scholarly journals Ultrasound Promoted Synthesis of 3-Carboxycoumarins in Aqueous Media

2006 ◽  
Vol 3 (1) ◽  
pp. 1-4 ◽  
Author(s):  
Jian-Long Du ◽  
Li-Jun Li ◽  
Da-Hai Zhang

An efficient and green procedure has been developed for synthesis of 3-carboxycoumarins, the reaction can be carried out in water under ultrasound irradiation, avoiding addition of catalyst

Synthesis ◽  
2020 ◽  
Vol 52 (11) ◽  
pp. 1707-1718
Author(s):  
Nasser Etivand ◽  
Jabbar Khalafy ◽  
Mohammad G. Dekamin

A simple, clean, straightforward, and environmentally benign one-pot, three-component reaction of various arylglyoxal monohydrates, β-naphthol, and barbituric acid [pyrimidine-2,4,6(1H,3H,5H)-trione] or thiobarbituric acid in the presence of catalytic amounts potassium phthalimide-N-oxyl (PPINO), as a mild and efficient organocatalyst in aqueous media under reflux conditions is reported. This transformation produced the novel diverse-substituted 12-benzoyl-8,12-dihydro-9H-benzo[5,6]chromeno[2,3-d]pyrimidine-9,11(10H)-diones and their sulfur analogues in 82–93% yield via filtration and without utilization of any chromatography. The high yields of products, very simple operation, easy workup, availability of starting materials, green process, and high atom-economy are the main benefits of this synthetic strategy.


2007 ◽  
Vol 8 (8) ◽  
pp. 1214-1218 ◽  
Author(s):  
Mohammad Ali Zolfigol ◽  
Peyman Salehi ◽  
Arash Ghaderi ◽  
Morteza Shiri

2004 ◽  
Vol 34 (6) ◽  
pp. 993-1000 ◽  
Author(s):  
Jin‐Hui Yang ◽  
Ji‐Tai Li ◽  
Jun‐Ling Zhao ◽  
Tong‐Shuang Li

2015 ◽  
Vol 70 (3) ◽  
pp. 171-176 ◽  
Author(s):  
Shahrzad Abdolmohammadi ◽  
Maryam Afsharpour

AbstractA green, efficient and simple protocol was developed for the synthesis of dihydropyrimido[4,5-d]pyrimidinetrione derivatives via a coupling reaction of 6-aminouracils, aromatic aldehydes and urea in aqueous media in the presence of nano-crystalline CuI at room temperature. The products were obtained in high yields. CuI nanoparticles can be recycled three times without significant loss of catalytic activity.


2009 ◽  
Vol 6 (5) ◽  
pp. 323-326 ◽  
Author(s):  
F. Silva ◽  
M. Galluzzi ◽  
B. Albuquerque ◽  
L. Pizzuti ◽  
V. Gressler ◽  
...  

2021 ◽  
Vol 08 ◽  
Author(s):  
Thais Cristina Mendonça Nogueiraa ◽  
Marcus Vinicius Nora de Souza

: Five- and six-membered N-heterocyclic compounds play an important role in medicinal chemistry and in the development of new drugs. In this manner, there is a constant demand for the development of novel biologically potent compounds and there is also an increasing pressure to develop alternative and more sustainable synthetic methodologies following the Green Chemistry principles. Thus, the present review aims to compile the latest progress in the use of ultrasound irradiation in water conditions to mediate the synthesis of five- and six-membered N-heterocyclic compounds in an environmentally benign manner.


ChemInform ◽  
2010 ◽  
Vol 41 (34) ◽  
pp. no-no
Author(s):  
Zi-Qiang Tang ◽  
Yan Chen ◽  
Chang-Ning Liu ◽  
Ke-Ying Cai ◽  
Shu-Jiang Tu

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