scholarly journals X-ray powder diffraction analysis of methionine sulfoxide

2001 ◽  
Vol 16 (3) ◽  
pp. 163-164
Author(s):  
Pedro P. Corbi ◽  
Petr Melnikov ◽  
Antonio C. Massabni
Keyword(s):  
Amino Acid ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Methionine Sulfoxide ◽  
X Ray Diffraction ◽  
X Ray ◽  
Cell Parameters ◽  
Monoclinic Cell

Powder X-ray diffraction data for methionine sulfoxide, C5H11NO3S, obtained from the commercial amino acid, are presented in this work. Monoclinic cell parameters are: a=15.500 Å; b=3.820 Å; c=13.490 Å; β=97.300 °.

scholarly journals X-ray powder diffraction analysis of a new palladium(II) amino acid complex

2004 ◽  
Vol 19 (3) ◽  
pp. 270-271 ◽  
Author(s):  
Pedro P. Corbi ◽  
Antonio C. Massabni ◽  
Claudio M. Costa-Neto
Keyword(s):  
Amino Acid ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Acid Complex ◽  
X Ray ◽  
Cell Parameters ◽  
Amino Acid Complex ◽  
Orthorhombic Cell

Powder X-ray diffraction data for a new palladium(II) amino acid complex, of composition PdC12H20N2O4S2, are presented in this paper. Orthorhombic cell parameters are: a=10.740 Å, b=19.999 Å, and c=5.2470 Å. © 2004 International Centre for Diffraction Data.

X-ray diffraction data of C16H14O4Ru2M (M=Ge,Si)

2002 ◽  
Vol 17 (1) ◽  
pp. 44-47
Author(s):  
Yu PuLan ◽  
Ding Shuang ◽  
Qiao YuanYuan ◽  
Yao XinKan ◽  
Liu Chong ◽  
...  
Keyword(s):  
Single Crystal ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Space Group ◽  
X Ray ◽  
Cell Parameters ◽  
Monoclinic Cell ◽  
Good Agreement

Two compounds have been studied by means of powder diffraction and their unit cell parameters are reported. The monoclinic cell parameters for dimethylgermanyl-bridged bis cyclopentadienyl tetracarbonyl diruthenium are a=11.03(2) Å, b=13.65(2) Å, c=11.609(2) Å, β=105.81(1)°, Z=4, space group P21/n (No. 14), Dx=2.135 mg/m3. The monoclinic cell parameters for λ-dimethylsilyl-dicyclopentadienyl-π, π′-tetracarbonyl diruthenium, are a=11.113(3) Å, b=13.60(1) Å, c=11.674(7) Å, and β=106.00(3)°, Z=4, space group P21/n (No. 14), and Dx=1.946 mg/m3. The cells found for the two compounds are in good agreement with those obtained from single crystal X-ray diffractometry.

X-ray powder diffraction analysis of tegafur

2006 ◽  
Vol 21 (3) ◽  
pp. 245-247 ◽  
Author(s):  
F. Needham ◽  
J. Faber ◽  
T. G. Fawcett ◽  
D. H. Olson
Keyword(s):  
Single Crystal ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Antineoplastic Agent ◽  
X Ray Diffraction ◽  
Triclinic Crystal System ◽  
X Ray ◽  
Cell Parameters ◽  
Structural Database

An experimental X-ray powder diffraction pattern was produced and analyzed for alpha-polymorphic tegafur, also called Ftorafur (an antineoplastic agent). The indexed data matched the powder patterns in the ICDD PDF-4/Organics database calculated from the reported single-crystal X-ray diffraction data in the Cambridge Structural Database. Alpha tegafur has a triclinic crystal system, with reduced cell parameters of a=16.720(6) Å, b=9.021(5) Å, c=5.995(3) Å, α=93.66(4)°, β=93.15(8)°, γ=100.14(4)°. There are four formula units contained in one unit cell. The cell volume and space group were determined to be 886.27 Å3 and P-1, respectively.

X-ray-diffraction data of Pb2(C2O4)(NO3)2·2H2O

1996 ◽  
Vol 11 (1) ◽  
pp. 7-8 ◽  
Author(s):  
Hee-Lack Choi ◽  
Nobuo Ishizawa ◽  
Naoya Enomoto ◽  
Zenbe-e Nakagawa
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Crystal System

X-ray powder-diffraction data for Pb2(C2O4)(NO3)2·2H2O were obtained. The crystal system was determined to be monoclinic. The unit-cell parameters were refined to a=10.613(2) Å, b=7.947(2) Å, c=6.189(1) Å, and β=104.48(2)°.

Synthesis and powder X-ray diffraction data of a new iron phosphate Fe(PO4)·0.5H2O

1998 ◽  
Vol 13 (4) ◽  
pp. 246-248 ◽  
Author(s):  
Nubuo Ishizawa ◽  
Atsushi Saiki ◽  
Kyoji Ohdan ◽  
Mamoru Ai
Keyword(s):  
Water Vapor ◽  
Oxalic Acid ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Iron Phosphate ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters

X-ray powder-diffraction data were collected for a new iron phosphate, Fe(PO4)·0.5H2O, obtained by reducing FePO4 with oxalic acid at 220 °C in the presence of water vapor and oxygen. The crystal system was determined to be orthorhombic with unit-cell parameters a=15.991(6) Å, b=20.156(7) Å, and c=7.223(2) Å.

X-ray diffraction analysis of (Na0.6H0.4)(Ta0.7Nb0.3)O3

1999 ◽  
Vol 14 (3) ◽  
pp. 231-233 ◽  
Author(s):  
Raj P. Singh ◽  
Michael J. Miller ◽  
Jeffrey N. Dann
Keyword(s):  
High Temperature ◽  
Diffraction Analysis ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Type Structure ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
X Ray

(Na0.6H0.4)(Ta0.7Nb0.3)O3 was synthesized by heating a tantalum/niobium scale containing two sodium tantalate/niobate phases :Na14(Ta0.7Nb0.3)12O37·31H2O and NaH2Ta0.7Nb0.3O4. Powder X-ray diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 indicated it to be a cubic perovskite (ABO3/ReO3 type structure) with unit cell a0=3.894 Å. The compound is analogous to the mineral lueshite (NaNbO3), and to the high temperature forms of NaTaO3 and NaNbO3. Powder diffraction data for (Na0.6H0.4)(Ta0.7Nb0.3)O3 will be useful in the analysis of synthetic tantalum/niobium concentrates.

X-ray diffraction data of Ti2O2(C2O4)(OH)2·H2O

1994 ◽  
Vol 9 (3) ◽  
pp. 187-188 ◽  
Author(s):  
Hee-Lack Choi ◽  
Naoya Enomoto ◽  
Nobuo Ishizawa ◽  
Zenbe-e Nakagawa
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Space Group ◽  
X Ray ◽  
Cell Parameters ◽  
Crystal System

X-ray powder diffraction data for Ti2O2(C2O4)(OH)2·H2O were obtained. The crystal system was determined to be orthorhombic with space group C2221. The unit cell parameters were refined to a = 1.0503(2) nm, b = 1.5509(3) nm, and c = 0.9700(1) nm.

X-ray powder diffraction analysis of imipenem monohydrate

2012 ◽  
Vol 27 (1) ◽  
pp. 20-24
Author(s):  
F. Needham ◽  
C. E. Crowder ◽  
J. W. Reid ◽  
T. G. Fawcett ◽  
J. Faber
Keyword(s):  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Orthorhombic Crystal ◽  
X Ray ◽  
Cell Parameters ◽  
Pharmaceutical Agent ◽  
Structural Database

An experimental X-ray powder diffraction pattern was produced and analyzed for imipenem monohydrate, an antimicrobial pharmaceutical agent. Although there are no experimental powder patterns in the ICDD PDF-4/Organics Database, there is one powder pattern calculated with single-crystal X-ray diffraction data from the Cambridge Structural Database. Here, we report the refined experimental powder diffraction data for imipenem monohydrate. These data for imipenem monohydrate are consistent with an orthorhombic crystal system having reduced unit-cell parameters of a = 8.2534(3) Å, b = 11.1293(4) Å, and c = 15.4609(6) Å. The resulting unit-cell volume, 1420.15(15) Å3, indicates four formula units per unit cell. Observed peaks are consistent with the P212121 space group.

X-ray powder diffraction data of lapatinib ditosylate monohydrate

2009 ◽  
Vol 24 (3) ◽  
pp. 250-253 ◽  
Author(s):  
Peter Varlashkin
Keyword(s):  
Breast Cancer ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Room Temperature ◽  
Powder Diffraction Data ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
X Ray ◽  
Cell Parameters ◽  
Diffraction Structure

The room temperature powder pattern of lapatinib ditosylate monohydrate (active ingredient in Tykerb used to treat refractory breast cancer) was indexed and the cell from the single crystal X-ray diffraction structure was refined using the experimental capillary data. Unit-cell parameters for the orthorhombic compound with space group Pbca refined from powder diffraction data are a=9.6850±0.0009 Å, b=29.364±0.003 Å, and c=30.733±0.003 Å, α=β=γ=90°, z=8, V=8740.1 Å3. Values of 2θ, d, I, and Miller indices are reported.

Synthesis and X-ray diffraction data of 1-N-(4-pyridylmethyl)amino naphthalene

2010 ◽  
Vol 25 (1) ◽  
pp. 72-74 ◽  
Author(s):  
H. A. Camargo ◽  
J. A. Henao ◽  
D. F. Amado ◽  
V. V. Kouznetsov
Keyword(s):  
Diffraction Pattern ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Unit Cell ◽  
X Ray Diffraction ◽  
Unit Cell Parameters ◽  
Monoclinic System ◽  
Space Group ◽  
X Ray ◽  
Cell Parameters

1-N-(4-pyridylmethyl)amino naphtalene was synthesized by means of a reaction of alpha-naphthylamine, 4-pyridylcarboxyaldehyde, in anhydrous ethanol to obtainN-(4-pyridylen)-alpha-naphthylamine and that was reduced with NaBH4 to produce the wanted compound. The X-ray powder diffraction pattern for the new compound 1-N-(4-pyrydylmethyl)amino naphtalene was obtained. This compound crystallizes in a monoclinic system with refined unit cell parameters a=10.375(5) Å, b=17.665(6) Å, c=5.566(2) Å, β=100.11(3), and V=1004.3(5) Å3, with space group P2/m (No. 10).

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