X-ray powder diffraction data for new ternary phases in the Al–Ti–Pt system

2008 ◽  
Vol 23 (4) ◽  
pp. 360-362 ◽  
Author(s):  
O. Zaikina ◽  
D. Pavlyuchkov ◽  
V. Khorujaya ◽  
T. Velikanova
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Hexagonal Structure ◽  
Tetragonal Structure ◽  
Equiatomic Composition ◽  
Powder Diffraction Data ◽  
Space Group ◽  
X Ray ◽  
Space Groups ◽  
Compositional Range

Two ternary phases, designated τ4 and τ5, were revealed in Al–Ti–Pt. The τ4-phase with equiatomic composition (i.e., AlTiPt) was found to have a hexagonal structure with a=4.3908(9) Å and c=5.4823(10) Å (space group P63/mmc), and the τ5-phase, forming in a compositional range between ∼ Al14Ti58Pt28 and Al21Ti63Pt16, has a tetragonal structure (possible space groups P42nm, P-4n2, and P42/mnm). The refined lattice parameters for Al15Ti60Pt25 are a=9.7019(20) Å and c=5.0231 (13) Å.

X-ray powder diffraction data for ω and C2 phases of Al–Cu–Ir

2008 ◽  
Vol 23 (4) ◽  
pp. 356-359 ◽  
Author(s):  
B. Grushko ◽  
D. Pavlyuchkov
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Tetragonal Structure ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
Structure Space ◽  
Cubic Structure

Ternary Al–Cu–Ir phases, isostructural to the Al–Cu–Rh ω and C2 phases, were found to be around the Al70Cu20Ir10 and Al60Cu15Ir25 compositions, respectively. Using powder X-ray diffraction, the former was found to have a tetragonal structure (space group P4/mnc) with a=6.4142(9) Å and c=14.842(4) Å, and the latter has a cubic structure (space group Fm3) with a=15.3928(6) Å.

X-ray powder diffraction data and Rietveld refinement for a new iodate: (LiFe1/3)(IO3)2

2002 ◽  
Vol 17 (2) ◽  
pp. 132-134
Author(s):  
Y. C. Lan ◽  
X. L. Chen ◽  
Z. Tao ◽  
A. Y. Xie ◽  
P. Z. Jiang ◽  
...  
Keyword(s):  
Rietveld Refinement ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Hexagonal Structure ◽  
Lattice Parameters ◽  
Powder Diffraction Data ◽  
Cation Site ◽  
Space Group ◽  
X Ray

The structure of a new iodate, (LiFe1/3)(IO3)2, has been determined. The new compound has a hexagonal structure with the lattice parameters a=5.4632(2) Å, c=5.0895(6) Å, Z=1. The density is 4.70 g cm−3. Rietveld refinement confirms that the compound has a space group of P63 (173). Fe and Li atoms randomly distribute on the 2a cation site.

X-ray powder diffraction data for three red azo pigments: sodium, barium, and ammonium lithol salts

2017 ◽  
Vol 32 (3) ◽  
pp. 187-192 ◽  
Author(s):  
Alicja Rafalska-Łasocha ◽  
Marta Grzesiak-Nowak ◽  
Piotr Goszczycki ◽  
Katarzyna Ostrowska ◽  
Wiesław Łasocha
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Monoclinic Space Group ◽  
Powder Diffraction Data ◽  
Space Group ◽  
X Ray ◽  
Space Groups ◽  
Cell Parameters ◽  
Synthesis Procedure ◽  
Diffraction Patterns

Lithol reds belong to the group of azo pigments, which were popular artists’ colouring materials in the first half of the twentieth century. These pigments were also used in many branches of industry. Here, we report X-ray powder diffraction data, unit-cell parameters, and space groups for three compounds from this group: sodium (E)-2-((2-hydroxynaphthalen-1-yl)diazenyl)naphthalene-1-sulphonate monohydrate (Na lithol red), monoclinic, space group C2/c, with cell parameters a = 33.343(7), b = 6.667(2), c = 16.397(4) Å, β = 90.83°, V = 3644.51 Å3, Z = 8; barium (E)-2-[(2-hydroxynaphthalen-1-yl)diazenyl]naphthalene-1-sulphonate trihydrate (Ba lithol red), monoclinic, space group P21/m, with cell parameters a = 17.758(9), b = 6.209(4), c = 16.857(8) Å, β = 92.07°, V = 1857.39 Å3, Z = 2; and ammonium (E)-2-[(2-hydroxynaphthalen-1-yl)diazenyl]naphthalene-1-sulphonate monohydrate (NH4 lithol red), monoclinic, space group P2/c, with cell parameters a = 17.721(5), b = 6.428(3), c = 16.911(5) Å, β = 100.31(3)°, V = 1895.31 Å3, and Z = 4. In the first and third cases we synthesised the pigments in their monohydrate form, performed X-ray powder diffraction measurements, and indexed all of the obtained diffraction maxima. In the case of the barium compound, despite many efforts in the course of the synthesis procedure, the powder diffraction patterns of the obtained samples were not of the best quality. Nevertheless, we indexed the best one and found a reliable space group and cell parameters.

Powder diffraction data of the PrAlFeNi3 quaternary compound

2014 ◽  
Vol 29 (4) ◽  
pp. 393-395
Author(s):  
Bing He ◽  
Ming Qin ◽  
Degui Li ◽  
Liuqing Liang ◽  
Lingmin Zeng
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Structure Type ◽  
Hexagonal Structure ◽  
Powder Pattern ◽  
Powder Diffraction Data ◽  
Quaternary Compound ◽  
Space Group ◽  
X Ray ◽  
Structure Space

A new quaternary compound PrAlFeNi3 was synthesized and studied by means of X-ray powder diffraction technique. The powder pattern of PrAlFeNi3 was indexed and refined, giving a hexagonal structure, space group P6/mmm (No. 191) with the CaCu5 structure type, a = 5.1132(2) Å, c = 4.0737(1) Å, V = 92.19 Å3, Z = 1, ρx = 7.20 g cm−3, F30 = 173.61 (0.0054, 32) and RIR = 0.77.

X-ray powder diffraction data for Al-Cu-W phases

2011 ◽  
Vol 26 (1) ◽  
pp. 70-73 ◽  
Author(s):  
B. Grushko ◽  
S. B. Mi
Keyword(s):  
Phase Space ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Ternary Phase ◽  
Hexagonal Structure ◽  
Powder Diffraction Data ◽  
Average Composition ◽  
Space Group ◽  
X Ray ◽  
Type Phase

Ternary Al-Cu-W alloys were investigated. The previously reported Al3Ti-type phase (space group I4/mmm) with the average composition Al67Cu11.5W21.5 was found to have a=3.7296(4) Å and c=8.3797(10) Å. The ternary phase forming around Al67Cu21W12 has a hexagonal structure with a=8.6594(13) Å and c=15.2677(21) Å.

Powder diffraction data of the AlCeCo2Ni2 quaternary compound

2016 ◽  
Vol 31 (3) ◽  
pp. 240-241
Author(s):  
Liuqing Liang ◽  
Chenzhong Jia ◽  
Degui Li ◽  
Lingmin Zeng ◽  
RanCheng Mo
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Structure Type ◽  
Hexagonal Structure ◽  
Powder Pattern ◽  
Powder Diffraction Data ◽  
Quaternary Compound ◽  
Space Group ◽  
X Ray ◽  
Structure Space

A new quaternary compound AlCeCo2Ni2 was synthesized and studied by means of X-ray powder diffraction technique. The powder pattern of AlCeCo2Ni2 was indexed and refined, giving a hexagonal structure, space group P6/mmm (No. 191) with the CaCu5 structure type. a = 4.9242(2) Å, c = 4.0524(1) Å, V = 85.1 Å3, Z = 1, ρx = 7.85 g cm−3, F30 = 130.2(0.010, 30), and RIR = 0.71(2).

X-ray powder diffraction data for the N-acylamino acids: ortho, meta, and para-methyl hippuric acids

2016 ◽  
Vol 31 (3) ◽  
pp. 242-247
Author(s):  
Gerzon E. Delgado ◽  
Marilia Guillén ◽  
Jeans W. Ramírez ◽  
Asiloé J. Mora ◽  
Jines E. Contreras ◽  
...  
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Powder Diffraction Data ◽  
Unit Cell Parameters ◽  
Space Group ◽  
X Ray ◽  
Space Groups ◽  
Cell Parameters ◽  
Methylhippuric Acid ◽  
Diffraction Peaks

N-acylamino acid isomers: ortho, meta, and para-methylhippuric acids, are specific xylene metabolites. Here, we report X-ray powder diffraction data, unit-cell parameters, and space groups for the three isomer (C10H11NO3), [ortho-methylhippuric acid 2 mHA, monoclinic P21/n cell, a = 8.522(1), b = 10.443(1), c = 10.734(1) Å, β = 92.43(1)°, V = 954.5(1) Å3; meta-methylhippuric acid 3 mHA, monoclinic C2/c cell a = 20.0951(2), b = 10.485(1), c = 10.074(2) Å, β = 119.08(1)°, V = 1933.9(1) Å3; para-methylhippuric acid 4 mHA, orthorhombic P212121 cell, a = 5.1794(7), b = 8.279(1), c = 22.276(2) Å, V = 955.2(2) Å3], space group. In each case, all measured diffraction peaks were indexed and are consistent with the corresponding space group.

Powder X-ray data for the ammonium trioxalatoaluminate (III) and its hydrates: (NH4Al(C2O4)3·xH2O, x=0,2,3

1995 ◽  
Vol 10 (3) ◽  
pp. 195-197 ◽  
Author(s):  
Mohamed Ezahri ◽  
Georges Coffy ◽  
Bernard F. Mentzen
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Powder Diffraction Data ◽  
Space Group ◽  
X Ray ◽  
Space Groups ◽  
The Stability

X-ray powder diffraction data are reported for the trihydrated (A3N), the dihydrated (A2N), and the anhydrous ammonium trioxalatoaluminate (III) (AN). A3N is triclinic with space group . A2N and AN are monoclinic with space groups P21/c and P21/n respectively. The stability domains are A3N: –7.8 to 86 °C; A2N: 86 to 102 °C; AN: 102 to 180 °C.

X-ray powder diffraction data for Ba3MnSi2O8—A new phase in the system BaO–MnO–SiO2

1996 ◽  
Vol 11 (1) ◽  
pp. 26-27 ◽  
Author(s):  
Irena Georgieva ◽  
Ivan Ivanov ◽  
Ognyan Petrov
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Data Interpretation ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Space Group ◽  
X Ray ◽  
New Phase

A new compound—Ba3MnSi2O8 in the system BaO–MnO–SiO2 was synthesized and studied by powder X-ray diffraction. The compound is hexagonal, space group—P6/mmm, a=5.67077 Å, c=7.30529 Å, Z=1, Dx=5.353. The obtained powder X-ray diffractometry (XRD) data were interpreted by the Powder Data Interpretation Package.

X-ray powder diffraction data for tetrazene nitrate monohydrate, C2H9N11O4

2021 ◽  
pp. 1-3
Author(s):  
J. Maixner ◽  
J. Ryšavý
Keyword(s):  
Cell Volume ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell Volume ◽  
Unit Cell ◽  
Powder Diffraction Data ◽  
Unit Cell Parameters ◽  
Space Group ◽  
X Ray ◽  
Cell Parameters

X-ray powder diffraction data, unit-cell parameters, and space group for tetrazene nitrate monohydrate, C2H9N11O4, are reported [a = 5.205(1) Å, b = 13.932(3) Å, c = 14.196(4) Å, β = 97.826(3)°, unit-cell volume V = 1019.8(4) Å3, Z = 4, and space group P21/c]. All measured lines were indexed and are consistent with the P21/c space group. No detectable impurities were observed.

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