (7) ◽  
pp. 526-530
Author(s):  
Imane Tebabel ◽  
Taoues Boumoud ◽  
Boudjemaa Boumoud ◽  
Debache Abdelmadjid

2021 ◽  
Author(s):  
Ting-Kai Xiong ◽  
Xue-Qi Zhou ◽  
Min Zhang ◽  
Hai-Tao Tang ◽  
Ying-Ming Pan ◽  
...  

An electrocatalyzed three-component cascade reaction of CO2, amines, and N-alkenylsulfonamides is developed, providing an environmentally friendly and efficient method of synthesizing a series of new carbamate compounds. This reaction meets...


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