scholarly journals A Simple Effective Flaw Model on Analyzing the Nanofiller Agglomeration Effect of Nanocomposite Materials

2012 ◽  
Vol 2012 ◽  
pp. 1-5 ◽  
Author(s):  
Arun Krishnan ◽  
L. Roy Xu

A special mechanics/material phenomenon involving nanocomposites is the agglomeration of nanofillers at high volume fractions of nanofillers. Numerous experimental investigations on nanocomposites have indicated a significant decrease in mechanical properties, due to the agglomeration of nanofillers. This paper describes a simple effective flaw model to correlate the local mechanical behavior of agglomerated nanoparticles with the change in global strengths of nanocomposites. The estimated bending strength reduction from our model is shown to be similar to experimental results reported by previous researchers. These results can be used as a guide for future nanocomposite design and development. Future nanomaterial manufacturing should be focused on eliminating the largest agglomerates, rather than limiting the nanofiller volume fraction. Meanwhile, by reducing the nanofiller agglomerate size, we expect that a high critical nanofiller volume fraction could be obtained to delay the mechanical property reduction.

2006 ◽  
Vol 321-323 ◽  
pp. 1070-1073
Author(s):  
Ye Yeon Won ◽  
Myong Hyun Baek ◽  
Wen Quan Cui ◽  
Kwang Kyun Kim

This study investigates micro-structural and mechanical properties of trabecular bone in human femoral head with and without osteoporosis using a micro-CT and a finite element model. 15 cored trabecular bone specimens with 20 of diameter were obtained from femoral heads with osteoporosis resected for total hip arthroplasty, and 5 specimens were removed from femoral head of cadavers, which has no history of musculoskeletal diseases. A high-resolution micro-CT system was used to scan each specimen to obtain histomorphometry indexes. Based on the micro-images, a FE-model was created to determine mechanical property indexes. While the non-osteoporosis group had increases the trabecular thickness, the bone volume, the bone volume fraction, the degree of anisotropy and the trabecular number compared with those of osteoporotic group, the non-osteoporotic group showed decreases in trabecular separation and structure model index. Regarding the mechanical property indexes, the reaction force and the Young's modulus were lower in the osteoporotic group than in non-osteoporotic group. Our data shows salient deteriorations in trabecular micro-structural and mechanical properties in human femoral head with osteoporosis.


2013 ◽  
Vol 589-590 ◽  
pp. 590-593 ◽  
Author(s):  
Min Wang ◽  
Jun Zhao

In order to investigate the effects of TiN content on Al2O3/TiN ceramic material (ATN), the ATN ceramic materials were prepared of TiN content in 30%, 40%, 50%, 60% in the condition of hot press sintering. The sintering temperature is 1700°C, the sintering press is 32MPa, and the holding time are 5min, 10min, 15min. The effects of TiN content on mechanical properties and microstructure of ATN ceramic materials were investigated by analyzing the bending strength, hardness, fracture toughness. The results show that ATN50 has the best mechanical property, its bending strength is 659.41MPa, vickers hardness is 13.79GPa, fracture toughness is 7.06MPa·m1/2. It is indicated that the TiN content has important effect on microstructure and mechanical properties of ATN ceramic materials.


Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1926 ◽  
Author(s):  
Lei Zhang ◽  
Zhifu Huang ◽  
Yangzhen Liu ◽  
Yupeng Shen ◽  
Kemin Li ◽  
...  

Mo2NiB2-Ni cermets have been extensively investigated due to their outstanding properties. However, studies have not systematically examined the effect of the powder milling process on the cermets. In this study, Mo, Ni, and B raw powders were subjected to mechanical ball milling from 1 h to 15 h. XRD patterns of the milled powders confirmed that a new phase was not observed at milling times of 1 h to 15 h. With the increase in the mechanical ball milling time from 1 h to 11 h, raw powders were crushed to small fragments, in addition to a more uniform distribution, and with the increase in the mechanical ball milling time to greater than 11 h, milled powders changed slightly. Mo2NiB2-Ni cermets were fabricated by reaction boronizing sintering using the milled powders at different ball milling times. The milling time significantly affected the microstructure and mechanical properties of Mo2NiB2-Ni cermets. Moreover, the Mo2NiB2 cermet powder subjected to a milling time of 11 h exhibited the finest crystal size and the maximum volume fraction of the Mo2NiB2 hard phase. Furthermore, the cermets with a milling time of 11 h exhibited a maximum hardness and bending strength of 87.6 HRA and 1367.3 MPa, respectively.


2020 ◽  
Vol 4 (1) ◽  
pp. 5
Author(s):  
Nhan Thi Thanh Nguyen ◽  
Obunai Kiyotaka ◽  
Okubo Kazuya ◽  
Fujii Toru ◽  
Shibata Ou ◽  
...  

In this research, three kinds of carbon fiber (CF) with lengths of 1, 3, and 25 mm were prepared for processing composite. The effect of submicron glass fiber addition (sGF) on mechanical properties of composites with different CF lengths was investigated and compared throughout static tests (i.e., bending, tensile, and impact), as well as the tension-tension fatigue test. The strengths of composites increased with the increase of CF length. However, there was a significant improvement when the fiber length changed from 1 to 3 mm. The mechanical performance of 3 and 25 mm was almost the same when having an equal volume fraction, except for the impact resistance. Comparing the static strengths when varying the sGF content, an improvement of bending strength was confirmed when sGF was added into 1 mm composite due to toughened matrix. However, when longer fiber was used and fiber concentration was high, mechanical properties of composite were almost dependent on the CF. Therefore, the modification effect of matrix due to sGF addition disappeared. In contrast to the static strengths, the fatigue durability of composites increased proportionally to the content of glass fiber in the matrix, regardless to CF length.


2013 ◽  
Vol 745-746 ◽  
pp. 700-705
Author(s):  
Huang Liu ◽  
Guo Qiang Luo ◽  
Pin Gan Chen ◽  
Qiang Shen ◽  
Lian Meng Zhang

SiC/Cu composites exhibit low density, low coefficient of thermal expansion and excellent mechanical properties. In this study, Zn of 2 wt. % was added as the sintering activator, and the high volume faction (60%) SiC/Cu composites was fabricated by hot pressing sintering technology. The phase composition and morphology of as-prepare samples were characterized by X-ray diffraction (XRD) system and scanning electron microscopy (SEM) equipped with an energy-dispersive spectroscopy (EDS) system. The as-prepared SiC/Cu composites were dense and uniform as well as void free. The results show that SiC/Cu composites can reach excellent mechanical properties of SiC/Cu composites. With the increase of sintering temperature, Vickers hardness and the bending strength of the samples increased obviously and the as-prepared SiC/Cu composites achieved a maximum Vickers hardness and bending strength respectively of 195MPa and 140MPa.


2014 ◽  
Vol 983 ◽  
pp. 94-98 ◽  
Author(s):  
Li Jun Wang ◽  
Jian Hui Qiu ◽  
Eiichi Sakai

The melting mixing was applied in the preparation of Multiwalled carbon nanotubes/Polycarbonate (MWCNTs/PC) nanocomposites. MWCNTs/PC nanocomposites with different MWCNTs contents were prepared under different injection conditions. The mechanical property of nanocomposites was comparatively investigated. The results demonstrated that: the tensile property of the nanocomposites was slightly improved by MWCNTs content increasing; but as the MWCNTs contents went on to increase to 10wt%, the tensile strength and bending strength were obviously decreased about 35% and 47%, respectively, but the impact strength and hardness were increased. The center hardness of MWCNTs/PC nanocomposites was greater than the surface hardness. Besides, the changes on the mechanical properties of the nanocomposites were studies by changing the injection conditions. By Scanning Electron Microscopy (SEM) observation, the microstructure and morphology of nanocomposites were analyzed, revealing that the center of the nanocomposite distributed more MWNTs, and the injection conditions would affect the MWNTs’ dispersion in the matrix and the interfacial interaction between MWCNTs and PC.


2015 ◽  
Vol 60 (1) ◽  
pp. 517-521
Author(s):  
S. Marciniak ◽  
E. Skołek ◽  
W. Świątnicki

AbstractThis paper presents the results of studies of X37CrMoV5-1 steel subjected to quenching processes with a one-step and a two-step isothermal annealing. The TEM observation revealed that steel after one-step treatment led is composed of carbide-free bainite with nanometric thickness of ferrite plates and of high volume fraction of retained austenite in form of thin layers or large blocks. In order to improve the strength parameters an attempt was made to reduce the austenite content by use of quenching with the two-step isothermal annealing. The temperature and time of each step were designed on the basis of dilatometric measurements. It was shown, that the two-step heat treatment led to increase of the bainitic ferrite content and resulted in improvement of steel's strength with no loss of steel ductility.


2021 ◽  
Vol 6 (1) ◽  
pp. 30-37
Author(s):  
Sri Hastuti ◽  
Herru Santosa Budiono ◽  
Diki Ilham Ivadiyanto ◽  
Muhammad Nurdin Nahar

Inovasi baru serat dari sabut kelapa dimanfaatkan untuk meningkatkan nilai ekonomis dari serat sabut kelapa, oleh karena itu dirancanglah pendayagunaan serat dari sabut kelapa untuk penguat komposit dengan material serat alam yang biodegradable. Hal ini untuk mendukung penggunaan komposit yang ramah terhadap lingkungan dan mengurangi penggunaan material komposit serat sintetis yang polutan. Tujuan penelitian adalah menganalisis sifat mekanik pada komposit serat alam bermaterial serat dari sabut kelapa yang ramah lingkungan. Metode penelitian pembuatan komposit berpenguat serat dari sabut kelapa dilakukan treatment NaOH 15% selama 5 jam dan fraksi volume serat 10 %, 15 %, dan 20 %. Komposit  serat dari sabut kelapa dengan matriks UPRs 157 BQTN dengan hardener MEXPO. Pengujian mekanik dilakukan uji bending menggunakan standar ASTM D790 dan uji impak  menggunakan standar ASTM D5941.  Pengujian impak komposit serat alam menunjukkan ketangguhan impak komposit pada fraksi volume serat 20% dengan nilai 0.017588J/mm2. Hasil pengujian menunjukkan peningkatan fraksi volume serta berpengaruh terhadap peningkatan kekuatan bending komposit serat dari sabut kelapa  dengan kekuatan optimum bending pada fraksi volume serat 10% dengan nilai 44,33N/mm2. Hal ini menunjukkan peningkatan fraksi volume serat dengan perendaman NaOH 15% akan meningkatkan sifat mekanik bending dan impak komposit. Perendaman NaOH memberikan pengaruh daya serap sabut kelapa terhadap matrik Unsaturated Polyester yang dapat meningkatkan daya rekat antara penguat serat dengan matrik sehingga meningkatkan sifat mekanik bending dan impak komposit. ABSTRACT The innovation of coco fiber is used to increase the economic value of coconut coir, therefore the utilization of coconut fiber for reinforcing composites with biodegradable natural fiber material is designed. This is to support the use of composites that are friendly to the environment and reduce the use of pollutant synthetic fiber composite materials. The research objective was to analyze the mechanical properties of natural fiber composites with environmentally friendly coconut fiber as material. The research method of making fiber-reinforced composites from coconut coir was carried out by 15% NaOH treatment for 5 hours and a fiber volume fraction of 10%, 15%, and 20%. Composite fiber from coconut coir with UPRs 157 BQTN matrix with MEXPO hardener. Mechanical testing is carried out using the ASTM D790 standard and the impact test using the ASTM D5941 standard. The impact test of natural fiber composites showed the impact toughness of the composite at a fiber volume fraction of 20% with a value of 0.017588 J/ mm2. The test results showed an increase in volume fraction and an effect on the increase in the bending strength of coconut fiber composites with the optimum bending strength at a fiber volume fraction of 10% with a value of 44.33N /mm2. This shows that the increase in fiber volume fraction by immersion in 15% NaOH will increase the bending mechanical properties and the impact of the composite. Soaking NaOH has an effect on the absorption power of coconut coir on the Unsaturated Polyester matrix which can increase the adhesion between the fiber reinforcement and the matrix thereby increasing the bending mechanical properties and impact of the composite.


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