Investigations of an Electrodeposited Tin‐Nickel Alloy: I . Thermal Stability by Differential Thermal Analysis and X‐Ray Diffraction

1976 ◽  
Vol 123 (7) ◽  
pp. 999-1003 ◽  
Author(s):  
J. E. Bennett ◽  
H. G. Tompkins
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Nickel Alloy ◽  
X Ray Diffraction ◽  
X Ray

Thermal Stability vs. Crystallization of the Lithiumsilicate Glasses with Addition Zirconium Dioxide and Titanium Dioxide

2008 ◽  
Vol 39-40 ◽  
pp. 399-401
Author(s):  
Viliam Pavlík ◽  
Eugen Jóna ◽  
Martina Sapietová ◽  
Soňa Šnircová
Keyword(s):  
Activation Energy ◽  
Thermal Stability ◽  
Thermal Analysis ◽  
Titanium Dioxide ◽  
Differential Thermal Analysis ◽  
Structural Analysis ◽  
Zirconium Dioxide ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Relationship

The glasses with composition of Li2O . 2 SiO2 . n ZrO2 . n TiO2 (where n = 0; 0.015; 0.031; 0.050; 0.075; 0.1; 0.15; 0.2) were prepared and the relationship between structural and selected parameters of thermal stability vs. crystallization has been studied by differential thermal analysis. Structural analysis was provided by X–ray diffraction. The order of thermal stability vs. crystallization representing of activation energy of studied glass systems which increase with higher addition both oxides. The same order was obtained from the values of XRD. On the comparison the glasses with zero addition titanium dioxide their activation energy was much higher.

Identification and Thermal Stability of Copper(I) Sulfate

1972 ◽  
Vol 50 (23) ◽  
pp. 3872-3875 ◽  
Author(s):  
Kim Vo Van ◽  
Fathi Habashi
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Thermogravimetric Analysis ◽  
Diffraction Pattern ◽  
Chemical Processes ◽  
X Ray Diffraction ◽  
X Ray ◽  
Thermal Stability Of

Anhydrous CU2SO4 was prepared and its X-ray diffraction pattern was established. Differential thermal analysis, thermogravimetric analysis, and X-ray diffraction methods were used to study the effect of heating in different atmospheres. The formation of CU2SO4 as an intermediate in chemical processes has been discussed.

PENINGKATAN LAJU DISOLUSI ACYCLOVIR DENGAN METODE SISTEM DISPERSI PADAT MENGGUNAKAN POLOXAMER 188

2016 ◽  
Vol 5 (1) ◽  
pp. 6
Author(s):  
Budi Setiawan ◽  
Erizal Zaini ◽  
Salman Umar
Keyword(s):  
Electron Microscopy ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Fourier Transform ◽  
Differential Thermal Analysis ◽  
Fourier Transform Infrared ◽  
X Ray Diffraction ◽  
Poloxamer 188 ◽  
X Ray ◽  
Scanning Electron

Sebuah penelitian tentang sistem dispersi padat dari asiklovir dengan poloxamer 188 telah dilakukan formulasi dengan pencampuran secara fisika dengan rasio 1 : 1, 1 : 3, 1 : 5 dan dispersi padat 1 : 1, 1 : 3, 1 : 5 dan penggilingan 1:1 sebagai pembanding. Dispersi padat dibuat menggunakan metode pencairan (fusi), yang digabung dengan poloxamer 188 pada hotplate kemudian asiklovir dimasukkan ke dalam hasil poloxamer 188 lalu di kocok hingga membentuk masa homogen. Semua formula yang terbentuk termasuk asiklovir poloxamer 188 murni dianalisis karakterisasinya dengan Differential Thermal Analysis (DTA), X-ray Diffraction, Scanning Electron Microscopy (SEM), dan Fourier Transform Infrared (FTIR), kemudian pengambilan dilakukan  (penentuan kadar) mengunakan spektrofotometer UV pada panjang gelombang 257,08 nm dan uji laju disolusi dengan aquadest bebas CO2 menggunakan metode dayung. Hasil pengambilan  (penentuan kadar) menunjukkan bahwa semua formula memenuhi persyaratan farmakope Amerika edisi 30 dan farmakope Indonesia edisi 4 yaitu 95-110%. Sedangkan hasil uji laju disolusi untuk campuran fisik 1: 1, dan dispersi padat 1: 1, dan penggilingan 1: 1 menunjukkan peningkatan yang nyata dibandingkan asiklovir murni. Hal ini juga dapat dilihat dari hasil perhitungan statistik  menggunakan analisis varian satu arah  SPSS 17.

scholarly journals The Potential for Natural Stones from Northeastern Brazil to Be Used in Civil Construction

Minerals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 440
Author(s):  
Fabiana Pereira da Costa ◽  
Jucielle Veras Fernandes ◽  
Luiz Ronaldo Lisboa de Melo ◽  
Alisson Mendes Rodrigues ◽  
Romualdo Rodrigues Menezes ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Chemical Resistance ◽  
Mechanical Analysis ◽  
Northeastern Brazil ◽  
X Ray Diffraction ◽  
X Ray ◽  
Chemical Agents ◽  
Natural Stones

Natural stones (limestones, granites, and marble) from mines located in northeastern Brazil were investigated to discover their potential for use in civil construction. The natural stones were characterized by chemical analysis, X-ray diffraction, differential thermal analysis, and optical microscopy. The physical-mechanical properties (apparent density, porosity, water absorption, compressive and flexural strength, impact, and abrasion) and chemical resistance properties were also evaluated. The results of the physical-mechanical analysis indicated that the natural stones investigated have the potential to be used in different environments (interior, exterior), taking into account factors such as people’s circulation and exposure to chemical agents.

The Roman Ceramics of Salobrena (Granada-Spain) and their Raw Materials

1992 ◽  
Vol 267 ◽  
Author(s):  
Ana M De Andres ◽  
Isabel MuÑOZ
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Raw Materials ◽  
Third Century ◽  
Western Coast ◽  
X Ray Diffraction ◽  
X Ray ◽  
The Third ◽  
Good Number ◽  
Scanning Electron

ABSTRACTNineteen roman ceramic sherds found near Salobreña (Granada, Spain), in the western coast of the Mediterranean Sea, as well as different ceramic clays from the surroundingsare studied. Both clays and ceramic sherds are characterizad by X-ray diffraction and spectrometry, differential thermal analysis, and scanning electron and optical microscopies. A good number of the ceramic pieces, among which some “Terrae Sigillatae”, have a composition similar to that of the local clays and, thus, have been probably manufactured at Salobreña. Only a few of them have a foreign origin. For most of them, the firing temperature was about 800-850 °C, although some have been produced at 900-1000 °C, and some others at 1000-1100 °C. It is concluded that Salobreña appearsto have been an important settlement just in the third century of the Christian era.

scholarly journals Silica-Kaolin Mix Effect on Evaporative Pattern Castings Surface Roughness

2016 ◽  
Vol 16 (3) ◽  
pp. 83-88 ◽  
Author(s):  
B.V. Omidiji ◽  
R.H. Khan ◽  
M.S. Abolarin
Keyword(s):  
Thermal Analysis ◽  
Surface Roughness ◽  
Differential Thermal Analysis ◽  
Ratio Method ◽  
Gating System ◽  
X Ray Diffraction ◽  
Pouring Temperature ◽  
Material Loss ◽  
Refractory Coating ◽  
X Ray

Abstract The influence of the refractory coating which is a mixture of silica flour and kaolin on the surface roughness of the plate castings produced using evaporative patterns had been considered in this work. The kaolin was used as a binder and ratio method was employed to form basis for the factorial design of experiment which led to nine runs of experiments. Methyl alcohol at 99% concentration was used as the carrier for the transfer of the coating to the surface of the patterns. Pouring temperature was observed as a process parameter alongside the mix ratios of the coating. Attempts were made to characterize the refractory coating by using two methods; differential thermal analysis (DTA) and X-ray diffraction. Attempt was also made to characterize the casting material. Gating system design was done for the plate casting to determine the correct proportions of the gating parameters in order to construct the gating system properly to avoid turbulence during pouring of liquid metal. A digital profilometer was used to take the measurements of the surface roughness. It was observed that the mix ratio 90% silica flour-10% kaolin produced the lowest value of the surface roughness of the plate castings and had the lowest material loss in the DTA test. The pouring temperature of 650°C produced best casting.

scholarly journals SOLUBILITY OF GERMANIUM DISELENIDE IN THE Cu3AsSe4

2021 ◽  
Vol 0 (4) ◽  
pp. 67-70
Author(s):  
Z.T. Hasanova ◽  
Keyword(s):  
Thermal Analysis ◽  
Differential Thermal Analysis ◽  
Phase Equilibria ◽  
Solid Solutions ◽  
X Ray Diffraction ◽  
X Ray

Differential thermal analysis and powder X-ray diffraction methods were used for phase equilibria studying in the Cu3AsSe4-GeSe2 system. It was established that wide (up to 30 mol.%) solid solutions based on Cu3AsSe4 are formed. GeSe2-rich alloys consist of various heterogeneous mixtures, including phases outside the T–x plane of this section

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