scholarly journals Further Insight into the Depth-Dependent Microstructural Response of Cartilage to Compression Using a Channel Indentation Technique

2013 ◽  
Vol 2013 ◽  
pp. 1-11 ◽  
Author(s):  
Ashvin Thambyah ◽  
Neil D. Broom

Stress relaxation and structural analysis were used to investigate the zonally differentiated microstructural response to compression of the integrated cartilage-on-bone tissue system. Fifteen cartilage-on-bone samples were divided into three equal groups and their stress relaxation responses obtained at three different levels of axial compressive strain defined as low (~20%), medium (~40%) and high (~60%). All tests were performed using a channel indenter which included a central relief space designed to capture the response of the matrix adjacent to the directly loaded regions. On completion of each stress relaxation test and while maintaining the imposed axial strain, the samples were formalin fixed, decalcified, and then sectioned for microstructural analysis. Chondron aspect ratios were used to determine the extent of relative strain at different zonal depths. The stress relaxation response of cartilage to all three defined levels of axial strain displayed an initial highly viscous response followed by a significant elastic response. Chondron aspect ratio measurements showed that at the lowest level of compression, axial deformation was confined to the superficial cartilage layer, while in the medium and high axial strain samples the deformation extended into the midzone. The cells in the deep zone remained undeformed for all compression levels.

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4384
Author(s):  
Mohd Aidy Faizal Johari ◽  
Asmawan Mohd Sarman ◽  
Saiful Amri Mazlan ◽  
Ubaidillah U ◽  
Nur Azmah Nordin ◽  
...  

Micro mechanism consideration is critical for gaining a thorough understanding of amorphous shear band behavior in magnetorheological (MR) solids, particularly those with viscoelastic matrices. Heretofore, the characteristics of shear bands in terms of formation, physical evolution, and response to stress distribution at the localized region have gone largely unnoticed and unexplored. Notwithstanding these limitations, atomic force microscopy (AFM) has been used to explore the nature of shear band deformation in MR materials during stress relaxation. Stress relaxation at a constant low strain of 0.01% and an oscillatory shear of defined test duration played a major role in the creation of the shear band. In this analysis, the localized area of the study defined shear bands as varying in size and dominantly deformed in the matrix with no evidence of inhibition by embedded carbonyl iron particles (CIPs). The association between the shear band and the adjacent zone was further studied using in-phase imaging of AFM tapping mode and demonstrated the presence of localized affected zone around the shear band. Taken together, the results provide important insights into the proposed shear band deformation zone (SBDZ). This study sheds a contemporary light on the contentious issue of amorphous shear band deformation behavior and makes several contributions to the current literature.


2010 ◽  
Vol 97-101 ◽  
pp. 3910-3915
Author(s):  
Kun Cai

The deformation of single-walled carbon nanotubes (SWCNTs) under large axial strain is studied by a geometrical mapping method. The interactions between atoms in carbon nanotubes (CNTs) are described by Tersoff-Brenner potential. Results show the strain energy depends on chirality but hardly on tubes’ radii. For graphitic sheet under large axial deformation, the elastic moduli decrease with the increase of engineering strain under tension. The modulus reaches the peak value as the axial engineering strain reaches -0.08 for armchair pattern and -0.15 for zigzag pattern under compression.


Author(s):  
Philip Boughton ◽  
James Merhebi ◽  
C. Kim ◽  
G. Roger ◽  
Ashish D. Diwan ◽  
...  

An elastomeric spinal disk prosthesis design (BioFI™) with vertebral interlocking anchors has been modified using an embedded TiNi wire array. Bioinert styrenic block copolymer (Kraton®) and polycarbonate urethane (Bionate®) thermoplastic elastomer (TPE) matrices were utilized. Fatigue resistant NiTi wire was pretreated to induce superelastic martensitic microstructure. Stent-like helical structures were produced for incorporation within homogenous TPE matrix. Composite prototypes were fabricated in a vacuum hot press using transfer moulding techniques. Implant prototypes were subject to axial compression using a BOSE ® ELF3400. The NiTi reinforced implants exhibited reduction in axial strain, compliance, and creep compared to TPE controls. The axial properties of the NiTi reinforced Bionate® BioFI™ implant best approximated those of a spinal disk followed by Kraton®-NiTi, Bionate® and Kraton® prototypes. An ovine lumbar segment biomechanical model was used to characterize the disk prosthesis prototypes. Specimens were subject to 7.5Nm pure moments in axial rotation, flexion-extension and lateral bending with a custom jig mounted on an Instron® 8874. The motion preserving ligamentous nature of this arthroplasty prototype was not inhibited by NiTi reinforcement. Joint stiffness for all prototypes was significantly less than the intact and discectomy controls. This was due to lack of vertebral anchor rigidity rather than BioFI™ motion segment matrix type or reinforcement. Implant stress profiles for axial compression and axial torsion conditions were obtained using finite element methods. The biomechanical testing and finite element modelling both support existing BioFI™ design specifications for higher modulus vertebral anchors, endplates and motion segment periphery with gradation to a low modulus core within the motion segment. This closer approximation of the native spinal disk form translates to improvements in prosthesis biomechanical fidelity and longevity. Axial compressive strain induced within a TiNi reinforced Kraton® BioFI™ was found to be linearly proportional to the NiTi helical coil electrical resistance. This neural network capability delivers opportunities to monitor and telemeterize in situ multiaxis joint structural performance and in vivo spine biomechanics.


2015 ◽  
Vol 22 (5) ◽  
pp. 969-987 ◽  
Author(s):  
Ivan Giorgio ◽  
Ugo Andreaus ◽  
Tomasz Lekszycki ◽  
Alessandro Della Corte

Since internal architecture greatly influences crucial factors for tissue regeneration, such as nutrient diffusion, cell adhesion and matrix deposition, scaffolds have to be carefully designed, keeping in mind case-specific mechanical, mass transport and biological requirements. However, customizing scaffold architecture to better suit conflicting requirements, such as biological and mechanical ones, remains a challenging issue. Recent advances in printing technologies, together with the synthesis of novel composite biomaterials, have enabled the fabrication of various scaffolds with defined shape and controlled in vitro behavior. Thus, the influence of different geometries of the assemblage of the matrix and scaffold on the remodeling processes of living bone and artificial material should be investigated. To this end, two implant shapes are considered in this paper, namely a circular inclusion and a rectangular groove of different aspect ratios. A model of a mixture of bone tissue and bioresorbable material with voids was used to numerically analyze the physiological balance between the processes of bone growth and resorption and artificial material resorption in a plate-like sample. The adopted model was derived from a theory for the behavior of porous solids in which the matrix material is elastic and the interstices are void of material.


Author(s):  
Turker Turkoglu ◽  
Sare Celik

Abstract In order to eliminate the agglomeration problem of reinforcement in the nanocomposite, a two-step dispersion process was employed. Under ultra-sonication and ball milling, 1 wt.% of multi-walled carbon nanotubes (MWCNTs) were properly dispersed in pure aluminum (Al) (used as the matrix phase). The composite powder mixture was then consolidated in an inert Ar gas atmosphere by hot pressing under certain fabrication parameters. The powder mixture was characterized by Raman Spectroscopy, and it was found that MWCNTs did not cause structural defects in the pre-production process. The microstructural analysis of the sintered composites by scanning electron microscope (SEM) and energy-dispersive x-ray spectroscopy (EDS), revealed that the reinforcement was uniformly distributed in the matrix. Wear test results indicated that the wear resistance of the composites increased with increase of MWCNT reinforcement, and the wear mechanism was determined to be a mixing type by examining the wear traces by SEM. In order to determine the effects of different process parameters on wear loss, a multilayer perceptron (MLP) based artificial neural network (ANN) was used, and experimental and predicted values were compared. It was noticed that the MLP based ANN model effectively evaluated the wear properties of the Al/MWCNT composites.


2018 ◽  
Vol 225 ◽  
pp. 03007
Author(s):  
Balaji Bakthavatchalam ◽  
Khairul Habib ◽  
Namdev Patil ◽  
Omar A Hussein

Microstructural Analysis plays an important role in enhancing the mechanical properties of metals and composites. Usually Aluminium Silicon Carbide (Al6063/SiC) alloys are mixed with strontium, sodium and antimony for high durability even though they are toxic and costly. As an alternative calcium is used as an alloying element to improve the mechanical property of Al6063/Sic alloy. In this paper Al6063 is chosen as the matrix material while Sic is used as a reinforcement where calcium powder is added to modify the silicon phase of the composite. Finally, concentration of Silicon carbide is varied from 0 to 150 mg to produce four specimens of Al6063 alloy and it is subjected to microstructure analysis which showed the reduction of grain size and therefore improvement in the hardness from 52.9 HV to 58.4 HV and decrease in the wear loss from 3.97 to 3.27 percentage.


Author(s):  
Rui Xie ◽  
Prof. Jie Zhang

Abstract Thaw settlement is one of main reason caused pipeline failure crossing cold region. Mechanical behavior of buried pipeline crossing thaw settlement zone is investigated. Effects of pipeline and soil parameters on the buried pipeline were discussed. The results show that the high stress area and the max axial strain of the pipeline is at the edge of the thaw settlement zone. The upper surface of the pipeline is tensile strain, while the lower surface is compressive strain. The max ovality of pipeline near the edge of thaw settlement zone tends to oval. The pipeline axial strain, ovality and displacement decreases with the increasing of pipeline wall thickness, while the change of high stress area is not obvious. The high stress area and ovality decrease with the increasing of pipeline diameter, while the high stress area is expanded along the axial direction, but axial strain decreases slightly. The high stress area, axial strain, ovality and displacement of pipeline decrease with the buried depth increases. With the internal pressure increases, the stress and axial strain of pipeline increase, but the ovality decreases. The soil`s elasticity modulus has no obvious effect on pipeline`s stress, axial strain and displacement, but it can affect ovality slightly.


2021 ◽  
Author(s):  
Hugo van Schrojenstein Lantman ◽  
David Wallis ◽  
Mattia Gilio ◽  
Marco Scambelluri ◽  
Matteo Alvaro

<p>Determining the stress state during metamorphism is a key challenge in metamorphic petrology as the effect of differential stress on metamorphic reactions is currently debated. Conventional piezometry generally gives stresses that correspond to overprinting deformation rather than to mineral growth of high-grade metamorphism, so an alternative approach is required. Garnetite lenses from the ultrahigh-pressure, low-temperature metamorphic Lago di Cignana unit (Western Alps, Italy) record compaction by a high degree of mineral dissolution in the fluid-rich environment of a cold subduction zone. This work combines microstructural analysis of deformed garnet with elastic strains of quartz inclusions to study the stresses in these metasedimentary rocks.</p><p>Garnet exhibits abundant evidence for incongruent pressure solution (IPS), most notably as truncated zones that mismatch across grain boundaries, interlocking structures, and shape-preferred orientation (SPO). The gap in garnet compositions represented by overgrown truncated zonation corresponds to undeformed garnet with inclusions of quartz and coesite, indicating that IPS operated during prograde to peak metamorphism. The distribution of aspect ratios in the garnet grain population suggests that pressure solution preferentially affected smaller grains. SPO analysis of many subregions across a garnetite sample reveals a complex distribution, however the local SPO is consistent with the stress orientation expected for local microstructures such as layering, garnet stacks, or fine-grained internal fluid pathways. Locally, two different preferential orientations are observed, interpreted as the result of two subsequent deformation stages under different stress configurations.</p><p>Quartz inclusions in prograde euhedral garnet, grown on the outer margin of coevally deformed garnetite, were analysed with Raman spectroscopy. Elastic strains obtained for these inclusions are in agreement with predicted strains for entrapment along the prograde <em>P</em>-<em>T</em> path for the Lago di Cignana unit (~1.5–2.0 GPa; ~450–500 °C), whereas significant differential stress during entrapment is expected to result in deviating strain components.</p><p>By combining microstructural analysis of garnet with elastic-strain analysis of quartz inclusions, stress orientations obtained from deformed garnet are combined with the stress magnitude for coeval garnet growth. The results indicate that the garnetite lenses were deformed and metamorphosed under low differential stress of variable orientation during subduction. These results are in agreement with a system where garnet is wet by a fluid phase that allows IPS.</p><p> </p><p>Acknowledgements: This project has received funding from the European Research Council under the H2020 research and innovation program (N. 714936 TRUE DEPTHS to M. Alvaro)</p>


1990 ◽  
Vol 194 ◽  
Author(s):  
J. J. Valencia ◽  
J. P. A. Löfvander ◽  
J. Rösler ◽  
C. G. Levi ◽  
R. Mehrabian

AbstractAdditions of ∼5%B1 and ∼9%Ta to binary γ-TiAl result in the formation of a monoboride isomorphous with TiB but containing Ta in solid solution. This boride exhibits strongly anisotropic growth from the melt, producing rod-like primary phases which are of potential interest for creep strengthening of the γ matrix. Fibrous borides with aspect ratios larger than ∼20 and volume fractions of ∼0.12 have been produced in arc-melted Ti-48AI-9Ta-4.3B alloys. Creep testing at 1255 K indicates that these “in-situ” composites have much higher creep strength than γ-TiAl, but the contribution of the reinforcements is relatively small compared with the solute-strengthening of the matrix.


2004 ◽  
Vol 126 (1) ◽  
pp. 92-97 ◽  
Author(s):  
Steven D. Abramowitch ◽  
Savio L.-Y. Woo

The quasi-linear viscoelastic (QLV) theory proposed by Fung (1972) has been frequently used to model the nonlinear time- and history-dependent viscoelastic behavior of many soft tissues. It is common to use five constants to describe the instantaneous elastic response (constants A and B) and reduced relaxation function (constants C, τ1, and τ2) on experiments with finite ramp times followed by stress relaxation to equilibrium. However, a limitation is that the theory is based on a step change in strain which is not possible to perform experimentally. Accounting for this limitation may result in regression algorithms that converge poorly and yield nonunique solutions with highly variable constants, especially for long ramp times (Kwan et al. 1993). The goal of the present study was to introduce an improved approach to obtain the constants for QLV theory that converges to a unique solution with minimal variability. Six goat femur-medial collateral ligament-tibia complexes were subjected to a uniaxial tension test (ramp time of 18.4 s) followed by one hour of stress relaxation. The convoluted QLV constitutive equation was simultaneously curve-fit to the ramping and relaxation portions of the data r2>0.99. Confidence intervals of the constants were generated from a bootstrapping analysis and revealed that constants were distributed within 1% of their median values. For validation, the determined constants were used to predict peak stresses from a separate cyclic stress relaxation test with averaged errors across all specimens measuring less than 6.3±6.0% of the experimental values. For comparison, an analysis that assumed an instantaneous ramp time was also performed and the constants obtained for the two approaches were compared. Significant differences were observed for constants B, C, τ1, and τ2, with τ1 differing by an order of magnitude. By taking into account the ramping phase of the experiment, the approach allows for viscoelastic properties to be determined independent of the strain rate applied. Thus, the results obtained from different laboratories and from different tissues may be compared.


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