Epitaxial Growth of PbS Thin Films from Aqueous Solution

1990 ◽  
Vol 137 (9) ◽  
pp. 2697-2700 ◽  
Author(s):  
M. Isshiki ◽  
T. Endo ◽  
K. Masumoto ◽  
Y. Usui
1996 ◽  
Vol 427 ◽  
Author(s):  
R. T. Tung

AbstractThe phenomenon of Ti-interlayer mediated epitaxy (TIME) of CoSi2 on Si(100) has attracted much academic and technological interest. As yet, the role of the interlayer, Ti, is not fully understood. The various drawbacks of the TIME process have driven the search for a better interlayer. New results are presented which demonstrate the efficacy of a thin SiOx layer, grown in a peroxide-containing aqueous solution, in inducing nearly perfect epitaxial growth of CoSi2 on practically all surfaces of Si. This technique, dubbed oxide mediated epitaxy (OME), allows a thin layer of epitaxial CoSi2 to grow sub-surface, leaving the SiOx layer largely on the surface of the silicide. An interesting result of the surface oxide cap is a significant re-evaporation of cobalt observed during deposition at elevated temperatures. Thicker (10-30nm), excellent quality, CoSi2 single crystal thin films have been grown by repeated growth sequences on Si(100), (110), (211) and (511). Nearly perfect type A oriented CoSi2 layers were grown on Si(111) using mixed A/B oriented template layers.


1999 ◽  
Vol 606 ◽  
Author(s):  
Keishi Nishio ◽  
Jirawat Thongrueng ◽  
Yuichi Watanabe ◽  
Toshio Tsuchiya

AbstructWe succeeded in the preparation of strontium-barium niobate (Sr0.3Ba0.7Nb2O6 : SBN30)that have a tetragonal tungsten bronze type structure thin films on SrTiO3 (100), STO, or La doped SrTiO3 (100), LSTO, single crystal substrates by a spin coating process. LSTO substrate can be used for electrode. A homogeneous coating solution was prepared with Sr and Ba acetates and Nb(OEt)5 as raw materials, and acetic acid and diethylene glycol monomethyl ether as solvents. The coating thin films were sintered at temperature from 700 to 1000°C for 10 min in air. It was confirmed that the thin films on STO substrate sintered above 700°C were in the epitaxial growth because the 16 diffraction spots were observed on the pole figure using (121) reflection. The <130> and <310> direction of the thin film on STO were oriented with the c-axis in parallel to the substrate surface. However, the diffraction spots of thin film on LSTO substrate sintered at 700°C were corresponds to the expected pattern for (110).


2018 ◽  
Vol 6 (1) ◽  
pp. 22-30
Author(s):  
C. Lalhriatpuia ◽  
◽  
Thanhming liana ◽  
K. Vanlaldinpuia

The photocatalytic activity of Nanopillars-TiO2 thin films was assessed in the degradation of Bromophenol blue (BPB) dye from aqueous solution under batch reactor operations. The thin films were characterized by the XRD, SEM and AFM analytical methods. BET specific surface area and pore sizes were also obtained. The XRD data showed anatase phase of TiO2 particles with average particle size of 25.4 and 21.9 nm, for S1 and S2 catalysts respectively. The SEM and AFM images indicated the catalyst composed with Nanosized pillars of TiO2, evenly distributed on the surface of the substrate. The average height of the pillars was found to be 180 and 40 nm respectively for the S1 and S2 catalyst. The BET specific surface area and pore sizes of S1 and S2 catalyst were found to be 5.217 and 1.420 m2/g and 7.77 and 4.16 nm respectively. The photocatalytic degradation of BPB using the UV light was studied at wide range of physico-chemical parametric studies to determine the mechanism of degradation as well as the practical applicability of the technique. The batch reactor operations were conducted at varied pH (pH 4.0 to 10.0), BPB initial concentration (1.0 to 20.0 mg/L) and presence of several interfering ions, i.e., cadmium nitrate, copper sulfate, zinc chloride, sodium chloride, sodium nitrate, sodium nitrite, glycine, oxalic acid and EDTA in the photocatalytic degradation of BPB. The maximum percent removal of BPB was observed at pH 6.0 and a low initial concentration of the pollutant highly favours the photocatalytic degradation using thin films. The presence of several interfering ions suppressed the photocatalytic activity of thin films to some extent. The time dependence photocatalytic degradation of BPB was demonstrated with the pseudo-first-order rate kinetics. Study was further extended with total organic carbon measurement using the TOC (Total Organic Carbon) analysis. This demonstrated an apparent mineralization of BPB from aqueous solutions.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 724
Author(s):  
Tong Li ◽  
Masaya Ichimura

Magnesium hydroxide (Mg(OH)2) thin films were deposited by the drop-dry deposition (DDD) method using an aqueous solution containing Mg(NO3)2 and NaOH. DDD was performed by dropping the solution on a substrate, heating-drying, and rinsing in water. Effects of different deposition conditions on the surface morphology and optical properties of Mg(OH)2 thin films were researched. Films with a thickness of 1−2 μm were successfully deposited, and the Raman peaks of Mg(OH)2 were observed for them. Their transmittance in the visible range was 95% or more, and the bandgap was about 5.8 eV. It was found that the thin films have resistivity of the order of 105 Ωcm. Thus, the transparent and semiconducting Mg(OH)2 thin films were successfully prepared by DDD.


2021 ◽  
pp. 130119
Author(s):  
Ik-Jae Lee ◽  
Hee Seob Kim ◽  
Young Duck Yun ◽  
Seen-Woong Kang ◽  
Hyo-Yun Kim ◽  
...  

2016 ◽  
Vol 45 (43) ◽  
pp. 17312-17318 ◽  
Author(s):  
Eun-Kyung Kim ◽  
Dasom Park ◽  
Nabeen K. Shrestha ◽  
Jinho Chang ◽  
Cheol-Woo Yi ◽  
...  

An aqueous solution based synthetic method for binder-free Ag2Te thin films using ion exchange induced chemical transformation of Ag/AgxO thin films.


1999 ◽  
Vol 19 (6-7) ◽  
pp. 1409-1412 ◽  
Author(s):  
S.M Zanetti ◽  
E.R Leite ◽  
E Longo ◽  
J.A Varela

2000 ◽  
Vol 18 (2) ◽  
pp. 536-542 ◽  
Author(s):  
Tomoko Wake ◽  
Koichiro Saiki ◽  
Atsushi Koma

1999 ◽  
Vol 85 (8) ◽  
pp. 4800-4802 ◽  
Author(s):  
J. Fontcuberta ◽  
M. Bibes ◽  
B. Martı́nez ◽  
V. Trtik ◽  
C. Ferrater ◽  
...  
Keyword(s):  

2003 ◽  
Vol 83 (26) ◽  
pp. 5500-5502 ◽  
Author(s):  
J.-R. Duclère ◽  
M. Guilloux-Viry ◽  
V. Bouquet ◽  
A. Perrin ◽  
E. Cattan ◽  
...  

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