scholarly journals Processing of CNTs Reinforced Al-Based Nanocomposites Using Different Consolidation Techniques

2013 ◽  
Vol 2013 ◽  
pp. 1-10 ◽  
Author(s):  
N. Al-Aqeeli
Keyword(s):  
Temperature Distribution ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
The Other ◽  
Milling Parameters ◽  
The Poor ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Hardness Values

In this work, the development of two types of Al-based alloys with different concentrations of Si reinforced with MWCNT’s at 0.5–2.0 wt% is presented. Sonication of the CNT’s in ethyl alcohol was carried out for dispersion, and the mixtures were ball milled for 1, 3, and 5 hrs. SEM/EDS were used to study the morphology and the effects of changing milling parameters in addition to changes caused due to increasing concentration of the CNT’s. Furthermore, three sintering techniques, namely, Spark Plasma Sintering (SPS), Microwave Sintering (μWS), and Hot Isostatic Press Sintering (HIP) were employed to consolidate the ball milled powders at varying temperatures of 400, 450, and 500°C. It was found that SPS consolidated samples showed the most promising results amongst the three with the highest hardness values; around 100% densification, as well as the finest microstructure. On the other hand, microwave sintered samples showed the least appealing results, this could be attributed to the poor temperature distribution and the pressureless nature of the technique. A sintering temperature of 500°C was found to be the most suitable for these types of alloys.

Fabrication of TiAl Intermetallic by Spark Plasma Sintering

2007 ◽  
Vol 336-338 ◽  
pp. 1050-1052 ◽  
Author(s):  
Hai Tao Wu ◽  
Yun Long Yue ◽  
Wei Bing Wu ◽  
Hai Yan Yin
Keyword(s):  
Mechanical Properties ◽  
Intermetallic Compounds ◽  
Spark Plasma Sintering ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Three Point Bending ◽  
The Poor ◽  
High Relative Density ◽  
Plasma Sintering ◽  
Spark Plasma

The γ-TiAl intermetallic compounds were produced at the temperature ranging from 850°C to 1050°C by the Spark Plasma Sintering (SPS) process. The effects of sintering temperature and holding time on the mechanical properties of γ-TiAl intermetallic compounds were investigated. The γ-TiAl intermetallic compounds sintered at 1050°C for 10 min showed a high relative density more than 98%, and had the best three-point bending strength of 643MPa, fracture toughness of 12 MPa·m1/2 and microhardness of 560MPa. The microstructural observations indicated typical characteristics of intergranular fracture, which meant the poor ductility of γ-TiAl intermetallic compounds.

TiO2 ceramic particles-reinforced aluminum matrix composite prepared by conventional, microwave, and spark plasma sintering

2017 ◽  
Vol 52 (19) ◽  
pp. 2609-2619 ◽  
Author(s):  
Ehsan Ghasali ◽  
Masoud Alizadeh ◽  
Touradj Ebadzadeh
Keyword(s):  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
Aluminum Matrix ◽  
High Energy ◽  
Conventional Heating ◽  
X Ray ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Ti Particles

Aluminum-10 wt% TiO2 metal matrix composites were fabricated with conventional, microwave, and spark plasma sintering processes. Aluminum and nano-sized TiO2 powders were mixed using a high-energy mixer, and the sintering process was done at 450℃ by spark plasma sintering and 600℃ under both microwave and conventional heating. The results showed microwave sintering led to form Al3Ti intermetallic compounds with flaky shape, while in the conventional heating at the same sintering temperature, Al3Ti was formed and confirmed by X-ray diffraction and scanning electron microscope investigations. Moreover, the nano-sized TiO2 particles as reinforcement with no additional phase were obtained by spark plasma sintering at the lowest sintering temperature. The maximum bending strength of 254 ± 12 MPa and Vickers hardness of 235 ± 13 were measured for samples sintered in microwave as a consequence of Al3Ti formation. The SEM and energy-dispersive X-ray spectroscopy analyses showed uniform distribution of Al3Ti particles in the microstructure of microwave sintered samples and nonuniform distribution of agglomerated Al3Ti particles and porosities in samples sintered by spark plasma sintering and conventional heating.

Microstructure and Mechanical Properties of ZrO2(Y2O3)-Al2O3 Nano Composites Prepared by Spark Plasma Sintering

2008 ◽  
Author(s):  
Shufeng Li ◽  
Hiroshi Izui ◽  
Michiharu Okano ◽  
Weihua Zhang ◽  
Taku Watanabe
Keyword(s):  
Mechanical Properties ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Alumina Ceramic ◽  
The Other ◽  
Sintering Behavior ◽  
Nanocomposite Powder ◽  
Mixed Powder ◽  
Plasma Sintering ◽  
Spark Plasma

Zirconia (Y2O3)-alumina ceramic nanocomposites were fabricated by spark plasma sintering (SPS). A commercially available nanocomposite powder TZP-3Y20A was used as starting powder, the other from conventionally mechanical mixed powder 3YSZ-20A used for comparison. The effect of sintering temperature on the densification, sintering behavior, mechanical properties, and microstructure of the composites were investigated. The results show that the density increase with increasing of sintering temperature, and thus mechanical properties were strengthened with enhancing of densification. The nanocomposite powder TZP-3Y20A was easily sintered and good mechanical properties were achieved, compared with the powder from conventionally mechanical mixed, where the maximum strength and toughness of composites are 967 MPa and 5.27 MPam1/2, respectively.

Effect of Spark Plasma Sintering Temperature on Microstructures and Properties of Copper-Diamond Composites

2013 ◽  
Vol 683 ◽  
pp. 573-576
Author(s):  
Abdul Rehman Niazi ◽  
Shu Kui Li ◽  
Ying Chun Wang ◽  
Jin Xu Liu ◽  
Zhi Yu Hu ◽  
...  
Keyword(s):  
Relative Density ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
The Other ◽  
Interface Bonding ◽  
Mechanical Mixing ◽  
Temperature Variations ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Diamond Powders

Temperature being one of the most important parameters of Spark plasma sintering (SPS) and its effects on the microstructures as well as on the physical properties of copper diamond composites fabricated by mechanical mixing of copper with 70 vol.% diamond powders, precoated with 1 wt% chromium has been studied. Experiments were performed at 900°C, 1000°C and 1100 °C for 10 minutes under 50 MPa. The results reveal that sintering temperature highly influences the copper/diamond interface bonding and microstructures. The composite’s properties like thermal conductivity (T.C), specific heat (Cp), diffusivity (Dff) and relative density (ρr) were also highly influenced by temperature variations. Except the relative density, all the other properties increased respectively with increasing sintering temperature.

Mechanical Properties of ZrO2 (Y2O3)-Al2O3 Nanocomposites with Addition of Hydroxyapatite Prepared by Spark Plasma Sintering

2009 ◽  
Vol 631-632 ◽  
pp. 413-423 ◽  
Author(s):  
Shu Feng Li ◽  
Hiroshi Izui ◽  
Michiharu Okano ◽  
Wei Hua Zhang ◽  
Taku Watanabe
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Spark Plasma Sintering ◽  
Vickers Hardness ◽  
Volume Fraction ◽  
Sintering Temperature ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Hardness Values

TZP-3Y20A/HA composites with addition of different volume fraction of hydroxyapatite (HA) were fabricated successfully using spark plasma sintering (SPS). The densification behavior and mechanical properties of composites are investigated as a function of sintering temperature and HA content respectively. The density of TZP-3Y20A composite increases steadily with temperature and a maximum value of 97.8% is obtained after sintering at 1400°C. Sintering the TZP-3Y20A/HA composites at 1400°C led to the decomposition of HA in the samples. Flexural strength, fracture toughness and Vickers hardness values increase with increasing sintering temperature, show decrease trend with increasing of HA content at the same temperature. They compared well with densities obtained at different sintering temperature. The maximum flexural strength, fracture toughness and Vickers hardness of 967.1 MPa, 5.27 MPam1/2 and 13.26 GPa were achieved for TZP-3Y20A composite respectively. Flexural strength, fracture toughness and Vickers hardness values of TZP-3Y20A/HA composite fell within the value range of dense HA and of TZP-3Y20A composite.

Effect of spark plasma sintering temperature on structure and phase composition of Ti-Al-Nb-based alloys

2017 ◽  
Vol 59 (11-12) ◽  
pp. 1033-1036 ◽  
Author(s):  
Sherzod Kurbanbekov ◽  
Mazhyn Skakov ◽  
Viktor Baklanov ◽  
Batyrzhan Karakozov
Keyword(s):  
Phase Composition ◽  
Spark Plasma Sintering ◽  
Sintering Temperature ◽  
Plasma Sintering ◽  
Spark Plasma

scholarly journals Influence of CFRC Insulating Plates on Spark Plasma Sintering Process

Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 393
Author(s):  
Alexander M. Laptev ◽  
Jürgen Hennicke ◽  
Robert Ihl
Keyword(s):  
Temperature Distribution ◽  
Spark Plasma Sintering ◽  
Energy Demand ◽  
Composite Powders ◽  
Fem Method ◽  
Plasma Sintering ◽  
Axial Temperature ◽  
Spark Plasma ◽  
Power And Energy ◽  
The Impact

Spark Plasma Sintering (SPS) is a technology used for fast consolidation of metallic, ceramic, and composite powders. The upscaling of this technology requires a reduction in energy consumption and homogenization of temperature in compacts. The application of Carbon Fiber-Reinforced Carbon (CFRC) insulating plates between the sintering setup and the electrodes is frequently considered as a measure to attain these goals. However, the efficiency of such a practice remains largely unexplored so far. In the present paper, the impact of CFRC plates on required power, total sintering energy, and temperature distribution was investigated by experiments and by Finite Element Modeling (FEM). The study was performed at a temperature of 1000 °C with a graphite dummy mimicking an SPS setup. A rather moderate influence of CFRC plates on power and energy demand was found. Furthermore, the cooling stage becomes considerably longer. However, the application of CFRC plates leads to a significant reduction in the axial temperature gradient. The comparative analysis of experimental and modeling results showed the good capability of the FEM method for prediction of temperature distribution and required electric current. However, a discrepancy between measured and calculated voltage and power was found. This issue must be further investigated, considering the influence of AC harmonics in the DC field.

Effect of Spark Plasma Sintering on the Microstructure Evolution and Properties of M3:2 High-Speed Steel

2014 ◽  
Vol 788 ◽  
pp. 329-333
Author(s):  
Rui Zhou ◽  
Xiao Gang Diao ◽  
Jun Chen ◽  
Xiao Nan Du ◽  
Guo Ding Yuan ◽  
...  
Keyword(s):  
Powder Metallurgy ◽  
Spark Plasma Sintering ◽  
High Speed ◽  
Bending Strength ◽  
Sintering Temperature ◽  
High Speed Steel ◽  
Continuous Heating ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
The Impact

Effects of sintering temperatures on the microstructure and mechanical performance of SPS M3:2 high speed steel prepared by spark plasma sintering was studied. High speed steel sintering curve of continuous heating from ambient temperature to 1200°C was estimated to analyze the sintering processes and sintering temperature range. The sintering temperature within this range was divided into groups to investigate hardness, relative density and microstructure of M3:2 high-speed steel. Strip and quadrate carbides were observed inside the equiaxed grains. SPS sintering temperature at 900°C can lead to nearly full densification with grain size smaller than 20μm. The hardness and bending strength are higher than that of the conventionally powder metallurgy fabricated ones sintered at 1270°C. However, fracture toughness of the high speed steel is lower than that of the conventional powder metallurgy steels. This can be attributed to the shape and distribution of M6C carbides which reduce the impact toughness of high speed steels.

Sign in / Sign up

Export Citation Format

Share Document