scholarly journals Synthesis of Novel N1and N2Indazole Derivatives

2012 ◽  
Vol 9 (4) ◽  
pp. 1676-1682 ◽  
Author(s):  
Prasanna Bethanamudi ◽  
Srinivas Bandari ◽  
Kanakaraju Sankari ◽  
Amarnath Velidandi ◽  
G. V. P. Chandramouli

The alkylation of 5-cyano indazoles 2 in the presence of readily available imidizolium salts (ionic liquids) (Bmim)BF4as phase transfer catalyst were performed to afford the regio isomersN1-andN2-(substituted alkyl)-5-cyano indazoles. TheN1-alkylated cyano indazoles were converted to the correspondingN1-(substituted alkyl)-5-aminomethyl and 5-carbaldehydes5(a-f)and6(a-f).

RSC Advances ◽  
2011 ◽  
Vol 1 (9) ◽  
pp. 1721 ◽  
Author(s):  
Vineet Kumar ◽  
Ian Jamie Talisman ◽  
Omar Bukhari ◽  
Jacqueline Razzaghy ◽  
Sanjay V. Malhotra

2020 ◽  
Vol 303 ◽  
pp. 112607 ◽  
Author(s):  
Emil Szepiński ◽  
Patrycja Smolarek ◽  
Maria J. Milewska ◽  
Justyna Łuczak

Tetrahedron ◽  
2016 ◽  
Vol 72 (14) ◽  
pp. 1773-1781 ◽  
Author(s):  
Zujin Yang ◽  
Xia Zhang ◽  
Xingdong Yao ◽  
Yanxiong Fang ◽  
Hongyan Chen ◽  
...  

2014 ◽  
Vol 625 ◽  
pp. 267-270 ◽  
Author(s):  
Sintayehu Mekuria Hailegiorgis ◽  
Mahadzir Shuhaimi ◽  
Duvvuri Subbarao

In the present work, microwave heat pretreatment of jatropha curcas seed particles and use of phase transfer catalyst (PTC) to enhance in-situ transesterification were utilized together. It was observed that use of alkaline BTMAOH as a PTC and microwave heat pretreatment of jatropha curcas seed particles had substantially increased the reaction rate of in-situ transesterification as compared to the reaction conducted with microwave untreated seeds in the absence of BTMAOH as a PTC. Statistical model equation was developed to investigate the interaction effect of reaction variables and establish optimum reaction condition. At optimum condition, experimentally obtained FAME yield (93.7±1.53% w/w) was in close agreement with statistical model predicted FAME yield (96.75%) at 38°C and 37 minutes of reaction time.


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