D001 Studies of local and intermediate range structure in crystalline, nanocrystalline and amorphous materials at high pressure using high-energy X-rays—invited

2006 ◽  
Vol 21 (2) ◽  
pp. 179-179
Author(s):  
J. B. Parise ◽  
S. Antao ◽  
F. M. Michel ◽  
C. D. Martin ◽  
L. Ehm ◽  
...  
Keyword(s):  
High Pressure ◽  
Amorphous Materials ◽  
High Energy ◽  
X Rays ◽  
Intermediate Range ◽  
Nanocrystalline And Amorphous

Studies of local and intermediate range structure in crystalline and amorphous materials at high pressure using high-energy X-rays

2007 ◽  
Vol 22 (2) ◽  
pp. 108-112 ◽  
Author(s):  
Lars Ehm ◽  
Sytle M. Antao ◽  
Jiuhua Chen ◽  
Darren R. Locke ◽  
F. Marc Michel ◽  
...  
Keyword(s):  
Phase Transition ◽  
High Pressure ◽  
Atomic Structure ◽  
Amorphous Materials ◽  
High Energy ◽  
Liquid Gallium ◽  
X Rays ◽  
X Ray ◽  
X Ray Scattering ◽  
Current State

The method of high-energy total elastic X-ray scattering to determine the atomic structure of nanocrystalline, highly disordered, and amorphous materials is presented. The current state of the technique, its potential, and limitations are discussed with two successful studies on the pressure induced phase transition in mackinawite (FeS) and the high-pressure behavior of liquid gallium.

Density measurements of liquid under high pressure and high temperature

1998 ◽  
Vol 5 (3) ◽  
pp. 1023-1025 ◽  
Author(s):  
Yoshinori Katayama ◽  
Kazuhiko Tsuji ◽  
Osamu Shimomura ◽  
Takumi Kikegawa ◽  
Mohamed Mezouar ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Synchrotron Radiation ◽  
High Energy ◽  
X Rays ◽  
Sample Container ◽  
Density Measurements ◽  
X Ray ◽  
Sample Shape ◽  
X Ray Absorption

A new method for density measurements by means of X-ray absorption under high pressure and high temperature using synchrotron radiation has been developed. The method has been modified for a large-volume Paris–Edinburgh press and combined with intense high-energy X-rays at the ESRF. In order to overcome effects of deformation of sample shape under pressure, a ruby cylinder was used as a sample container. The density was determined from the intensity profile of transmitted X-rays. The densities of crystalline and liquid Bi were successfully measured up to 750 K at 1 GPa.

Miniature diamond anvils for X-ray Raman scattering spectroscopy experiments at high pressure

2017 ◽  
Vol 24 (1) ◽  
pp. 276-282 ◽  
Author(s):  
Sylvain Petitgirard ◽  
Georg Spiekermann ◽  
Christopher Weis ◽  
Christoph Sahle ◽  
Christian Sternemann ◽  
...  
Keyword(s):  
High Pressure ◽  
Raman Scattering ◽  
Signal To Noise Ratio ◽  
High Energy ◽  
X Rays ◽  
Signal To Noise ◽  
X Ray ◽  
Custom Made ◽  
Diamond Anvils ◽  
Noise Ratio

X-ray Raman scattering (XRS) spectroscopy is an inelastic scattering method that uses hard X-rays of the order of 10 keV to measure energy-loss spectra at absorption edges of light elements (Si, Mg, Oetc.), with an energy resolution below 1 eV. The high-energy X-rays employed with this technique can penetrate thick or dense sample containers such as the diamond anvils employed in high-pressure cells. Here, we describe the use of custom-made conical miniature diamond anvils of less than 500 µm thickness which allow pressure generation of up to 70 GPa. This set-up overcomes the limitations of the XRS technique in very high-pressure measurements (>10 GPa) by drastically improving the signal-to-noise ratio. The conical shape of the base of the diamonds gives a 70° opening angle, enabling measurements in both low- and high-angle scattering geometry. This reduction of the diamond thickness to one-third of the classical diamond anvils considerably lowers the attenuation of the incoming and the scattered beams and thus enhances the signal-to-noise ratio significantly. A further improvement of the signal-to-background ratio is obtained by a recess of ∼20 µm that is milled in the culet of the miniature anvils. This recess increases the sample scattering volume by a factor of three at a pressure of 60 GPa. Examples of X-ray Raman spectra collected at the OK-edge and SiL-edge in SiO2glass at high pressures up to 47 GPa demonstrate the significant improvement and potential for spectroscopic studies of low-Zelements at high pressure.

The Basic Physical Principles of Ion, Electron, and X-Ray Detectors and Their Application to Microanalysis

1985 ◽  
Vol 43 ◽  
pp. 154-157
Author(s):  
A.J. Tousimis
Keyword(s):  
Ion Beam ◽  
Depth Resolution ◽  
Sample Surface ◽  
High Energy ◽  
X Rays ◽  
X Ray ◽  
Electrons And Ions ◽  
Spatial Depth ◽  
Minimum Surface Area ◽  
Physical Principles

An integral and of prime importance of any microtopography and microanalysis instrument system is its electron, x-ray and ion detector(s). The resolution and sensitivity of the electron microscope (TEM, SEM, STEM) and microanalyzers (SIMS and electron probe x-ray microanalyzers) are closely related to those of the sensing and recording devices incorporated with them.Table I lists characteristic sensitivities, minimum surface area and depth analyzed by various methods. Smaller ion, electron and x-ray beam diameters than those listed, are possible with currently available electromagnetic or electrostatic columns. Therefore, improvements in sensitivity and spatial/depth resolution of microanalysis will follow that of the detectors. In most of these methods, the sample surface is subjected to a stationary, line or raster scanning photon, electron or ion beam. The resultant radiation: photons (low energy) or high energy (x-rays), electrons and ions are detected and analyzed.

“Cartography” in 7-Dimensions at CHESS: Mapping of Structure in Real Space, Reciprocal Space, and Time Using High-Energy X-rays

2020 ◽  
Vol 33 (6) ◽  
pp. 11-16
Author(s):  
K. E. Nygren, ◽  
D. C. Pagan, ◽  
J. P. C. Ruff ◽  
E. Arenholz ◽  
J. D. Brock
Keyword(s):  
High Energy ◽  
Real Space ◽  
Reciprocal Space ◽  
X Rays ◽  
Space And Time

scholarly journals The interstellar medium in young supernova remnants: key to the production of cosmic X-rays and $\gamma $-rays

2021 ◽  
Vol 366 (6) ◽  
Author(s):  
Hidetoshi Sano ◽  
Yasuo Fukui
Keyword(s):  
Interstellar Medium ◽  
Supernova Remnants ◽  
Cosmic Ray ◽  
High Energy ◽  
X Rays ◽  
Interstellar Gas ◽  
High Energy Radiation ◽  
Dense Cores ◽  
The Relationship ◽  
Turbulent Velocity Field

AbstractWe review recent progress in elucidating the relationship between high-energy radiation and the interstellar medium (ISM) in young supernova remnants (SNRs) with ages of ∼2000 yr, focusing in particular on RX J1713.7−3946 and RCW 86. Both SNRs emit strong nonthermal X-rays and TeV $\gamma $ γ -rays, and they contain clumpy distributions of interstellar gas that includes both atomic and molecular hydrogen. We find that shock–cloud interactions provide a viable explanation for the spatial correlation between the X-rays and ISM. In these interactions, the supernova shocks hit the typically pc-scale dense cores, generating a highly turbulent velocity field that amplifies the magnetic field up to 0.1–1 mG. This amplification leads to enhanced nonthermal synchrotron emission around the clumps, whereas the cosmic-ray electrons do not penetrate the clumps. Accordingly, the nonthermal X-rays exhibit a spatial distribution similar to that of the ISM on the pc scale, while they are anticorrelated at sub-pc scales. These results predict that hadronic $\gamma $ γ -rays can be emitted from the dense cores, resulting in a spatial correspondence between the $\gamma $ γ -rays and the ISM. The current pc-scale resolution of $\gamma $ γ -ray observations is too low to resolve this correspondence. Future $\gamma $ γ -ray observations with the Cherenkov Telescope Array will be able to resolve the sub-pc-scale $\gamma $ γ -ray distribution and provide clues to the origin of these cosmic $\gamma $ γ -rays.

scholarly journals Introducing the HD+B model for pulsar wind nebulae: a hybrid hydrodynamics/radiative approach

2020 ◽  
Vol 494 (3) ◽  
pp. 4357-4370
Author(s):  
B Olmi ◽  
D F Torres
Keyword(s):  
Gamma Ray ◽  
High Energy ◽  
Theoretical Modelling ◽  
X Rays ◽  
Pulsar Wind Nebulae ◽  
New Approach ◽  
Energy Gamma ◽  
Radiative Model ◽  
Pulsar Wind

ABSTRACT Identification and characterization of a rapidly increasing number of pulsar wind nebulae is, and will continue to be, a challenge of high-energy gamma-ray astrophysics. Given that such systems constitute -by far- the most numerous expected population in the TeV regime, such characterization is important not only to learn about the sources per se from an individual and population perspective, but also to be able to connect them with observations at other frequencies, especially in radio and X-rays. Also, we need to remove the emission from nebulae in highly confused regions of the sky for revealing other underlying emitters. In this paper, we present a new approach for theoretical modelling of pulsar wind nebulae: a hybrid hydrodynamic-radiative model able to reproduce morphological features and spectra of the sources, with relatively limited numerical cost.

X‐ray determination of the Debye temperature at high pressure using high‐energy synchrotron radiation

1990 ◽  
Vol 68 (6) ◽  
pp. 2719-2722 ◽  
Author(s):  
A. Matsumuro ◽  
M. Kobayashi ◽  
T. Kikegawa ◽  
M. Senoo
Keyword(s):  
High Pressure ◽  
Synchrotron Radiation ◽  
Debye Temperature ◽  
High Energy ◽  
X Ray
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